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Green Synthesis of Reduced Graphene Oxide Using Lime Juice Reductor From Citrus aurantifolia Said Ali Akbar; Fitriya Nanda; Nispi Mawaddah; Mima Yuriati
Elkawnie: Journal of Islamic Science and Technology Vol 5, No 2 (2019)
Publisher : Universitas Islam Negeri Ar-Raniry Banda Aceh

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22373/ekw.v5i2.4948

Abstract

In this study, the reduced graphene oxide (rGO) synthesized by using lime juice as an environmentally friendly reducing agent and inexpensive cost. The synthesis was carried out by oxidizing graphite with the Hummer method to form graphene oxide (GO) was formed, then the GO was reduced by using lime as the natural reducing agent. X-ray analysis shown a vital diffraction pattern for graphite at 2θ = 26.4°, for graphene oxide appears around 2θ = 10° and 43o, and rGO at 2θ = 23.8°. Furthermore, the infrared spectrum of the three samples showed the peak of the hydroxyl group at 3412 cm-1, which appeared on graphene oxide, but was not observed in rGO. The vibrational mode of carbonyl (C=O) at 1723 cm-1 was also observed with high intensity on graphene oxide. This information showed that GO has a large number of oxygen-containing groups. Then, in the dissolution test shown that the GO was more soluble in polar solvents such as water than ethanol.
Pemanfaatan Ekstrak Bunga Dadap Merah (Erythrina Crista-Galli L) sebagai Inhibitor Korosi pada Logam Fe Said Ali Akbar; Muttakin; Sri Ismulyati; Ainun Mardhiah; Nispi Mawaddah
KATALIS: Jurnal Penelitian Kimia dan Pendidikan Kimia Vol 5 No 2 (2022): Katalis: Jurnal Penelitian Kimia dan Pendidikan Kimia
Publisher : Universitas Samudra

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33059/katalis.v5i2.6720

Abstract

Korosi logam terjadi melalui reaksi elektrokimia simultan membentuk rangkaian arus listrik tertutup pada wilayah anoda dan katoda, penambahan inhibitor dapat digunakan sebagai salah satu cara untuk menghambat korosi. Ekstrak bunga dadap merah dapat berfungsi dengan baik sebagai inhibitor alami untuk mencegah korosi pada besi, baik pada media air akuades maupun air laut. Pengaruh perbedaan konsentrasi ekstrak bunga dadap merah yang diberikan memberikan efek penurunan bertambahnya massa logam Fe. Pada ekstrak konsentrasi 20%, mula-mula berat paku 2,484 gram menjadi 2,488 gram pada media air akuades dan 2,436 gram menjadi 2,442 gram pada media air laut. Hal ini menunjukkan bahwa besar konsentrasi, maka proses terjadinya korosi sangat sulit terjadi.