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Ngurah Ardha
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LEACHING THE LEAD FROM ANODE SLIME BY AMMONIUM ACETATE SOLUTION Isyatun Rodliyah; Ngurah Ardha; Nuryadi Saleh; M. Zaki Mubarok
Indonesian Mining Journal Vol 14, No 3 (2011): INDONESIAN MINING JOURNAL Vol. 14 No. 3 October 2011
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (165.449 KB) | DOI: 10.30556/imj.Vol14.No3.2011.488

Abstract

Selective leaching the lead from anode slime from PT. Smelting (PTS) was investigated. The presence of large amount of lead in electrometallurgical anode slime courses of extraction of precious metals (Au, Ag) and other valuable metals (Bi, Se, Te, Pt and Pd) from the slime is more difficult. A process for taking off lead content in anode slime was subjecting the latter to first and second-stage leaching in a medium of an ammonium acetate solution at temperature not exceeding 80°C. Whereby lead dissolution is maximized and other metals are minimized. The effects of various parameters such as solvent concentration, leaching time, temperature, and solid/liquid ratio on the percent extraction of lead were studied. The highest recovery of lead is attained 94.9% Pb at the leaching temperature of 70°C, solvent concentration of 8 M and percent solid 20% after 120 minutes of leaching time. The leaching kinetics of lead sulfate in an ammonium acetate solution followed the ash diffusion control model and this further confirms that the activation energy of leaching is found to be 4.8 kcal/mol, to show that rate reaction can increased by mixing.
DE-ZINCING OF LEAD-COPPER SULPHIDE MINERALS FLOTATION NGURAH ARDHA
Indonesian Mining Journal Vol 14, No 1 (2011): INDONESIAN MINING JOURNAL Vol. 14 No. 1 February 2011
Publisher : Puslitbang tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (400.597 KB) | DOI: 10.30556/imj.Vol14.No1.2011.508

Abstract

Typical lead-copper-zinc sulphide minerals were found hard to be separated selectively by froth flotation in the plant practice operation due to part of sphalerite was progressively entrapped into lead-copper bulk flotation. A series of de-zincing on lead-copper flotation tests has been conducted in the laboratory to reduce unwanted zinc content. Dosages variation of common sphalerite depressant such as sodium cyanide, sodium bisulphite combined with zinc sulphate were employed in addition to flotation time and pH regula- tors alteration. The flotation results exhibit that lesser zinc component is still presence in lead-copper concentrate due to intricate association of the minerals particle. However, this study in general performs tendency of de-zincing requirement as well as improvement of lead-copper recovery by increasing con- sumption of such depressant agent and may regrind otherwise.
LEACHING THE LEAD FROM ANODE SLIME BY AMMONIUM ACETATE SOLUTION Isyatun Rodliyah; Ngurah Ardha; Nuryadi Saleh; M. Zaki Mubarok
Indonesian Mining Journal Vol 14 No 3 (2011): INDONESIAN MINING JOURNAL Vol. 14 No. 3 October 2011
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol14.No3.2011.488

Abstract

Selective leaching the lead from anode slime from PT. Smelting (PTS) was investigated. The presence of large amount of lead in electrometallurgical anode slime courses of extraction of precious metals (Au, Ag) and other valuable metals (Bi, Se, Te, Pt and Pd) from the slime is more difficult. A process for taking off lead content in anode slime was subjecting the latter to first and second-stage leaching in a medium of an ammonium acetate solution at temperature not exceeding 80°C. Whereby lead dissolution is maximized and other metals are minimized. The effects of various parameters such as solvent concentration, leaching time, temperature, and solid/liquid ratio on the percent extraction of lead were studied. The highest recovery of lead is attained 94.9% Pb at the leaching temperature of 70°C, solvent concentration of 8 M and percent solid 20% after 120 minutes of leaching time. The leaching kinetics of lead sulfate in an ammonium acetate solution followed the ash diffusion control model and this further confirms that the activation energy of leaching is found to be 4.8 kcal/mol, to show that rate reaction can increased by mixing.
DE-ZINCING OF LEAD-COPPER SULPHIDE MINERALS FLOTATION NGURAH ARDHA
Indonesian Mining Journal Vol 14 No 1 (2011): INDONESIAN MINING JOURNAL Vol. 14 No. 1 February 2011
Publisher : Balai Besar Pengujian Mineral dan Batubara tekMIRA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30556/imj.Vol14.No1.2011.508

Abstract

Typical lead-copper-zinc sulphide minerals were found hard to be separated selectively by froth flotation in the plant practice operation due to part of sphalerite was progressively entrapped into lead-copper bulk flotation. A series of de-zincing on lead-copper flotation tests has been conducted in the laboratory to reduce unwanted zinc content. Dosages variation of common sphalerite depressant such as sodium cyanide, sodium bisulphite combined with zinc sulphate were employed in addition to flotation time and pH regula- tors alteration. The flotation results exhibit that lesser zinc component is still presence in lead-copper concentrate due to intricate association of the minerals particle. However, this study in general performs tendency of de-zincing requirement as well as improvement of lead-copper recovery by increasing con- sumption of such depressant agent and may regrind otherwise.
Co-Authors Isyatun Rodliyah M. Zaki Mubarok NURYADI SALEH