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All Journal Indonesian Journal of Chemistry
Hilyati Hilyati
Pusat Penelitian Kimia –LIPI, Kawasan PUSPIPTEK-Serpong
Chemical Engineering, Chemistry & Bioengineering Chemistry

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Innovative High-Speed Homogenizer Approach for Synthesizing PVDF-GO Membranes from Recycled Battery Graphite Febriasari, Arifina; Ferdiansyah, Ferry; Salsabila, Shafa Marwa; Ridwan, Muhammad; Mahardika, Muhammad Bagas Adhistya; Hilyati, Hilyati; Sudjarwo, Wisnu Arfian Anditya; Arlofa, Nina; Supriyadi, Supriyadi; Toca-Herrera, Jose Luis; Kartohardjono, Sutrasno
Indonesian Journal of Chemistry Vol 25, No 5 (2025)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.103909

Abstract

Effective waste management is essential for achieving a zero-waste environment, particularly in handling hazardous domestic waste like used dry cell batteries. This study explores a sustainable approach by recovering graphite from battery waste to synthesize graphene oxide (GO) for enhancing poly-vinylidene fluoride (PVDF) membranes. GO was synthesized using the Hummers method and a modified high-speed homogenization approach, then characterized via Raman spectroscopy and X-ray diffraction (XRD). The fabricated PVDF-GO membranes were further analyzed using SEM-EDS, AFM, water contact angle measurements, and bacterial rejection tests. Results confirmed successful GO synthesis and integration into the polymer matrix. GO incorporation improved hydrophilicity, reducing the water contact angle from 120° (pure PVDF) to 66° and 56° in PVDF/PVP-GO membranes via high-speed homogenization and conventional methods, respectively. The modified membranes exhibited a 5–6 times larger pore size than pure PVDF and achieved nearly 100% bacterial rejection. Additionally, PVDF/PVP-GO(h) showed a 91.76% faster production time efficiency than PVDF/PVP-GO(s).
Co-Authors Arlofa, Nina Febriasari, Arifina Ferry Ferdiansyah, Ferry Mahardika, Muhammad Bagas Adhistya Muhammad Ridwan Salsabila, Shafa Marwa Sudjarwo, Wisnu Arfian Anditya Supriyadi Supriyadi Sutrasno Kartohardjono Toca-Herrera, Jose Luis