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All Journal Bulletin of Electrical Engineering and Informatics Bulletin of Electrical Engineering and Informatics Bulletin of Electrical Engineering and Informatics Indonesian Journal of Electrical Engineering and Computer Science
A. S. Ismail
Universiti Teknologi MARA (UiTM)
Computer Science & IT Electrical & Electronics Engineering Engineering

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Effect of substrate placement in schott vial to hematite properties Wan Rosmaria Wan Ahmad; M. H. Mamat; A. S. Zoolfakar; Z. Khusaimi; A. S. Ismail; T. N. T. Yaakub; M. Rusop
Bulletin of Electrical Engineering and Informatics Vol 8, No 1: March 2019
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1283.262 KB) | DOI: 10.11591/eei.v8i1.1391

Abstract

In the present study, hematite (α-Fe2O3) nanostructures were deposited on fluorine doped tin oxide (FTO) coated glass substrate using sonicated immersion synthesis method. The effect of FTO glass substrate placement in Schott vial during immersion process was studied on the growth of the hematite nanostructure and its properties. XRD pattern has revealed seven diffraction peaks of α-Fe2O3 for both hematite nanostructures samples attributed to polycrystalline with rhombohedral lattice structure. The surface morphologies from FESEM have shown that the hematite nanostructures were grown uniformly in both samples with FTO conductive layer facing up and down. Hematite sample with FTO facing down exhibits a smaller size of nanorod, 26.7 nm average diameter, compared to the hematite sample that FTO face up with 53.8nm average diameter. Optical properties revealed higher transmittance in the sample with FTO facing down, probably due to smaller size of nanostructure. The optical band gap energy plotted and extrapolated at 2.50eV and 2.55eV for FTO face up and FTO face down hematite samples respectively, presenting the sample with FTO face up has a lower optical bandgap energy.
Effect of substrate placement in schott vial to hematite properties Wan Rosmaria Wan Ahmad; M. H. Mamat; A. S. Zoolfakar; Z. Khusaimi; A. S. Ismail; T. N. T. Yaakub; M. Rusop
Bulletin of Electrical Engineering and Informatics Vol 8, No 1: March 2019
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (911.043 KB) | DOI: 10.11591/eei.v8i1.1391

Abstract

In the present study, hematite (α-Fe2O3) nanostructures were deposited on fluorine doped tin oxide (FTO) coated glass substrate using sonicated immersion synthesis method. The effect of FTO glass substrate placement in Schott vial during immersion process was studied on the growth of the hematite nanostructure and its properties. XRD pattern has revealed seven diffraction peaks of α-Fe2O3 for both hematite nanostructures samples attributed to polycrystalline with rhombohedral lattice structure. The surface morphologies from FESEM have shown that the hematite nanostructures were grown uniformly in both samples with FTO conductive layer facing up and down. Hematite sample with FTO facing down exhibits a smaller size of nanorod, 26.7 nm average diameter, compared to the hematite sample that FTO face up with 53.8nm average diameter. Optical properties revealed higher transmittance in the sample with FTO facing down, probably due to smaller size of nanostructure. The optical band gap energy plotted and extrapolated at 2.50eV and 2.55eV for FTO face up and FTO face down hematite samples respectively, presenting the sample with FTO face up has a lower optical bandgap energy.
Effect of substrate placement in schott vial to hematite properties Wan Rosmaria Wan Ahmad; M. H. Mamat; A. S. Zoolfakar; Z. Khusaimi; A. S. Ismail; T. N. T. Yaakub; M. Rusop
Bulletin of Electrical Engineering and Informatics Vol 8, No 1: March 2019
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1283.262 KB) | DOI: 10.11591/eei.v8i1.1391

Abstract

In the present study, hematite (α-Fe2O3) nanostructures were deposited on fluorine doped tin oxide (FTO) coated glass substrate using sonicated immersion synthesis method. The effect of FTO glass substrate placement in Schott vial during immersion process was studied on the growth of the hematite nanostructure and its properties. XRD pattern has revealed seven diffraction peaks of α-Fe2O3 for both hematite nanostructures samples attributed to polycrystalline with rhombohedral lattice structure. The surface morphologies from FESEM have shown that the hematite nanostructures were grown uniformly in both samples with FTO conductive layer facing up and down. Hematite sample with FTO facing down exhibits a smaller size of nanorod, 26.7 nm average diameter, compared to the hematite sample that FTO face up with 53.8nm average diameter. Optical properties revealed higher transmittance in the sample with FTO facing down, probably due to smaller size of nanostructure. The optical band gap energy plotted and extrapolated at 2.50eV and 2.55eV for FTO face up and FTO face down hematite samples respectively, presenting the sample with FTO face up has a lower optical bandgap energy.
Influence of annealing temperature on the sensitivity of nickel oxide nanosheet films in humidity sensing applications N. Parimon; M. H. Mamat; A. S. Ismail; I. B. Shameem Banu; M. K. Ahmad; A. B. Suriani; M. Rusop
Indonesian Journal of Electrical Engineering and Computer Science Vol 18, No 1: April 2020
Publisher : Institute of Advanced Engineering and Science

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.11591/ijeecs.v18.i1.pp284-292

Abstract

Nickel oxide (NiO) nanosheet films were successfully grown onto NiO seed-coated glass substrates at different annealing temperatures for humidity sensing applications. NiO seed layers and NiO nanosheet films were prepared using a sol-gel spin coating and sonicated sol-gel immersion techniques, respectively. The properties of NiO nanosheet films at as-deposited, 300 ℃, and 500 ℃-annealed were examined by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), ultraviolet-visible (UV-vis) spectroscopy, and humidity sensor measurement system. The XRD patterns demonstrate that the grown NiO films have crystalline cubic structures at temperature of 300 ℃ and 500 ℃. The FESEM images show that the large porous nanosheet network spread over the layers as the annealing temperature increased. The UV-vis spectra revealed that all the nanosheet films have the average transmittance below than 50% in the visible region, with absorption edges ~ 350 nm. The optical band gap energy was evaluated in ranges of 3.39 to 3.61 eV. From the obtained humidity sensing results, it shows that 500 ℃-annealed film exhibited the best sensitivity of 257, as well as the slowest response time, and the fastest recovery time compared with others.
Co-Authors A. B. Suriani A. S. Zoolfakar I. B. Shameem Banu M. H. Mamat M. K. Ahmad M. Rusop N. Parimon T. N. T. Yaakub Wan Rosmaria Wan Ahmad Z. Khusaimi