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All Journal JURNAL KIMIA SAINS DAN APLIKASI Jurnal Ilmu Dasar BERKALA SAINSTEK Bulletin of Chemical Reaction Engineering & Catalysis Warta Pengabdian Indonesian Physical Review Indonesian Chimica Letters Molekul: Jurnal Ilmiah Kimia InSTEM Bulletin of Chemical Reaction Engineering & Catalysis
Yudi Aris Sulistiyo, Yudi Aris
Jurusan Kimia, Fakultas Matematika Dan Ilmu Pengetahuan Alam, Universitas Jember
Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Control & Systems Engineering Education Engineering Materials Science & Nanotechnology Mathematics Physics Other

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Synthesis zeolitic Imidazolate Framework-8 (Zif-8) In Solvothermal: The Effect Comparison of Metal-Ligand Muhammad Nadjib; Ratna Ediati; Yudi Aris Sulistiyo; Lutfiatun Nadifah
Jurnal ILMU DASAR Vol 17 No 1 (2016)
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (214.748 KB) | DOI: 10.19184/jid.v17i1.2674

Abstract

Synthesis of ZIF-8 (zeolitic Imidazolate Frameworks-8) have been successfully carried out by the reaction of zinc nitrate and 2-methylimidazolate in DMF (N'N-dimethylformamide) solvent at a temperature of 120 °C for 24 hours. Synthesis of ZIF-8 has been conducted five times with variations molar ratio of metal (Zn2+):ligand (MeIM) consecutive 1:1; 1:1.5; 1:2; 1:2.5 and 1:3 to study the influence of metal-ligand ratio of the crystallinity and morphology of ZIF-8 that was produced. The results of characterization by X-ray diffraction, FTIR and SEM show that ZIF-8 is synthesized with a ratio of metal: ligand = 1:2 showed the highest crystallinity and has the most irregular surface morphology with form box. Keywords: ZIF-8, solvotermal, metal/ligand ratio 
Silica Gels from Coal Fly Ash as Methylene Blue Adsorbent: Isotherm and Kinetic Studies Yudi Aris Sulistiyo; Nida Andriana; Bambang Piluharto; Zulfikar Zulfikar
Bulletin of Chemical Reaction Engineering & Catalysis 2017: BCREC Volume 12 Issue 2 Year 2017 (August 2017)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (16.758 KB) | DOI: 10.9767/bcrec.12.2.766.263-272

Abstract

A lot of dye pollutants were released in the aquatic environment as waste from industrial coloring process. This research aimed to study silica gels (SG) as a potential adsorbent to remove the dyes. The SG can be synthesized from coal fly ash (FA), which is industrial solid waste rarely utilized, using the sol-gel method. Its properties were then characterized by FTIR, XRD, SEM, and isothermal ads-des N2. As a result, FTIR spectra and XRD diffractogram exhibited the successfully SG synthesized from FA with the amorphous structure. The image analysis using SEM demonstrated that SG particles are spherical. The isotherm type, based on isotherm ads-des N2, is type II without hysteresis loop which represents the nonporous material SG with the surface area and pore diameter of 25.977 m2/g and 1.52 nm, respectively. The adsorption capacity performance of SG to remove methylene blue (MB) as a basic dye is 62.70 % which is higher than FA, following Langmuir isotherm adsorption model. The kinetics of adsorption rate of SG are based on the pseudo second order models accelerated by 3.37 times faster than FA. 
Biobriket Arang Sekam Padi sebagai Sumber Energi Terbarukan untuk Aplikasi Pandai Besi Wenny Maulina; Yudi Aris Sulistiyo; Endhah Purwandari
Warta Pengabdian Vol 14 No 4 (2020): Warta Pengabdian
Publisher : LP2M Universitas Jember

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Abstract

Sumber energi terbarukan berbasis biomassa merupakan sumber daya potensial menggantikan kayu bakar atau batu bara yang persediannya semakin menipis sebagai bahan bakar industri pandai besi. Salah satu potensi biomassa adalah sekam padi yang dapat dijadikan bahan baku pembuatan biobriket. Oleh karena itu, tujuan pelaksanaan kegiatan ini adalah untuk menghasilkan biobriket arang sekam padi sebagai bahan bakar alternatif pada industri pandai besi. Kegiatan ini dilakukan dalam beberapa tahapan yaitu 1) pembuatan alat pencetak yang mampu menghasilkan 4 buah biobriket sekali produksi, 2) pembuatan biobriket arang sekam dan diuji sifat dan karakteristiknya, dan 3) pelatihan pembuatan dan penerapan langsung biobriket untuk proses pemanasan besi pada industri pandai besi. Karakteristik biobriket arang sekam diuji berdasarkan nilai kapasitas kalor, kadar air, kadar abu, dan volatile matter berturut–turut adalah 3709,47 kalori per gram; 4,27%; 3,93%; dan 59,20%. Hasil pengujian pembakaran secara langsung menghasilkan nyala api berwarna biru dengan suhu berkisar 533,8 – 704,3 oC. Hasil biobriket telah diimplementasikan dan mampu diterima untuk menggantikan kayu bakar yang selama ini digunakan pada sentra pengrajin pandai besi di Desa Suger Kidul, Kec. Jelbuk, Kab. Jember.
The Application of Slow Sand Filtration Technology for Improving Water Quality at Taman Gading Housing Area, Kaliwates District, Jember Muflihah, Yeni Maulidah; Utomo, Denny Trias; Handayani, Wuryanti; Sulistiyo, Yudi Aris; Andarini, Novita; Asnawati, Asnawati; Indarti, Dwi
Jurnal Inovasi Sains dan Teknologi untuk Masyarakat Vol. 1 No. 2 (2023): November
Publisher : Faculty of Mathematics and Natural Sciences, University of Jember. Jl. Kalimantan No.37, Krajan Timur, Jemberlor, Kec. Sumbersari, Jember Regency, East Java 68121

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/instem.v1i2.470

Abstract

Water is a basic need for all living organisms. Water quality implies living quality. Several parameters influencing water quality include minerals, dissolved organic substances, and turbidity. The water consumed must meet proven water quality standards. However, water quality still needs to be improved in several areas before consumption. The well water in residential areas placed on rice fields generally needs to meet the requirements for consumption. Many Taman Gading housing complex residents, especially in RW 036 RT 006, still use the well water to meet their daily needs. The well water quality in this area tends to be smelly and somewhat misty. Proper treatment is needed to improve the quality of well water in this area to reduce the negative impact on the population's health in the long term. This training focused on well water purification and filtration using slow sand filtration technology (SPL) to improve water quality. This method uses activated charcoal, sand, gauze, and pumice as filter media in specific proportions. The use of this method is effective and efficient in reducing the turbidity level of the sample water to the threshold for drinking water (<500 ppm), with a neutral pH (close to 7.00). This technology is effortless for residents to use and apply independently at a relatively low cost.
Synthesis of Zeolite Y from Lapindo Mud with the Comparative Variation of the Weight of NaOH/Mud and Molar SiO2/Al2O3 Andarini, Novita; Haryati, Tanti; Suwardiyanto, Suwardiyanto; Sulistiyo, Yudi Aris
Indonesian Chimica Letters Vol. 1 No. 1 (2022)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (514.618 KB) | DOI: 10.19184/icl.v1i1.5

Abstract

Lapindo mud is a waste that can be used as a zeolite formation material. Zeolite is a mineral there are silica and alumina. The zeolite synthesized was the zeolite Y. The synthesis of zeolite Y is carried out the melting method followed by hydrothermal process. The ratio of NaOH/sludge weight varied the weight of NaOH added to the sludge weight which was made constant, there were 1.1 gram of NaOH/1 gram of sludge; 1.3 gram of NaOH/1 gram of sludge; 1.5 gram of NaOH/1 gram of sludge; and 1.7 gram of NaOH/ 1 gram of sludge. The sludge was pretreated using HCl in the leaching process and NaOH for smelting. The melted sludge from the four variations was characterized using XRF. The results of characterization are used as the basis for determining the mass of SiO2 and NaOH that need to be added in the synthesis. The melted sludge was added with water, SiO2, and NaOH and cured for 48 hours at room temperature. The mixture that has been brooded is then filtered, the result of the filtering is the filtrate of sodium silicate and sodium aluminate solution. The filtrate was hydrothermal 100-105 °C for 24 hours. The resulting crystals were filtered and neutralized using aquademine. The resulting synthetic zeolite was white, then characterization was carried out using XRF and XRD. The characterization results on the variation of NaOH/sludge weight ratio could be seen from the XRF results. Zeolite Y varies the weight ratio of NaOH/sludge based on the character of the best zeolite produced at a weight ratio of NaOH/sludge 1.5.
Solid State Transformation of TiO2 Rutile and its Photocatalytic Activity Sulistiyo, Yudi Aris; Kamila, Wilda; Andarini, Novita; Suwardiyanto, Suwardiyanto; Sunnardianto, Gagus Ketut; Haryati, Tanti
Indonesian Chimica Letters Vol. 1 No. 2 (2022)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (716.495 KB) | DOI: 10.19184/icl.v1i2.205

Abstract

Transformation phase TiO2 Rutile was conducted to improve the photocatalytic activity. This study evaluated the transformation phase of TiO2 rutil using solid state rection method and tested for gycerol conversion reaction. a semiconductor material that can be applied for glycerol conversion. The solid state reaction using a mixture of TiO2 Rutile and sodium titanate in mole rasio 1:4 that was heated in 750 oC. XRD analysis evaluated the transformation phase of the solid state reaction product, while band gap energi was calculated following UV-Vis diffuse reflectance data. The photoactivity of glycerol was exposed by UV-Light in various time (5, 10, 15 h) that of the liquid product was analyzed by gas chromatography. Solid state reaction transformed TiO2 rutil to polymorph structure (TiO2 rutile, TiO2 anatase, and sodium titanate Na4O12Ti5). The band gap energy of the product was 3.2 eV. The optimum photocatalytic activity was 62.7% in glycerol concentration 0.25 M for 15 h time reaction.
Hydrothermal Synthesis of Hematite (α-Fe2O3) from Indonesia Iron Sand Furqonul Hakin Al Hadi; Tanti Haryati; Novita Andarini; Suwardiyanto; Sulistiyo, Yudi Aris
Indonesian Chimica Letters Vol. 2 No. 1 (2023)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/icl.v2i1.367

Abstract

High potency of Indonesian iron sand can be optimized by transforming to valuable iron oxide product namely Hematite (α-Fe2O3). Hydrothermal synthesis was carried out to transform iron oxide phase to hematite that can be analyzed by x-ray diffraction method. Utilization of ion sand as raw material produced multyphase in product reaction, while  the usage of Fe(OH)x that extracted from iron sand attained high purity of hematite. The best conditions of reaction were at 160 oC for 24 h. Higher temperature and longer time reaction transformed α- α-Fe2O3 to be γ-Al2O3 and Fe3O4 as more stable phase.
Synthesis and Characterisation of Bentonite/Poly(Acrylic Acid) Hybrid Material for Its Application as A Catalyst in Esterification of Glycerol with Acetic Acid Sholehah, Hidayati Nur Mohammad; Suwardiyanto; Tanti Haryati; Novita Andarini; Sulistiyo, Yudi Aris
Indonesian Chimica Letters Vol. 3 No. 1 (2024)
Publisher : Department of Chemistry, Faculty of Mathematics and Natural Sciences, University of Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/icl.v3i1.798

Abstract

Bentonite/poly(acrylic acid) (BTAA) hybrid material commonly applied as superabsorbent was prepared via intercalation method coupled with in situ polymerisation of partially neutralised acrylic acid monomers. The structural characteristics of various BTAA ratios and their constituents were scrutinised using XRF, XRD, and FTIR. Basal spacing of BTAA hybrid materials decreased as a result of intercalation with polyacrylic acid. Interaction between bentonite and polyacrylic acid was also observed in the shifting and reduced intensity of O–H, C=O, and Si–O–Al absorption bands. Catalytic activity of BTAA was investigated through its ability to facilitate the esterification reaction of glycerol with acetic acid. The result suggests that catalytic activity is present in BTAA hybrid materials, as evidenced by the production of monoacetin and triacetin.
Variasi Penambahan CTABr Sebagai Template Terhadap Pembentukan TiO2 Anatase Dari Senyawa Natrium Titanat dan Aplikasinya Sebagai Fotokatalis Dewi, Widya Puspita; Haryati, Tanti; Suwardiyanto, Suwardiyanto; Sulistiyo, Yudi Aris; Andarini, Novita
BERKALA SAINSTEK Vol 7 No 2 (2019)
Publisher : Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/bst.v7i2.12857

Abstract

TiO2 anatase mesopori (ukuran pori 2-50 nm) memiliki aktivitas fotokatalitik yang besar. Metode sintesis kimia padat dapat digunakan sebagai alternatif untuk memperoleh TiO2 anatase dari natrium titanat dengan menggunakan prekursor yang murah berupaTiO2 rutile komersial. Surfaktan CTABr (Cetyltrimethylammonium Bromide) mampu menghasilkan TiO2 anatase mesopori dengan kemampuannya sebagai template atau agen pembentuk pori. Penelitian ini bertujuan mengetahui pengaruh variasi penambahan CTABr terhadap distribusi ukuran pori, volume total pori, luas permukaan TiO2 dan dan aktivitas fotokatalitik TiO2 hasil sintetis. Sintesis dilakukan menggunakan metode reaksi kimia padat dengan penambahan variasi perbandingan mol CTABr dan tanpa penambahan CTABr sebagai pembanding. Karakterisasi menggunakan XRD (X- Ray Powder Difraction), SEM (Scanning Electron Microscopy) dan Gas Sorption Analyer (GSA) untuk mengetahui struktur, morfologi dan sifat pori TiO2. TiO2 anatase mesopori hasil sintesis diaplikasikan sebagai fotokatalis dalam mendegradasi metilen biru. Hasil penelitian ini menunjukkan bahwa TiO2 anatase mesopori berhasil didapatkan dengan morfologi partikelnya berbentuk seperti balok, sisi tidak seragam serta ukuran partikel berkisar 200-500 nm. Variasi penambahan CTABr tidak memberikan pengaruh yang signifikan terhadap distribusi ukuran pori, volume total pori, luas permukaan dan aktivitas fotokatalitik dari TiO2 anatase mesopori, dengan hasil distribusi pori mayoritas pada 2 nm dan aktivitas fotokatalitik sekitar 77%
Sintesis Silika Gel Berbasis Fly Ash Batu Bara PLTU Paiton Sebagai Adsorben Zat Warna Rhodamin B Aisah, Siti; Zulfikar, Z.; Sulistiyo, Yudi Aris
BERKALA SAINSTEK Vol 6 No 1 (2018)
Publisher : Universitas Jember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.19184/bst.v6i1.7761

Abstract

Abu terbang batu bara dengan prosentase kandungan SiO 2 telah berhasil digunakan sebagai bahan baku pembuatan Silika Gel. Karakteristik silika gel diketahui dengan munculnya gugus fungsi silanol dan siloksan dengan FTIR, struktur kristal tak beraturan (amorf) dengan XRD, bentuk partikel bola (spherical) dan analisis unsur dengan EDX. Silika gel yang dihasilkan masih mengandung sedikit pengotor oksida alumina dan oksida natrium. Pengujian kapasitas adsorpsi Rhodamin-B silika gel lebih besar dibandingkan abu terbang dengan model adsorsi keduanya mengikuti model isotermal Langmuir dengan konsentrasi optimum pada 200 ppm. Kinetika adsorpsi mengikuti model Pseudo Second Order dimana laju adsorpsi silika gel sedikit lebih tinggi dibanding abu terban, tepai perbedaaanya tidak signifikan.Kata Kunci: zat warna Rhodamin B, silika gel, abu terbang batubara, Isotermal adsorpsi, kinetika adsorpsi
Co-Authors Artoto Arkundato Asnawati Asnawati Assiddiq, Mustafid A’yun Bambang Piluharto Denny Trias Utomo, Denny Trias Dewi, Widya Puspita Diana, Alvina Nur Dwi Indarti Endhah Purwandari Furqonul Hakin Al Hadi Habibah, Putri Sifa Kamila, Wilda Lestari, Wiwit Puji Lutfiatun Nadifah Maziyyah, Deys Sya’fatul Nadjib, Muhammad Nelumbium, Tusiana Putri Nida Andriana Novita Andarini Novita Andarini Purwo Handoko, Donatus Setyawan Ratna Ediati Sholehah, Hidayati Nur Mohammad Siti Aisah Sofiyah, Ovy Sukmawati, Nissa Sunnardianto, Gagus Ketut Sutisna Sutisna Suwardiyanto Suwardiyanto Suwardiyanto Suwardiyanto, S. Syarifah, Ratna Dewi Tanti Haryati Wenny Maulina, Wenny Wuryanti Handayani Yeni Maulidah Muflihah Zakaria, Helmy Ahmad Zulfikar Zulfikar Zulfikar, Z.