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All Journal Wood Research Journal : Journal of Indonesian Wood Research Society Wood Research Journal : Journal of Indonesian Wood Research Society
Toshimitsu Hata
Laboratory of Innovative Humano-habitability Research Institute for Sustainable Humanosphere, Kyoto University Uji Campus, Gokasho, Uji, Kyoto 611-0011
Agriculture, Biological Sciences & Forestry

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 1 
The Changes in Microstructure and Thermal Constant in Conversion of Carbonized Wood to Silicon Carbide Composite Joko Sulistyo; Sri Nugroho Marsoem; Toshimitsu Hata
Wood Research Journal Vol 6, No 1 (2015): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2015.6.1.30-36

Abstract

Carbonized wood which possesses microstructure with random orientation graphitic crystallites and with pores between the graphitic crystallites, is potentially developed into new material of silicon carbide (SiC) composite, a high performance material for engineering purposes. This paper investigates the development of the microstructure in the turbostratic carbon phase and the formation of SiC crystal from the reaction of carbon and SiO2. Results show the turbostratic microstructure in carbonized wood lead to the possible formation of SiC compound in the manufacturing of SiC/SiO2/Ccomposite. The heat treatment at 1800ºC on the mixture of SO2 and carbonized wood creates the formation of SiC compound, which improves the degree of microstructure ordering. The improvement of microstructure turbostratic carbon and the growth of graphitic crystallites in turbostratic carbon improves the thermal conductivity of SiC/SiO2/C composite comparingwith those of carbonized wood composite.
Green Aromatics from Catalytic Fast Pyrolysis of Fast Growing Meranti Biomass Joko Sulistyo; Toshimitsu Hata; Sensho Honma; Ryohei Asakura; Sri Nugroho Marsoem
Wood Research Journal Vol 4, No 1 (2013): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2013.4.1.13-18

Abstract

The study on catalytic pyrolysis decomposition of Shorea leprosula wood biomass to form aromatic compounds in fast pyrolysis was performed by pyrolytic-gas chromatography/mass spectroscopy (Py-GC/MS) and transmission electron microscope (TEM) - electron energy-loss spectroscopy (EELS) to analyze the chemical compound and solid residue microstructure. Py-GC/MS and TEM-EELS analysis showed that the fast pyrolysis increased the decomposition of hardwood, in which in the presence of ZSM-5 catalyst, the liquid products from wood decomposition was then diffused into the pore of ZSM-5 catalyst to form aromatics including benzene, toluene, styrene, naphthalenes and indanes. The carbonaceous solid compounds or cokes were not deposited on the surface of pores of ZSM-5 catalyst in the fast pyrolysis, as shown by the EELS spectrum that exhibited no detection of any solid carbonaceous compound in the solid residue.
The Changes in Microstructure and Thermal Constant in Conversion of Carbonized Wood to Silicon Carbide Composite Joko Sulistyo; Sri Nugroho Marsoem; Toshimitsu Hata
Wood Research Journal Vol 6, No 1 (2015): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2015.6.1.30-36

Abstract

Carbonized wood which possesses microstructure with random orientation graphitic crystallites and with pores between the graphitic crystallites, is potentially developed into new material of silicon carbide (SiC) composite, a high performance material for engineering purposes. This paper investigates the development of the microstructure in the turbostratic carbon phase and the formation of SiC crystal from the reaction of carbon and SiO2. Results show the turbostratic microstructure in carbonized wood lead to the possible formation of SiC compound in the manufacturing of SiC/SiO2/Ccomposite. The heat treatment at 1800ºC on the mixture of SO2 and carbonized wood creates the formation of SiC compound, which improves the degree of microstructure ordering. The improvement of microstructure turbostratic carbon and the growth of graphitic crystallites in turbostratic carbon improves the thermal conductivity of SiC/SiO2/C composite comparingwith those of carbonized wood composite.
Green Aromatics from Catalytic Fast Pyrolysis of Fast Growing Meranti Biomass Joko Sulistyo; Toshimitsu Hata; Sensho Honma; Ryohei Asakura; Sri Nugroho Marsoem
Wood Research Journal Vol 4, No 1 (2013): Wood Research Journal
Publisher : Masyarakat Peneliti Kayu Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.51850/wrj.2013.4.1.13-18

Abstract

The study on catalytic pyrolysis decomposition of Shorea leprosula wood biomass to form aromatic compounds in fast pyrolysis was performed by pyrolytic-gas chromatography/mass spectroscopy (Py-GC/MS) and transmission electron microscope (TEM) - electron energy-loss spectroscopy (EELS) to analyze the chemical compound and solid residue microstructure. Py-GC/MS and TEM-EELS analysis showed that the fast pyrolysis increased the decomposition of hardwood, in which in the presence of ZSM-5 catalyst, the liquid products from wood decomposition was then diffused into the pore of ZSM-5 catalyst to form aromatics including benzene, toluene, styrene, naphthalenes and indanes. The carbonaceous solid compounds or cokes were not deposited on the surface of pores of ZSM-5 catalyst in the fast pyrolysis, as shown by the EELS spectrum that exhibited no detection of any solid carbonaceous compound in the solid residue.
Co-Authors Joko Sulistyo Joko Sulistyo Ryohei Asakura Sensho Honma Sri Nugroho Marsoem Sri Nugroho Marsoem