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SITI HAJAR SHEIKH MD FADZULLAH
Faculty of Mechanical Engineering, Universiti Teknikal Malaysia Melaka, Hang Tuah Jaya, 76100, Durian Tunggal, Melaka, Malaysia
Agriculture, Biological Sciences & Forestry Astronomy Biochemistry, Genetics & Molecular Biology Chemistry Earth & Planetary Sciences Energy Immunology & microbiology Neuroscience Physics

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Determination of the crystallite size and crystal structure of magnesium powder by x-ray diffraction ISMAIL ISMAIL; RESI MULIANI; ZULFALINA ZULFALINA; SITI HAJAR SHEIKH MD FADZULLAH
Jurnal Natural Volume 20 Number 3, October 2020
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (338.682 KB) | DOI: 10.24815/jn.v20i3.16584

Abstract

Magnesium powder has become an important material in the development of science and technology such as alloy and hydrogen storage. In this work, the chemical composition, crystallite size, and crystal structure of the magnesium powder sample have been studied by using x-ray fluorescent and x-ray diffraction. The x-ray diffraction data of the magnesium powder sample was analyzed by using the Rietveld method to obtain the crystal structure. Our results show that the purity of our magnesium powder sample is 93.1%. Our sample has good crystallinity with the average crystallite size of 31 nm. The crystal structure is found to be a hexagonal closed-packed structure with the lattice constants of 3.2100 Å (a and b-axis) and 5.2107 Å (c-axis). Our result revealed that the lattice constant in the c-axis of magnesium powder is influenced by impurity. This finding suggests that the impurity can affect the crystal structure of a material in general.
Determination of the crystallite size and crystal structure of magnesium powder by x-ray diffraction ISMAIL ISMAIL; RESI MULIANI; ZULFALINA ZULFALINA; SITI HAJAR SHEIKH MD FADZULLAH
Jurnal Natural Volume 20 Number 3, October 2020
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jn.v20i3.16584

Abstract

Magnesium powder has become an important material in the development of science and technology such as alloy and hydrogen storage. In this work, the chemical composition, crystallite size, and crystal structure of the magnesium powder sample have been studied by using x-ray fluorescent and x-ray diffraction. The x-ray diffraction data of the magnesium powder sample was analyzed by using the Rietveld method to obtain the crystal structure. Our results show that the purity of our magnesium powder sample is 93.1%. Our sample has good crystallinity with the average crystallite size of 31 nm. The crystal structure is found to be a hexagonal closed-packed structure with the lattice constants of 3.2100 Å (a and b-axis) and 5.2107 Å (c-axis). Our result revealed that the lattice constant in the c-axis of magnesium powder is influenced by impurity. This finding suggests that the impurity can affect the crystal structure of a material in general.
Co-Authors ISMAIL ISMAIL RESI MULIANI ZULFALINA ZULFALINA