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All Journal Journal on Education Sang Pencerah: Jurnal Ilmiah Universitas Muhammadiyah Buton IJCR (Indonesian Journal of Chemical Research)
Amirul Mukminin
STT Migas Balikpapan
Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Social Sciences Other

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Analisis Kandungan Biodiesel Hasil Reaksi Transesterifikasi Minyak Jelantah Berdasarkan Perbedaan Kosentrasi Katalis NaOH Menggunakan GC-MS Amirul Mukminin; Eka Megawati; I Ketut Warsa; Yuniarti Yuniarti; Wildan Azizul Umaro; Dian Islamiati
Sang Pencerah: Jurnal Ilmiah Universitas Muhammadiyah Buton Vol 8 No 1 (2022): Sang Pencerah: Jurnal Ilmiah Universitas Muhammadiyah Buton
Publisher : Lembaga Penelitian dan Pengabdian Masyarakat Universitas Muhammadiyah Buton

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1768.979 KB) | DOI: 10.35326/pencerah.v8i1.1897

Abstract

Pada penelitian ini telah diteliti pengaruh % konsentrasi massa katalis NaOH terhadap produksi metil ester (biodiesel) melalui transterifikasi minyak goreng bekas (minyak jelantah) dan metanol. Hasil tertinggi ditemukan pada katalis NaOH 0,6% dengan rendemen 85%. Sedangkan untuk penggunaan katalis NaOH 0,4; 0,5; dan 0,7% massa katalis adalah masing-masing 65,5%, 67,8% dan 72%. Instrumen Gas Chromatography (GC) dan Mass Spectrocopy (MS) telah mampu mendeskripsikan secara kualitatif dan kuantitatif kandungan biodiesel sintetik. Analisis GC-MS telah mengidentifikasi 3 puncak yang memiliki nilai area lebih tinggi dari 14 puncak yang terdeteksi sebagai metil ester asam lemak. Hasil kromatogram deteksi GC-MS menunjukkan bahwa 3 puncak tertinggi adalah pada puncak ke 7 yaitu metil oleat, luas area 55,47 % dan waktu retensi 17,967 menit; puncak ke 4 adalah metil palmitat dengan luas 36,66% dan waktu retensi 16,127 menit; dan puncak ke 8 adalah metil stearat dengan luas 4,41% dan waktu retensi 18,101 menit. Sementara itu, puncak 2 adalah metil mersitat dengan luas area hanya 1,15%.
Pengaruh Waktu Kalsinasi Abu Cangkang Kelomang (Paguroidea) pada Suhu Tinggi dalam Pembentukan Katalis Padat CaO Amirul Mukminin; Muhammad Firdaus; Yuniarti Yuniarti; Muh Wahyu Syabani
INDONESIAN JOURNAL OF CHEMICAL RESEARCH (IJCR) VOLUME 4, ISSUE 1, 2019
Publisher : Universitas Islam Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (583.598 KB) | DOI: 10.20885/ijcr.vol4.iss1.art1

Abstract

Katalis CaO dari abu cangkang kelomang (Paguroidea) telah berhasil dibuat melalui proses kalsinasi pada suhu 900°C selama 4 jam. Variasi waktu kalsinasi 2, 3, dan 4 jam dilakukan untuk mempelajari tentang perubahan fasa sampel. Hasil difraksi sinar-X dari abu cangkang kelomang untuk 2 dan 3 jam menunjukkan bahwa puncak-puncak karakteristik CaCO3 kalsit sedangkan untuk 4 jam berupa kalsium oksida (CaO) dengan puncak karaktersitik pada 2 theta = 32,16°; 37,15°; 53,54°; 64,16° dan 67,5° yang dikonfirmasi sesuai dengan standard CaO (JCPDS N. 82-1690). Hasil SEM menunjukkan informasi topografi dari morfologi partikel katalis untuk waktu 2 dan 3 jam berbentuk agregat yang kurang homogen, jika dibandingkan dengan hasil kalsinasi pada waktu yang lebih lama yaitu 4 jam. Sebaran ukuran parikel untuk 2, 3 dan 4 jam masing-masing memberikan ukuran 0,3 mm-1,5 µm, 34,7 µm – 1,25 µm, dan 11,4 µm – 1 µm. Hasil TGA/DSC menunjukan 43,92 % cangkang kelomang mampu terkonversi menjadi CaO dan CaCO3 pada 900°C. Kata kunci: Katalis CaO, katalis heterogen, biodisel
Pengaruh Waktu Reaksi Pembuatan Biodiesel dari Minyak Jelantah dengan Bantuan Katalis Bassa NaOH terhadap Sifat Fisika dan Kimia Produk Biodiesel Amirul Mukminin; Eka Megawati; Debora Ariyani; I Ketut Warsa; Junety Monde; Sapril Sapril
Journal on Education Vol 5 No 2 (2023): Journal on Education: Volume 5 Nomor 2 Tahun 2023
Publisher : Departement of Mathematics Education

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31004/joe.v5i2.1250

Abstract

The effect of the transesterification reaction time of 0.6% mass % NaOH catalyst in the formation of methyl ester (biodiesel) made from used waste cooking oil as raw material 6 times usage and methanol 1: 5 mass has been studied at 60°C. The reaction times used were 30, 40, and 45 minutes. All samples resulting from the transesterification reaction have been studied for their chemical and physical properties. Parameters of chemical properties included in the Indonesian National Standard (SNI) for all samples were % FFA, pH, while the water content was above the SNI standard. The physical property parameters for all samples that meet SNI are only flash point, color and 90% distillation. While the density of all test samples was lower than the SNI which was set at 850-890 Kg/m3, the results obtained for reaction times of 30, 40 and 45 minutes were 828, 833 and 836 Kg/m3 respectively. The highest yield was owned by a reaction time of 40 minutes, namely 80%. As for the reaction time of 35 and 45 minutes respectively 79 and 65%.
Pengaruh Waktu Reaksi Pembuatan Biodiesel dari Minyak Jelantah dengan Bantuan Katalis Bassa NaOH terhadap Sifat Fisika dan Kimia Produk Biodiesel Amirul Mukminin; Eka Megawati; Debora Ariyani; I Ketut Warsa; Junety Monde; Sapril Sapril
Journal on Education Vol 5 No 2 (2023): Journal on Education: Volume 5 Nomor 2 Tahun 2023
Publisher : Departement of Mathematics Education

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

The effect of the transesterification reaction time of 0.6% mass % NaOH catalyst in the formation of methyl ester (biodiesel) made from used waste cooking oil as raw material 6 times usage and methanol 1: 5 mass has been studied at 60°C. The reaction times used were 30, 40, and 45 minutes. All samples resulting from the transesterification reaction have been studied for their chemical and physical properties. Parameters of chemical properties included in the Indonesian National Standard (SNI) for all samples were % FFA, pH, while the water content was above the SNI standard. The physical property parameters for all samples that meet SNI are only flash point, color and 90% distillation. While the density of all test samples was lower than the SNI which was set at 850-890 Kg/m3, the results obtained for reaction times of 30, 40 and 45 minutes were 828, 833 and 836 Kg/m3 respectively. The highest yield was owned by a reaction time of 40 minutes, namely 80%. As for the reaction time of 35 and 45 minutes respectively 79 and 65%.
Co-Authors Debora Ariyani Dian Islamiati Eka Megawati I Ketut Warsa Junety Monde Muh. Wahyu Syabani Muhammad Firdaus Sapril Sapril Wildan Azizul Umaro Yuniarti Yuniarti Yuniarti Yuniarti