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Nelly Fadliyani
Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Negeri Yogyakarta
Decision Sciences, Operations Research & Management

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THE UTILIZATION OF GLYCEROL, BIODIESEL SIDE PRODUCT OF USED COOKING OIL AS GLYCEROL ACETATE MATERIAL SYNTHESIS Nelly Fadliyani; Sri Atun
Jurnal Penelitian Saintek Vol 20, No 2: Oktober 2015
Publisher : Institute of Research and Community Services, Universitas Negeri Yogyakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1755.712 KB) | DOI: 10.21831/jps.v20i2.9601

Abstract

The research aimed at using glycerol of biodiesel synthesis side product from used cooking oil as glycerol acetate material synthesis, and charactering synthesized material based on data of IR spectroscopy and GCMS. The method used to synthesize glycerol acetate was refl ux during 50 minute at 80 C. Glycerol from biodiesel synthesis side product from used cooking oil was purifi  ed with acetic anhydride reacted at 80 0C, for 50 minutes. The synthesis product was characterized by IR and GCMS spectroscopies. The result of this research shows that glycerol derived from synthesizing glycerol 1–monoacetate and glycerol 2-monoacetate in the form of yellow liquid with 145 148 0 0 C boiling point, soluble in ethanol and insoluble in n-hexane. IR spectrum shows the presence of C=O carbonyl, C-O ester, -OH, and C-H aliphatic group; GCMS spectrum shows a mixture from two glycerol monoacetate with SI (Similiar Index) of 97 and 93.
Co-Authors SRI ATUN