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Sekarayu Dianing Putri
Department of Chemistry, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo Surabaya 60111
Chemical Engineering, Chemistry & Bioengineering Chemistry

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SYNTHESIS AND MAGNETIC PROPERTIES OF BINUCLEAR COMPLEX [N(n-C4H9)4][MnIIFeIII(ox)3] Fahimah Martak; Hamzah Fansuri; Sekarayu Dianing Putri
Indonesian Journal of Chemistry Vol 12, No 1 (2012)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (423.294 KB) | DOI: 10.22146/ijc.21377

Abstract

Binuclear complex, [N(n-C4H9)4][MnIIFeIII(ox)3] (ox=oxalate), has been synthesized and characterized. Binuclear complex with formula of [N(n-C4H9)4][MnIIFeIII(ox)3] was synthesized by forming precursor K3[Fe(ox)3] which was followed by adding manganese chloride and tetrabutyl ammonium chloride. Characterization of the complex was made by microanalysis, FT-IR spectroscopy, x-ray diffraction and Magnetic Susceptibility Balance. Magnetic moment of binuclear complex [N(n-C4H9)4][MnIIFeIII(ox)3] is 7.81 BM. The compound has higher magnetic moment than the previously reported compound with different organic cation, [N(n-C5H11)4][MnIIFeIII(ox)3]. This behavior might be associated with the decreasing range among layers on polymeric network.
Co-Authors Fahimah Martak Hamzah Fansuri