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Erasti Pratiwi
Brawijaya University
Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology Medicine & Pharmacology

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Modification of Screen Printed Carbon Electrode (SPCE) with Polypyrrole (Ppy)-SiO2 for Phenol Determination Erasti Pratiwi; Ani Mulyasuryani; Akhmad Sabarudin
The Journal of Pure and Applied Chemistry Research Vol 7, No 1 (2018): Edition January-April 2018
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (884.633 KB) | DOI: 10.21776/ub.jpacr.2018.007.01.364

Abstract

Electrode modification on screen printed carbon electrode (SPCE) with polypyrrole (Ppy)-SiO2 was done by electropolymerization. Polypyrrole (Ppy)-SiO2 was used for phenol determination. The analysis of this material was done by using Scanning Electron Microscopy (SEM), cyclic voltammetry method and differential pulse voltammetry. In a cyclic voltammetry analysis, we used potential range of -1 to 1 V with Ag/AgCl comparator electrode at scan rate of 100 mV/sec, while in differential pulse voltammetry method the potential range was 0 to 1 V toward Ag/AgCl, the scan rate of 50 mV/sec, the pulse rate is 0,2 V and the pulse width is 50 ms. From the analysis result with SEM, cyclic voltammetry and differential pulse voltammetry method, Polypyrrole (Ppy) -SiO2 is the best material and can be used as phenol measurement.
Co-Authors Akhmad Sabarudin Ani Mulyasuryani