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All Journal JURNAL REKAYASA KIMIA & LINGKUNGAN
Koichi Fujie
Department of Ecological Engineering, Toyohashi University of Technology, Toyohashi
Chemical Engineering, Chemistry & Bioengineering Energy Engineering

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Rapid Determination of Microbial Quinones using Supercritical CO2 Extraction Faisal, Muhammad; Irvan, Irvan; Atsuta, Yoichi; Daimon, Hiroyuki; Fujie, Koichi
Jurnal Rekayasa Kimia & Lingkungan Vol 5, No 1 (2006): Jurnal Rekayasa Kimia & Lingkungan
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

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The supercritical CO2 extraction of microbial quinones from activated sludge samples obtained from various activated sludge was investigated and compared to the conventional method using organic solvent extraction. The extraction was carried out in a supercritical fluid extraction (SFE) system in the temperature range of 25 to75 oC and the pressure up to 30 MPa. Different extraction conditions, such as the temperature, pressure, extraction time and modifier were employed to maximize the SFE efficiency. Significant amount of microbial quinones (ubiquinones and menaquinones) could be extracted rapidly with supercritical CO2. Results on the value of diversity and dissimilarity suggested that the SFE with supercritical CO2 extraction was a reliable technique for quinones extraction.
Recovery of Organic and Amino Acids from Sludge and Fish Waste in Sub Critical Water Conditions Faisal, Muhammad; Daimon, Hiroyuki; Fujie, Koichi
Jurnal Rekayasa Kimia & Lingkungan Vol 8, No 2 (2011): Jurnal Rekayasa Kimia & Lingkungan
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

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The possibility of organic and amino acid production from the treatment of sludge and fish waste using water at sub critical conditions was investigated. The results indicated that at sub-critical conditions, where the ion product of water went through a maximum, the formation of organic acids was favorable. The presence of oxidant favored formation of acetic and formic acid. Other organic acids of significant amount were propionic, succinic and lactic acids. Depending on the type of wastes, formation of other organic acids was also possible. Knowing the organic acids obtained by hydrolysis and oxidation in sub-critical water of various wastes are useful in designing of applicable waste treatment process, complete degradation of organic wastes into volatile carbon and water, and also on the viewpoint of resource recovery. The production of lactic acid was discussed as well. The results indicated that temperature of 573 K, with the absence of oxidant, yield of lactic acid from fish waste was higher than sewage sludge. The maximum yield of total amino acids (137 mg/g-dry fish) from waste fish entrails was obtained at subcritical condition (T = 523 K, P = 4 MPa) at reaction time of 60 min by using the batch reactor. The amino acids obtained in this study were mainly alanine and glycine.Keywords: organic acids, amino acids, sub-critical water, hydrothermal, resources recovery
Co-Authors Hiroyuki Daimon Irvan Irvan Muhammad Faisal Yoichi Atsuta