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Yuhelda Dahlan
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ALTERING FERROUS SULPHATE TO SYNTHETIC GOETHITE Dessy Amalia; Yuhelda Dahlan; Suganal Suganal
Indonesian Mining Journal Vol 12, No 2 (2009): INDONESIAN MINING JOURNAL Vol. 12 No. 2 June 2009
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (211.461 KB) | DOI: 10.30556/imj.Vol12.No2.2009.563

Abstract

Catalyst is required in any reaction. Coal liquefaction is one of the processes to have need of it. The most common catalyst used in the process is ferrous based catalyst. It is very influenced by pyrhotite, which may be occurred from goethite while goethite can be composed of any iron sources. The research had the use of ferrous sulphate as the main iron source, which was reacted with caustic soda. Parameters on molar ratio of the FeSO4.7H2O/NaOH were 0.2 and 0.33, reaction time applied were 3.5; 6.5 and 17.15 hours, oxygen flow rates of 100; 200; 300; 400 and 500 cc/minute were also observed. The best result was achieved at 0.2 molar ratio of the FeSO4.7H2O/NaOH within 6.5 hours by oxidation process that was containing pure goethite, while 100 cc/minute of oxygen rate was enough for the process to be happened.
APPLICATION OF REVERSE FLOTATION METHOD FOR THE UPGRADING OF IRON OXIDE CONTAINED IN CALCINE LATERITE ORE PRAMUSANTO PRAMUSANTO; NURYADI SALEH; MUTA’ALIM MUTA’ALIM; YUHELDA DAHLAN; Muchtar Aziz
Indonesian Mining Journal Vol 11, No 1 (2008): INDONESIAN MINING JOURNAL Vol. 11 No. 1 February 2008
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (510.563 KB) | DOI: 10.30556/imj.Vol11.No1.2008.600

Abstract

Reverse flotation was adopted for Indonesian iron-rich laterite ore from Pomalaa to float siliceous minerals in the separation of iron mineral. Nickel siliceous mineral such as garnierite is one of the silicate minerals containing in laterite ore that are undesirable and must be eliminated from the ore before used as raw material for iron making industry. Calcine laterite product was obtained from reduction process in rotary kiln for 3 hours at 900 °C by transforming limonite/goethite to magnetite containing Fe 45.6 % and Ni 1.16 %. The reverse flotation tests were focused on the separation of iron mineral from nickel mineral using amine complex, ARMAC-C, a commercially available amine thioacetate as collector. Influences of pulp pH, dosages of collector amine complex and frother, and also solid percent of pulp on the reverse flotation of calcine laterite ore were investigated. The optimal condition was obtained at pH 10, collector 1000 g/t and frother 25 g/t at solid percent of 30%. The test results show that after one-stage rough reverse flotation the concentrate had Fe and Ni grades of 77.5% and 0.5% with recoveries of 57.3% and 33.7%, respectively. Therefore, it is possible to use iron-rich lateritic ore to produce magnetic concentrates by using magnetizing roasting followed by reverse iron flotation.
ALTERING FERROUS SULPHATE TO SYNTHETIC GOETHITE Dessy Amalia; Yuhelda Dahlan; Suganal Suganal
Indonesian Mining Journal Vol 12 No 2 (2009): INDONESIAN MINING JOURNAL Vol. 12 No. 2 June 2009
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol12.No2.2009.563

Abstract

Catalyst is required in any reaction. Coal liquefaction is one of the processes to have need of it. The most common catalyst used in the process is ferrous based catalyst. It is very influenced by pyrhotite, which may be occurred from goethite while goethite can be composed of any iron sources. The research had the use of ferrous sulphate as the main iron source, which was reacted with caustic soda. Parameters on molar ratio of the FeSO4.7H2O/NaOH were 0.2 and 0.33, reaction time applied were 3.5; 6.5 and 17.15 hours, oxygen flow rates of 100; 200; 300; 400 and 500 cc/minute were also observed. The best result was achieved at 0.2 molar ratio of the FeSO4.7H2O/NaOH within 6.5 hours by oxidation process that was containing pure goethite, while 100 cc/minute of oxygen rate was enough for the process to be happened.
APPLICATION OF REVERSE FLOTATION METHOD FOR THE UPGRADING OF IRON OXIDE CONTAINED IN CALCINE LATERITE ORE PRAMUSANTO PRAMUSANTO; NURYADI SALEH; MUTA’ALIM MUTA’ALIM; YUHELDA DAHLAN; Muchtar Aziz
Indonesian Mining Journal Vol 11 No 1 (2008): INDONESIAN MINING JOURNAL Vol. 11 No. 1 February 2008
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol11.No1.2008.600

Abstract

Reverse flotation was adopted for Indonesian iron-rich laterite ore from Pomalaa to float siliceous minerals in the separation of iron mineral. Nickel siliceous mineral such as garnierite is one of the silicate minerals containing in laterite ore that are undesirable and must be eliminated from the ore before used as raw material for iron making industry. Calcine laterite product was obtained from reduction process in rotary kiln for 3 hours at 900 °C by transforming limonite/goethite to magnetite containing Fe 45.6 % and Ni 1.16 %. The reverse flotation tests were focused on the separation of iron mineral from nickel mineral using amine complex, ARMAC-C, a commercially available amine thioacetate as collector. Influences of pulp pH, dosages of collector amine complex and frother, and also solid percent of pulp on the reverse flotation of calcine laterite ore were investigated. The optimal condition was obtained at pH 10, collector 1000 g/t and frother 25 g/t at solid percent of 30%. The test results show that after one-stage rough reverse flotation the concentrate had Fe and Ni grades of 77.5% and 0.5% with recoveries of 57.3% and 33.7%, respectively. Therefore, it is possible to use iron-rich lateritic ore to produce magnetic concentrates by using magnetizing roasting followed by reverse iron flotation.
Co-Authors Dessy Amalia Muchtar Aziz MUTA’ALIM MUTA’ALIM NURYADI SALEH PRAMUSANTO PRAMUSANTO Suganal Suganal