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All Journal Jurnal Sains dan Seni ITS Turbo : Jurnal Program Studi Teknik Mesin
Guruh Sartika
Sekolah Tinggi Teknologi Industri Bontang
Arts Humanities Mechanical Engineering

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Sintesis dan Karakterisasi Katalis Mg1-xNixF2±δ Guruh Sartika; Irmina Kris Murwani
Jurnal Sains dan Seni ITS Vol 3, No 2 (2014)
Publisher : Lembaga Penelitian dan Pengabdian Kepada Masyarakat (LPPM), ITS

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2966.16 KB) | DOI: 10.12962/j23373520.v3i2.7026

Abstract

Pada penelitian ini telah dilakukan sintesis katalis Mg1-xNixF2(x= 0,025; 0,05; 0,1 dan 0,15) dengan metode sol-gel. Semua katalis dikarakterisasi struktur kristal dengan difraksi sinar X. Hasil difraktogram Mg1-xNixF2menunjukkan bahwa struktur kristal katalis Mg1-xNixF2masih masuk dalam struktur utama MgF2 yang dicocokkan dengan database JCPDS-International Centre of Diffraction Data PCPDFWIN tahun 2001, PDF No.70-2269.Hasil difraktogram katalis Mg1-xNixF2 menunjukkan adanya perbedaan intensitas puncak sehingga doping logam Ni terhadap MgF2 berpengaruh. Adanya puncak katalis Mg1-xNixF2yang bergeser diakibatkan penambahan jumlah mol doping yang berbeda-beda
Sintesis dan Karakterisasi Bunga Sepatu dan Karbon Kayu Ulin Untuk Katalis Pada Proses Pirolisis Sampah Plastik Guruh Sartika; Yano Hurung Anoi; Rosmiati; Asriwulan; Tatang Wiyadi; Amir Maulana; Ahmad Yani
TURBO [Tulisan Riset Berbasis Online] Vol 15 No 2 (2026): TURBO: Jurnal Program Studi Teknik Mesin (in Progress)
Publisher : Universitas Muhammadiyah Metro

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24127/trb.v15i2.5363

Abstract

Plastic waste pyrolysis requires catalysts that are thermally stable, accessible, and economically viable. This study synthesizes and characterizes a biomass-based catalytic material derived from hibiscus flower powder and activated Ulin wood carbon. Hibiscus petals were dried under sunlight for 6 h, oven-dried at 55 °C for 1 h, ground, and sieved to 200 mesh. Ulin wood carbon was reduced by high-energy milling, sieved to 200 mesh, activated in 3 M NaOH using 8 g carbon for 12 h, washed to pH 6–7, and dried at 105 °C for 8 h. UV–Vis analysis showed that hibiscus powder contained 676.62 mg EQ/100 g flavonoids, 2305.06 mg GAE/100 g phenols, 369.69 ppm antioxidant activity, and 122.40 ppm anthocyanins. Activated Ulin carbon contained 166.28 mg EQ/100 g flavonoids, 32.04 mg GAE/100 g phenols, 0 ppm antioxidant activity, and 0.54 ppm anthocyanins. Thermal, morphological, functional group, and crystallinity analyses were conducted using TGA-DTA, SEM, FTIR, and XRD. The results indicate that hibiscus contributes oxygenated bioactive compounds, whereas activated Ulin carbon provides a carbonaceous support structure. The combined characteristics suggest potential use as a sustainable catalyst precursor for plastic waste pyrolysis. Keywords: Hibiscus flower; ulin wood carbon; activated carbon; biomass catalyst; plastic waste pyrolysis
Co-Authors Ahmad Yani Amir Maulana Asriwulan Kris Murwani, Irmina Rosmiati Tatang Wiyadi Yano Hurung Anoi