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All Journal Jurnal Matematika & Sains Journal of Aceh Physics Society INDONESIAN JOURNAL OF APPLIED PHYSICS Jurnal Teori dan Aplikasi Fisika Jurnal Natural Aceh International Journal of Science and Technology Jurnal Pendidikan Sains Indonesia (Indonesian Journal of Science Education)
Adi Rahwanto
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Agriculture, Biological Sciences & Forestry Astronomy Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Control & Systems Engineering Decision Sciences, Operations Research & Management Earth & Planetary Sciences Education Energy Immunology & microbiology Materials Science & Nanotechnology Mathematics Neuroscience Physics

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Journal : Jurnal Natural

 1 
SYNTHESIS AND CHARACTERIZATION OF HEMATITE (Fe2O3) EXTRACTED FROM IRON ORE BY PRECIPITATION METHOD Andia Andia; Adi Rahwanto; Zulkarnanin Jalil
Jurnal Natural Volume 16, Number 1, March 2016
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (80.678 KB) | DOI: 10.24815/jn.v16i1.4361

Abstract

Indonesia has a lot of mining material of iron ore that could be used for various purposes in the steel industry or for other. This research, has synthesized and characterization of hematite from local iron ore from Lhoong area by precipitation mechanism. The iron ore powder was magnetic separation with magnet then mixed with HCl and NH4OH. Then, it was dried at temperature of 150 ºC and calcinated at 500º C for 2 hours. Characterizations were perfomed using X-ray Diffraction (XRD) and X-ray Fluorescence (XRF). As the results, it was found that the magnetic separation iron ore showed the composition of Fe2O3 (95.99%), SiO2 (2.10%). Then, by precipitation mechanism, the composition of Fe2O3 found around 96.58%. Next, the synthesis result are characterized with XRD show that the main phase is dominan in iron ore of Lhoong is hematit (Fe2O3). Scherrer calculations showed that precipitation mechanism to reducing grain size, the process of magnetic separation (58.009 µm) and the precipitation mechanism (20.950 µm.)
THE EFFECT OF MAGNETITE (Fe3O4)CATALYST FROM IRON SANDS ON DESORPTION TEMPERATURE OF MgH2 HYDROGEN STORAGE MATERIAL Maulinda Maulinda; zulkarnain Jalil; Adi Rahwanto
Jurnal Natural Volume 16, Number 1, March 2016
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (153.14 KB) | DOI: 10.24815/jn.v16i1.4362

Abstract

One of the future technologies for a safe hydrogen storage media is  metal hydrides. Currently, Mg-based metal hydride has a safety factor and efficient for vehicle applications. However, the thermodynamic properties of magnesium hydride (MgH2) found a relatively high temperature. High desorption temperatures caused MgH2 high thermodynamic stability resulting desorption enthalpy is also high. In this study, natural mineral (iron ore) has been extracted from iron sand into powder of magnetite (Fe3O4) and used as a catalyst in an effort to improve the desorption properties of MgH2. Magnetie has been successfully extracted from iron sand using precipitation method with a purity of 85 % , where the purity of the iron sand before extracted was 81%. Then, MgH2-Fe3O4 was milling using mechanical alloying method with a variety of catalysts and milling time. The observation by XRD showed the material was reduced to nanocrystalline scale. MgH2 phase appears as the main phase. DSC test results showed with the addition of Fe3O4, the desorption temperature can be reduced up to 366oC, compared to pure pure MgH2 reached by 409o C. Furthermore, based on gravimetric test, the hydrogen release occurs at a temperature of 388o C, weight loss  of 0.66 mg during 16 minutes.
SYNTHESIS AND CHARACTERIZATION OF HEMATITE (Fe2O3) EXTRACTED FROM IRON ORE BY PRECIPITATION METHOD Andia Andia; Adi Rahwanto; Zulkarnanin Jalil
Jurnal Natural Volume 16, Number 1, March 2016
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jn.v16i1.4361

Abstract

Indonesia has a lot of mining material of iron ore that could be used for various purposes in the steel industry or for other. This research, has synthesized and characterization of hematite from local iron ore from Lhoong area by precipitation mechanism. The iron ore powder was magnetic separation with magnet then mixed with HCl and NH4OH. Then, it was dried at temperature of 150 ºC and calcinated at 500º C for 2 hours. Characterizations were perfomed using X-ray Diffraction (XRD) and X-ray Fluorescence (XRF). As the results, it was found that the magnetic separation iron ore showed the composition of Fe2O3 (95.99%), SiO2 (2.10%). Then, by precipitation mechanism, the composition of Fe2O3 found around 96.58%. Next, the synthesis result are characterized with XRD show that the main phase is dominan in iron ore of Lhoong is hematit (Fe2O3). Scherrer calculations showed that precipitation mechanism to reducing grain size, the process of magnetic separation (58.009 µm) and the precipitation mechanism (20.950 µm.)
THE EFFECT OF MAGNETITE (Fe3O4)CATALYST FROM IRON SANDS ON DESORPTION TEMPERATURE OF MgH2 HYDROGEN STORAGE MATERIAL Maulinda Maulinda; zulkarnain Jalil; Adi Rahwanto
Jurnal Natural Volume 16, Number 1, March 2016
Publisher : Universitas Syiah Kuala

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24815/jn.v16i1.4362

Abstract

One of the future technologies for a safe hydrogen storage media is  metal hydrides. Currently, Mg-based metal hydride has a safety factor and efficient for vehicle applications. However, the thermodynamic properties of magnesium hydride (MgH2) found a relatively high temperature. High desorption temperatures caused MgH2 high thermodynamic stability resulting desorption enthalpy is also high. In this study, natural mineral (iron ore) has been extracted from iron sand into powder of magnetite (Fe3O4) and used as a catalyst in an effort to improve the desorption properties of MgH2. Magnetie has been successfully extracted from iron sand using precipitation method with a purity of 85 % , where the purity of the iron sand before extracted was 81%. Then, MgH2-Fe3O4 was milling using mechanical alloying method with a variety of catalysts and milling time. The observation by XRD showed the material was reduced to nanocrystalline scale. MgH2 phase appears as the main phase. DSC test results showed with the addition of Fe3O4, the desorption temperature can be reduced up to 366oC, compared to pure pure MgH2 reached by 409o C. Furthermore, based on gravimetric test, the hydrogen release occurs at a temperature of 388o C, weight loss  of 0.66 mg during 16 minutes.
Co-Authors Anak Agung Istri Sri Wiadnyani Andia Andia Habib Satria Indri Dayana Maidar Maidar Martha Rianna Maulinda Maulinda Nasrullah Idris Nirmala Sari Nurwijayanti Pajriana, Elisa Syarifah Rita Zahara Yusrizal Yusrizal Zulkarnain Jalil Zulkarnain Jalil Zulkarnain Jalil Zulkarnanin Jalil