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NURYADI SALEH
R&D Centre for Mineral and Coal Technology
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APPLICATION OF REVERSE FLOTATION METHOD FOR THE UPGRADING OF IRON OXIDE CONTAINED IN CALCINE LATERITE ORE PRAMUSANTO PRAMUSANTO; NURYADI SALEH; MUTA’ALIM MUTA’ALIM; YUHELDA DAHLAN; Muchtar Aziz
Indonesian Mining Journal Vol 11, No 1 (2008): INDONESIAN MINING JOURNAL Vol. 11 No. 1 February 2008
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (510.563 KB) | DOI: 10.30556/imj.Vol11.No1.2008.600

Abstract

Reverse flotation was adopted for Indonesian iron-rich laterite ore from Pomalaa to float siliceous minerals in the separation of iron mineral. Nickel siliceous mineral such as garnierite is one of the silicate minerals containing in laterite ore that are undesirable and must be eliminated from the ore before used as raw material for iron making industry. Calcine laterite product was obtained from reduction process in rotary kiln for 3 hours at 900 °C by transforming limonite/goethite to magnetite containing Fe 45.6 % and Ni 1.16 %. The reverse flotation tests were focused on the separation of iron mineral from nickel mineral using amine complex, ARMAC-C, a commercially available amine thioacetate as collector. Influences of pulp pH, dosages of collector amine complex and frother, and also solid percent of pulp on the reverse flotation of calcine laterite ore were investigated. The optimal condition was obtained at pH 10, collector 1000 g/t and frother 25 g/t at solid percent of 30%. The test results show that after one-stage rough reverse flotation the concentrate had Fe and Ni grades of 77.5% and 0.5% with recoveries of 57.3% and 33.7%, respectively. Therefore, it is possible to use iron-rich lateritic ore to produce magnetic concentrates by using magnetizing roasting followed by reverse iron flotation.
EFFECT OF OXIDIZING AGENTS IN EXTRACTING GOLD FROM ANODE SLIME Isyatun Rodliyah; Nuryadi Saleh; Ngurah Ardha; Zaki Mubarok
Indonesian Mining Journal Vol 16, No 3 (2013): INDONESIAN MINING JOURNAL Vol. 16 No. 3 OCTOBER 2013
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2306.431 KB) | DOI: 10.30556/imj.Vol16.No3.2013.382

Abstract

Anode slime is a byproduct collected from electro refining copper process. The valuable metals present in the slime are Au, Ag, Pt, Pd and Pb. Yet, the slime has not been processed in Indonesia but sent to another country. Extracting the gold from anode slime had been attempted in the laboratory by applying wet chlorination method. Sodium hypochlorite (NaOCl) and hydrogen peroxide (H2O2) served as the oxidizing agents. Effects of various parameters such as solvent concentration, leaching time and temperature on the percent extraction of gold were studied. The optimum recovery of gold with NaOCl is 98.86 % Au at leaching temperature of 40°C, solvent concentration 5 M, NaOCl 5 mL and 20% solid after 120 minutes leaching time. Silver loss under this condition is 2–3%. Leaching the gold by H2O2 provided the highest gold extraction of 99.99% Au at 7M HCl concentration, temperature 60°C, H2O2 0.5 M, leaching time 180 minutes, and 20% solid. The silver loss under this condition is only 0.6%.
STUDY ON REDUCTION OF IRON ORE CONCENTRATE IN ROTARY KILN TO PRODUCE DIRECT REDUCED IRON Nuryadi Saleh; Siti Rochani
Indonesian Mining Journal Vol 22, No 2 (2019): INDONESIAN MINING JOURNAL, Vol. 22 No. 2, October 2019
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1371.761 KB) | DOI: 10.30556/imj.Vol22.No2.2019.1016

Abstract

A direct reduced iron (DRI) was prepared using iron concentrate pellets and a coal as a reductant through three stages, namely, the first: iron concentrate pellets were dried by slow heating at 150°C to remove water content, the second: they were heated at 1,200°C to reduce magnetite into hematite which was treated in two different conditions, namely by oxygen and without oxygen injections; and the third: they were reduced in an atmosphere of CO/CO2 at various temperatures of 950-1,200°C. In this reduction process of iron oxide would be reduced by CO to metallic iron (Fe). The experimental results showed that the metallization without oxygen injection produced the best metallization at 1,100°C and the ratio of carbon/iron (FC/Fe) of 0.52 to result 84.54%, contained 74.68% Fe and 88.34% Fetotal. The metallization by oxygen injection produced the best metallization at 1,100°C, providing result of 96.81%, Femetal of 87.88% and 90.78% of Fetotal. The iron oxides on the DRI were relatively low, namely 2.9%. In this research, prior pellets preparation a magnetic oxidation process on iron ore concentrate was also conducted and changed the magnetite into hematite. The reduction process on its pellets produced 94.15% metallization at 1,100°C, and the DRI contained 97.85% of Fetotal, 85.32% of Femetal and 5.35% of Fe oxides. Furthermore, analyzing a remained carbon of the DRI using microscopy to seek the metal structure formed. The remained carbon was reported around 1-6% C. Next smelting process, it is suggested to have a high residual carbon concentration as there will be a carbon boil mechanism to reduce iron oxides that are still lagging on the DRI.
EFFECT OF OXIDIZING AGENTS IN EXTRACTING GOLD FROM ANODE SLIME Isyatun Rodliyah; Nuryadi Saleh; Ngurah Ardha; Zaki Mubarok
Indonesian Mining Journal Vol 16 No 3 (2013): INDONESIAN MINING JOURNAL Vol. 16 No. 3 OCTOBER 2013
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol16.No3.2013.382

Abstract

Anode slime is a byproduct collected from electro refining copper process. The valuable metals present in the slime are Au, Ag, Pt, Pd and Pb. Yet, the slime has not been processed in Indonesia but sent to another country. Extracting the gold from anode slime had been attempted in the laboratory by applying wet chlorination method. Sodium hypochlorite (NaOCl) and hydrogen peroxide (H2O2) served as the oxidizing agents. Effects of various parameters such as solvent concentration, leaching time and temperature on the percent extraction of gold were studied. The optimum recovery of gold with NaOCl is 98.86 % Au at leaching temperature of 40°C, solvent concentration 5 M, NaOCl 5 mL and 20% solid after 120 minutes leaching time. Silver loss under this condition is 2–3%. Leaching the gold by H2O2 provided the highest gold extraction of 99.99% Au at 7M HCl concentration, temperature 60°C, H2O2 0.5 M, leaching time 180 minutes, and 20% solid. The silver loss under this condition is only 0.6%.
APPLICATION OF REVERSE FLOTATION METHOD FOR THE UPGRADING OF IRON OXIDE CONTAINED IN CALCINE LATERITE ORE PRAMUSANTO PRAMUSANTO; NURYADI SALEH; MUTA’ALIM MUTA’ALIM; YUHELDA DAHLAN; Muchtar Aziz
Indonesian Mining Journal Vol 11 No 1 (2008): INDONESIAN MINING JOURNAL Vol. 11 No. 1 February 2008
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol11.No1.2008.600

Abstract

Reverse flotation was adopted for Indonesian iron-rich laterite ore from Pomalaa to float siliceous minerals in the separation of iron mineral. Nickel siliceous mineral such as garnierite is one of the silicate minerals containing in laterite ore that are undesirable and must be eliminated from the ore before used as raw material for iron making industry. Calcine laterite product was obtained from reduction process in rotary kiln for 3 hours at 900 °C by transforming limonite/goethite to magnetite containing Fe 45.6 % and Ni 1.16 %. The reverse flotation tests were focused on the separation of iron mineral from nickel mineral using amine complex, ARMAC-C, a commercially available amine thioacetate as collector. Influences of pulp pH, dosages of collector amine complex and frother, and also solid percent of pulp on the reverse flotation of calcine laterite ore were investigated. The optimal condition was obtained at pH 10, collector 1000 g/t and frother 25 g/t at solid percent of 30%. The test results show that after one-stage rough reverse flotation the concentrate had Fe and Ni grades of 77.5% and 0.5% with recoveries of 57.3% and 33.7%, respectively. Therefore, it is possible to use iron-rich lateritic ore to produce magnetic concentrates by using magnetizing roasting followed by reverse iron flotation.
STUDY ON REDUCTION OF IRON ORE CONCENTRATE IN ROTARY KILN TO PRODUCE DIRECT REDUCED IRON Nuryadi Saleh; Siti Rochani
Indonesian Mining Journal Vol 22 No 2 (2019): INDONESIAN MINING JOURNAL, Vol. 22 No. 2, October 2019
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol22.No2.2019.1016

Abstract

A direct reduced iron (DRI) was prepared using iron concentrate pellets and a coal as a reductant through three stages, namely, the first: iron concentrate pellets were dried by slow heating at 150°C to remove water content, the second: they were heated at 1,200°C to reduce magnetite into hematite which was treated in two different conditions, namely by oxygen and without oxygen injections; and the third: they were reduced in an atmosphere of CO/CO2 at various temperatures of 950-1,200°C. In this reduction process of iron oxide would be reduced by CO to metallic iron (Fe). The experimental results showed that the metallization without oxygen injection produced the best metallization at 1,100°C and the ratio of carbon/iron (FC/Fe) of 0.52 to result 84.54%, contained 74.68% Fe and 88.34% Fetotal. The metallization by oxygen injection produced the best metallization at 1,100°C, providing result of 96.81%, Femetal of 87.88% and 90.78% of Fetotal. The iron oxides on the DRI were relatively low, namely 2.9%. In this research, prior pellets preparation a magnetic oxidation process on iron ore concentrate was also conducted and changed the magnetite into hematite. The reduction process on its pellets produced 94.15% metallization at 1,100°C, and the DRI contained 97.85% of Fetotal, 85.32% of Femetal and 5.35% of Fe oxides. Furthermore, analyzing a remained carbon of the DRI using microscopy to seek the metal structure formed. The remained carbon was reported around 1-6% C. Next smelting process, it is suggested to have a high residual carbon concentration as there will be a carbon boil mechanism to reduce iron oxides that are still lagging on the DRI.
Co-Authors Isyatun Rodliyah Muchtar Aziz MUTA’ALIM MUTA’ALIM Ngurah Ardha PRAMUSANTO PRAMUSANTO Siti Rochani Yuhelda Dahlan Zaki Mubarok