Garuda - Garba Rujukan Digital

INFLUENCE OF CARBON AND NITROGEN ADDITION ON THE CORROSION RESISTANCE OF Co-28Cr-6Mo-0,8Si-0,8Mn-0,4Fe-0,2Ni ALLOYS Fendy Rokhmanto; Cahya Sutowo; Ika Kartika
Widyariset Vol 4, No 1 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Cobalt alloys is one of the implant materials that is used in orthopedic and dentistry, because of its biocompatibility, good mechanical properties, and high corrosion resistance. The mechanical properties and corrosion resistance can be enhanced by thermomechanical treatment and addition of alloying element. Carbon and nitrogen were added to enhance mechanical properties and high corrosion resistance. Effect of carbon variation and nitrogen to the corrosion resistance in Co-Cr-Mo (CCM) alloys were measured by corrosion measurement system (CMS) device in Hank’s Solutions after thermomechanical treatment process. Corrosion rate of Co-Cr-Mo alloys with carbon variation dropped to 5.8 x 10-4 mmpy and 5.2 x 10-4 mmpy with carbon variation and nitrogen. Decreasing corrosion rate indicated that the corrosion resistance of alloys is increased with the addition of carbon and nitrogen.

CORROTION RATE AND MORPHOLOGY OF POROUS METAL ALLOY Mg-Ca-Zn WITH CaCO3 AS FOAMING AGENT Aprilia Erryani; Franciska Pramuji Lestari; Dhyah Annur; Muhammad Ikhlasul Amal; Ika Kartika
Widyariset Vol 4, No 1 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Magnesium alloy is a material that has been developed as a biodegradable implant material in orthopedic applications. Magnesium alloys have good biocompatibility, biodegradability, and good mechanical properties which make them have the potential to be used as a biomedical material. The main objective of this paper is to investigate corrotion rate and morphology after corrotion of biocompatibility of implant-based alloys Mg-Ca-Zn with CaCO3 as a foaming agent. Mg-Ca-Zn Alloy was made by the method of powder metallurgy with the addition of CaCO3 as a foaming agent with three variations of composition (96Mg-Ca-3Zn-CaCO3, 91Mg-Ca-3Zn-5 CaCO3, and 86Mg-Ca-3Zn-10 CaCO3 wt%). Sintering process was carried out at 600 °C and 650 °C with a holding time of five hours. Corrosion test was performed using G750 Gamry Instrument in accordance with ASTM standard G5-94. Simulated body fluid electrolyte used is Hank's solution with a pH value of 7.4 and a temperature of 37 °C. Then the analysis of the microstructure after corrosion test was conducted using scanning electron microscopy (JEOL, JSM-6390A Japan) equipped with energy dispersive spectrometry data (EDS). Alloy corrosion rate of Mg-Ca-Zn-CaCO3 increases with the amount of CaCO3 in the alloy and the temperature rise in the sintering. From the test results, the smallest corrosion rate is in the alloy 91Mg-Ca-3Zn-CaCO3 at 600 °C sintering (58.3045 mpy) and the highest occurs in alloy 86Mg-Ca-3Zn-10CaCO3 at 650 °C sintering (91.4007 mpy). Surface morphology of the alloy after the corrosion process is the type of volcano. This localized corrosion occurs where an electrochemical reaction takes place to form a distinctive structure with a circle and a hole in the middle.

CORROTION RATE AND MORPHOLOGY OF POROUS METAL ALLOY Mg-Ca-Zn WITH CaCO3 AS FOAMING AGENT Aprilia Erryani; Franciska Pramuji Lestari; Dhyah Annur; Muhammad Ikhlasul Amal; Ika Kartika
Widyariset Vol 4, No 1 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Magnesium alloy is a material that has been developed as a biodegradable implant material in orthopedic applications. Magnesium alloys have good biocompatibility, biodegradability, and good mechanical properties which make them have the potential to be used as a biomedical material. The main objective of this paper is to investigate corrotion rate and morphology after corrotion of biocompatibility of implant-based alloys Mg-Ca-Zn with CaCO3 as a foaming agent. Mg-Ca-Zn Alloy was made by the method of powder metallurgy with the addition of CaCO3 as a foaming agent with three variations of composition (96Mg-Ca-3Zn-CaCO3, 91Mg-Ca-3Zn-5 CaCO3, and 86Mg-Ca-3Zn-10 CaCO3 wt%). Sintering process was carried out at 600 °C and 650 °C with a holding time of five hours. Corrosion test was performed using G750 Gamry Instrument in accordance with ASTM standard G5-94. Simulated body fluid electrolyte used is Hank's solution with a pH value of 7.4 and a temperature of 37 °C. Then the analysis of the microstructure after corrosion test was conducted using scanning electron microscopy (JEOL, JSM-6390A Japan) equipped with energy dispersive spectrometry data (EDS). Alloy corrosion rate of Mg-Ca-Zn-CaCO3 increases with the amount of CaCO3 in the alloy and the temperature rise in the sintering. From the test results, the smallest corrosion rate is in the alloy 91Mg-Ca-3Zn-CaCO3 at 600 °C sintering (58.3045 mpy) and the highest occurs in alloy 86Mg-Ca-3Zn-10CaCO3 at 650 °C sintering (91.4007 mpy). Surface morphology of the alloy after the corrosion process is the type of volcano. This localized corrosion occurs where an electrochemical reaction takes place to form a distinctive structure with a circle and a hole in the middle.

INFLUENCE OF CARBON AND NITROGEN ADDITION ON THE CORROSION RESISTANCE OF Co-28Cr-6Mo-0,8Si-0,8Mn-0,4Fe-0,2Ni ALLOYS Fendy Rokhmanto; Cahya Sutowo; Ika Kartika
Widyariset Vol 4, No 1 (2018): Widyariset
Publisher : Pusbindiklat - LIPI

Cobalt alloys is one of the implant materials that is used in orthopedic and dentistry, because of its biocompatibility, good mechanical properties, and high corrosion resistance. The mechanical properties and corrosion resistance can be enhanced by thermomechanical treatment and addition of alloying element. Carbon and nitrogen were added to enhance mechanical properties and high corrosion resistance. Effect of carbon variation and nitrogen to the corrosion resistance in Co-Cr-Mo (CCM) alloys were measured by corrosion measurement system (CMS) device in Hank’s Solutions after thermomechanical treatment process. Corrosion rate of Co-Cr-Mo alloys with carbon variation dropped to 5.8 x 10-4 mmpy and 5.2 x 10-4 mmpy with carbon variation and nitrogen. Decreasing corrosion rate indicated that the corrosion resistance of alloys is increased with the addition of carbon and nitrogen.

Analisis Variasi Temperatur Sintering dan Ukuran Agen Pengembang Dolomit terhadap Fabrikasi Paduan Logam Mg-Ca-Zn Berpori Tertutup dengan Proses Metalurgi Serbuk Franciska P. Lestari; Brama A. Saputra; Aprilia Erryani; Inti Mulyati; Made Subekti Dwijaya; Ika Kartika
TEKNIK Vol 42, No 2 (2021)
Publisher : Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/teknik.v42i2.36978

Paduan logam berpori berbasis magnesium sangat potensial dalam aplikasi prostesis biomedis. Kalsium, seng dan agen pengembang ditambahkan untuk melengkapi fungsi dan aplikasi paduan. Dalam studi ini, paduan logam berpori Mg-Ca-Zn dikembangkan dengan proses metalurgi serbuk menggunakan dolomit (CaMg(CO3)2) sebagai agen pengembang untuk menghasilkan pori jenis tertutup. Variasi ukuran agen pengembang dan temperatur sintering dilakukan dengan tujuan untuk mencapai ukuran, persentasi dan kehomogenan pori yang terbentuk dalam paduan, dimana pori berfungsi untuk pertumbuhan tulang baru. Komposisi (%berat) paduan yang dikembangkan adalah 84,5Mg-0,5Ca-5Zn-10CaMg(CO3)2, dengan variasi temperatur sintering T = 650, 675, dan 700°C dan waktu tahan 5 jam, sedangkan ukuran dolomit CaMg(CO3)2 divariasikan -30 #, -50 #, -80 #. Paduan hasil sintering diuji XRD (x-ray diffraction) untuk menganalisis fasa yang terbentuk. Ukuran dan kehomogenan pori hasil sintering diamati dengan SEM (scanning electron microscopy), dan persentasi pori yang terbentuk diukur dengan menggunakan metode Archimedes sesuai standar ASTM B311-93. Sifat mekanik dari paduan hasil sintering diuji dengan alat uji kompresi mengacu pada standar ASTM D-695-02. Analisis XRD (x-ray diffraction) dalam paduan 84,5Mg-0,5Ca-5Zn-10CaMg(CO3)2hasil sintering terbentuk fasa Mg sebagai matriks, MgO, CaCO3 dan dolomit (CaMg(CO3)2). Persentasi porositas tertinggi diperoleh sebesar 32,60% dengan ukuran pori terbesar adalah ≤300 μm dan kekuatan tekan 143 MPa. Kondisi ini dihasilkan dalam paduan dengan ukuran partikel dolomit -30# dan temperatur sintering 700°C. Teknologi metalurgi serbuk dengan variasi temperatur sintering dan variasi ukuran agen pengembang dolomit berpengaruh signifikan terhadap ukuran, persentasi, dan kehomogenan pori serta sifat mekanik yang dihasilkan dalam paduan 84,5Mg-0,5Ca-5Zn.

Title

Found 5 Documents
Search

Abstract

Abstract

Abstract

Abstract

Abstract

Title Search

Found 5 Documents Search

Abstract

Abstract

Abstract

Abstract

Abstract

Title

Found 5 Documents
Search