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All Journal The Journal of Pure and Applied Chemistry Research CARADDE: Jurnal Pengabdian Kepada Masyarakat EDUKATIF : JURNAL ILMU PENDIDIKAN Acta Chimica Asiana
Tutik Setianingsih
Department of Chemistry, Faculty of Mathematics and Natural Sciences, Brawijaya University, Jl. Veteran Malang 65145
Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Mathematics Medicine & Pharmacology Social Sciences

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Journal : The Journal of Pure and Applied Chemistry Research

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Study of Structural Properties of Mesoporous Carbon From Fructose with Zinc Borosilicate Activator Setianingsih, Tutik; Kartini, Indriana; Arryanto, Yateman
The Journal of Pure and Applied Chemistry Research Vol. 3 No. 3 (2014)
Publisher : Chemistry Department, The University of Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (446.981 KB) | DOI: 10.21776/ub.jpacr.%y.03.03.173

Abstract

Structural properties, including pore structure, functional group of carbon surface, and crystal structure of carbon built by zinc borosilicate (ZBS) and ZnCl2 (Z) have been investigated in this work. Physically, ZBS and ZnCl2 may act as template of carbon, whereas the Zn(II) cation act as chemical activator of carbonization. All precursors of ZBS (silicagel, boric acid, and ZnCl2) may act as catalysts of caramelization. The caramelization was conducted hydrothermally at 85oC and thermally 130oC. The carbonization was conducted at 450oC. The resulted carbons were washed by using HF 48% solution, 1M HCl solution, and aquadest respectively. The solid products were characterized by using nitrogen gas adsorption, infrared spectrophotometry, X-ray diffraction, and Transmition Electron Microscopy. Result of research showed that ZBS built larger mesopore volume, larger pore domination of pore size, more hydrophobic carbon, and more amorf than ZnCl2.
Co-Authors Adi Kurnia Soesantyo Afif Eka Rahma Setiyanto Danar Purwonugroho Danar Purwonugroho Dzakwan, M. Naufal Tsaqif Ewies, Ewies Fawzy Indriana Kartini Kashifa Maria Jihan Silvi Zakiyatul Ilmiyah Syarifah, Nidatul Yateman Arryanto Yuniar Ponco Prananto