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Green-Synthesis Nanopartikel SnO2 Termediasi Ekstrak Daun Pelawan (Tristaniopsis merguensis Griff.) Mustari Mustari; Evi J; Aliefia Noor; Rifqi Almusawi Rafsanjani; Yuant Tiandho
EduMatSains : Jurnal Pendidikan, Matematika dan Sains Vol 4 No 1 (2019): Juli
Publisher : Fakultas Keguruan dan Ilmu Pendidikan, Universitas Kristen Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33541/edumatsains.v4i1.1043

Abstract

SnO2 nanoparticles are materials that have great potential in gas sensor devices. In this article, the synthesis of SnO2 nanoparticles is carried out through the mediation of pelawan (Tristaniopsis merguensis Griff.) leaf extract. The use of mediators of natural materials in this synthesis aims to make the synthesis process more environmentally friendly and lower in cost compared to conventional chemical and physical methods. Pelawan extract contains high antioxidant compounds. Thus, it can inhibit the agglomeration of SnO2 particles. Based on the variation of pH synthesis, it is known that the highest purity of SnO2 phase occurs at pH 7 while for alkaline conditions, there is an impurity, i.e., Sn6O4(OH)4. Calcination temperature has a very significant effect on the growth of SnO2 nanoparticle crystals. High temperatures will increase the size of the crystallite and the crystallinity. Keywords: green-synthesis, pelawan, tin oxide
Synthesis of α-Fe2O3 and α-Fe2O3/SiO2 Composite from Geothermal Waste by Sol-Gel Method and Their Characterization Mulmeyda, Rinda; Reinardo Ramawijaya Widakusuma; Sabrina Putri Chaerani; Agus Purwanto; Rifqi Almusawi Rafsanjani; Habib Muhammad Zapar; Bagaskoro Pranata Ardhi
Chemistry and Materials Vol. 4 No. 1 (2025)
Publisher : Pusat Inovasi Sains

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.56425/cma.v4i1.91

Abstract

Iron oxide materials, especially hematite (α-Fe2O3), have many important applications. Improving the characteristics and physical properties of hematite has been widely developed, one of which is to combine it as a composite structure with porous materials such as silica (SiO2) as α-Fe2O3/SiO2 composite. This research aims to synthesize α-Fe2O3 particles and α-Fe2O3/SiO2 composites. The α-Fe2O3/SiO2 composite was successfully synthesized by using geothermal waste as an alternative source of silica prepared by the sol-gel method. Both synthesized samples were characterized by X-ray diffraction, scanning electron microscopy equipped with energy dispersive spectroscopy, and X-ray fluorescence techniques. The results showed that silica composites on hematite structure slightly affect the morphology, color, or particle size compared to α-Fe2O3.