Widyariset
Vol 4, No 1 (2018): Widyariset

CORROTION RATE AND MORPHOLOGY OF POROUS METAL ALLOY Mg-Ca-Zn WITH CaCO3 AS FOAMING AGENT

Aprilia Erryani (Pusat Penelitian Metalurgi dan Material, Lembaga Ilmu Pengetahuan Indonesia)
Franciska Pramuji Lestari (Pusat Penelitian Metalurgi dan Material, Lembaga Ilmu Pengetahuan Indonesia)
Dhyah Annur (Pusat Penelitian Metalurgi dan Material, Lembaga Ilmu Pengetahuan Indonesia)
Muhammad Ikhlasul Amal (Pusat Penelitian Metalurgi dan Material, Lembaga Ilmu Pengetahuan Indonesia)
Ika Kartika (Pusat Penelitian Metalurgi dan Material, Lembaga Ilmu Pengetahuan Indonesia)



Article Info

Publish Date
31 May 2018

Abstract

Magnesium alloy is a material that has been developed as a biodegradable implant material in orthopedic applications. Magnesium alloys have good biocompatibility, biodegradability, and good mechanical properties which make them have the potential to be used as a biomedical material. The main objective of this paper is to investigate corrotion rate and morphology after corrotion of biocompatibility of implant-based alloys Mg-Ca-Zn with CaCO3 as a foaming agent. Mg-Ca-Zn Alloy was made by the method of powder metallurgy with the addition of CaCO3 as a foaming agent with three variations of composition (96Mg-Ca-3Zn-CaCO3, 91Mg-Ca-3Zn-5 CaCO3, and 86Mg-Ca-3Zn-10 CaCO3 wt%). Sintering process was carried out at 600 °C and 650 °C with a holding time of five hours. Corrosion test was performed using G750 Gamry Instrument in accordance with ASTM standard G5-94. Simulated body fluid electrolyte used is Hank's solution with a pH value of 7.4 and a temperature of 37 °C. Then the analysis of the microstructure after corrosion test was conducted using scanning electron microscopy (JEOL, JSM-6390A Japan) equipped with energy dispersive spectrometry data (EDS). Alloy corrosion rate of Mg-Ca-Zn-CaCO3 increases with the amount of CaCO3 in the alloy and the temperature rise in the sintering. From the test results, the smallest corrosion rate is in the alloy 91Mg-Ca-3Zn-CaCO3 at 600 °C sintering (58.3045 mpy) and the highest occurs in alloy 86Mg-Ca-3Zn-10CaCO3 at 650 °C sintering (91.4007 mpy). Surface morphology of the alloy after the corrosion process is the type of volcano. This localized corrosion occurs where an electrochemical reaction takes place to form a distinctive structure with a circle and a hole in the middle.

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Journal Info

Abbrev

widyariset

Publisher

Subject

Engineering

Description

Widyariset is a scientific journal which publishes the results of research and development, assessment and systematic thinking about science and technology. The writers of the scientific papers in this journal come from researchers/researcher candidates from various institutions' research and ...