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All Journal Spektra: Jurnal Fisika dan Aplikasinya
La Isa
Department Mathematics and Natural Sciences, IAIN Kendari, Southeast Sulawesi, Indonesia
Aerospace Engineering Electrical & Electronics Engineering Energy Materials Science & Nanotechnology Physics

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SYNTHESIS AND CHARACTERIZATION OF STRUCTURAL NANOCOMPOSITE TITANIUM DIOXIDE COPPER-DOPED USING THE IMPREGNATION METHOD La Ode Asmin; La Isa
Spektra: Jurnal Fisika dan Aplikasinya Vol 5 No 1 (2020): SPEKTRA: Jurnal Fisika dan Aplikasinya, Volume 5 Issue 1, April 2020
Publisher : Program Studi Fisika Universitas Negeri Jakarta

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (286.71 KB) | DOI: 10.21009/SPEKTRA.051.03

Abstract

Nanocomposite Titanium Dioxide (TiO2) doped Copper (Cu), Cu-TiO2 is synthesized by the impregnation method. This study aims to determine the effect of adding Cu to the TiO2 structure. The 1, 3, and 5 Cu with% TiO2 dissolved in 50 ml of deionized water, and 3 grams of TiO2 added. The compound is then stirred for 2 hours at 90oC and dried in an oven at 110oC for 30 minutes. Drying samples were calcined at 500oC for 3 hours. Cu-TiO2 nanocomposites were characterized by XRD, SEM-EDX Mapping, and FTIR. The XRD analysis results show that Cu-TiO2 nanocomposite has a high level of crystallinity and has an anatase phase structure. The size of TiO2 crystals decreased with Cu doping and increased from 49.66 nm to 49.68 nm, with an increase in the composition of the doping mass of Cu. The SEM-EDX Mapping results show that all samples tend to clot, and Cu dopants evenly distributed on the surface of TiO2. FTIR analysis explained the presence of hydroxyl ions in the sample marked with the appearance of the absorption peak at 1658.78 cm-1 associated with OH bending of Ti-OH.
Co-Authors La Ode Asmin