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All Journal Jurnal Teknoin Seminar Nasional Aplikasi Teknologi Informasi (SNATI) PROSIDING SEMINAR KIMIA Jurnal Kimia Mulawarman Jurnal Kimia Riset JURNAL ATOMIK Unisia
Chairul Saleh
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Religion Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Economics, Econometrics & Finance Education Energy Engineering Environmental Science Mechanical Engineering Social Sciences

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Journal : PROSIDING SEMINAR KIMIA

 1 
KORELASI KADAR ION LOGAM Pb TERHADAP KADAR PROTEIN PADA KERANG TAHU(Meretrix meretrix) YANGDIAMBIL DI PERAIRAN PANTAI BUNYU KALIMANTAN UTARA Edi Novian Jaya; Rudi Kartika; Chairul Saleh
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2017
Publisher : PROSIDING SEMINAR KIMIA

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The Research on "Correlation Pb metal ion concentration the protein content in the shells Tahu (Meretrix meretrix) taken in coastal waters Bunyu Island North Borneo". This study aims to determine the levels of metal ions Pb and protein levels in Shell tahu based on the size and area of different sampling. Then the metal ion content of Pb and protein correlated using Least Square method. Analysis of Pb metal ion levels by using AAS (Atomic Absorption Spectrophotometer) and analysis of protein content using the Kjeldahl method. In this study, the levels of metal ions Pb at area 1 with an average of 0.638 mg / L, the levels of metal ions Pb at area 2 with an average of 0,940 mg / L, the levels of metal ions Pb in area 3 with an average of 0.664 mg / L. The protein content of the mussels out in area 1 with an average of 13.9244%, protein content in area 2 obtained an average protein content of 20.3020% and area 3 obtained an average protein content of 16.1540%. Correlation Pb levels against the protein content of the Shells tahu (Meretrix meretrix) r = 0.856 Keywords: Metal Pb, Protein, Shells Tahu (Meretrix meretrix), AAS (atomic absorption spectrophotometer), Kjeldahl Method
SINTESIS GLUTAMIDA DARI METIL ESTER MINYAK BIJI KARET (Hevea brasiliensis) DENGAN ASAM GLUTAMAT Citra Uli Sitompul; Chairul Saleh; Daniel Daniel
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2017
Publisher : PROSIDING SEMINAR KIMIA

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Synthesis of glutamide from methyl ester of rubber seed oil (Hevea brasiliensis) with glutamic acid by amidation reaction has been performed. The synthesis process involves extracting, esterification and amidation. The results showed that rubber seed oil content was 39,75%, acid number 20,98 mg KOH / gr and FFA level was 10,472%. Rubber seed oil was previously converted to methyl esters through esterification process so as to obtain a decrease of FFA to 1.34%. The result of GC-MS analysis shows the most dominant methyl ester composition is methyl linoleate which is 43,11%. The amidation process is carried out by reacting the rubber seed oil methyl esters with glutamic acid. Fourier Transform-Infra Red spectrum of glutamide, showing the absorption peak for N-H group at wave number 3429,43 cm-1 and the absorption peak for C=O amide group at wave number 1643,35 cm-1. Keywords: Rubber Seed Oil, Esterification, Amidation, Glutamide.
PROFIL TUMBUHAN UMBI LOKIO (Allium chinense G.Don) Yohana Pebrina Pasaribu; Chairul Saleh; Daniel Daniel
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2019
Publisher : PROSIDING SEMINAR KIMIA

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Tumbuhan umbi Lokio (Allium chinense G.Don) merupakan tanaman pangan yang dikonsumsi sebagai bumbu masakan, sayuran dan obat sehingga perlu dilakukan pengujian untuk mengetahui profil dari umbi Lokio. Profil ekstrak kasar umbi Lokio ditinjau dari hasil uji fitokimia terkandung senyawa metabolit sekunder alkaloid, fenolik, triterpenoid, flavonoid dan saponin. Berdasarkan senyawa metabolit sekunder yang terkandung maka dilakukan uji aktivitas antioksidan. Uji aktivitas antioksidan ekstrak kasar umbi Lokio menunjukkan aktivitas antioksidan sangat kuat dengan nilai I50 sebesar 99,18 ppm dan dilakukan pengujian toksisitas dengan metode Brine Shirmp Lethality Test (BSLT). Uji toksisitas ekstrak umbi Lokio menunjukkan tingkat toksisitas yang toksik dengan nilai L50 sebesar 145,3647 ppm sehingga dapat dimanfaatkan untuk bahan pencarian senyawa bioaktif antikanker. Kata Kunci: Lokio (Allium chinense G.Don), Uji Fitokimia, Uji Aktivitas Antioksidan, DPPH (1,1diphenyl-2-picrylhidrazyl), Uji Toksisitas, Brine Shirmp Lethality Test (BSLT)
SINTESIS ETILENDIAMIDA DARI METIL ESTER MINYAK BIJI BINTARO (Cerbera manghas L.) MELALUI REAKSI AMIDASI DENGAN KATALIS NaOCH3 Fath Ali Akbar; Daniel Daniel; Chairul Saleh
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2017
Publisher : PROSIDING SEMINAR KIMIA

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Synthesis of ethylendimide from methyl ester of bintaro seed (Cerbera manghas L) through amidation reaction using NaOCH3 as catalyst have been done. Result of the sythesis have showed oil amount of bintaro seed are 50,36 % with acid value are 2,9192 mg KOH/g and free fatty acid are 1,4671 %. Oil of bintaro seed are converted to methyl ester using H2SO4 as catalyst for 5 hours in temperature 60-70 ºC in benzene which ratio of methanol and oil are 6:1 gave acid value are 21,4967 mg KOH/g and saponification value are 53,2352 mg KOH/g. Methyl ester of bintaro seed are reacterd with ethylendiamine and with NaOCH3 as catalyst. The result of amidation are viscous liquid and yellowish white color with acid value are 102,8435 mg KOH/g and saponification value are 33,7064 mg KOH/gram with HLB value are 13,446 which is higher than theoritically HLB value are 12,94. Analysis of FTIR showed ethylenediamide have formed which have proven by vibration of wave number at 1643,35 cm­-1 for tetiary carbonyl amide group, 1056,99 cm-1 for ─C─N─ group and 3302,13 cm-1 for ─N─H─ group, but there are wave number appearance for ester carbonyl group at 1743,65 cm-1 which showed that methyl ester are not compeletely converted into ethylenediamide. Keywords: oil of bintaro seed, esterification, amidation, ethylenediamide
SINTESIS ESTER GALAKTOSA ASAM LEMAK DARI METIL ESTER MINYAK BIJI KOPI ARABIKA (Coffea arabica) DAN GALAKTOSA ASETAT Josua K. Panannangan; Daniel Daniel; Chairul Saleh
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2017
Publisher : PROSIDING SEMINAR KIMIA

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The synthesis of ester galactose fatty acid from methyl ester of arabica coffee seed oil (Coffea arabica) and galactose acetate with a toxic solvent-free synthesis process has been performed. Methyl ester oil of coffee beans is synthesized from coffee seed oil that has been macerated for 3 days with oil content of 17% and the result of methyl ester synthesis of coffee seed oil has a yield percentage of 87.93% with methanol reaction medium with 1% H2SO4 catalyst. Galactose acetate was synthesized from galactose and anhydrous acetic acid on a 1: 1 ratio resulting in galactose acetate with a yield percentage of 91.29%. The synthesis of fatty acid galactose ester from methyl ester coffee seed oil and galactose acetate was synthesized with a 1: 1 mole ratio using a 1 M M NaHCO3 catalyst with a temperature of 80-100 ºC for 6 hours yielding galactosil ester of fatty acid coffee seed oil. FTIR analysis showed that ester group formed from coffee seed oil methyl ester at wave number 1745,58 cm-1. FTIR analysis of galactosil acetate showed the presence of ester group formed from galactose at wave number 1728,22 cm-1. FTIR analysis of galactose oil seed oil ester showed the presence of ester group at wave number 1743,65 cm-1 and group (CH2)n at wave number 721,38 cm-1 with value of HLB obtained 3,494. Keywords: Coffee bean oil, galactose acetate, interesterification, fatty acid ester galactose
SINTESIS ETIL ASETAT DARI HASIL FERMENTASI KULIT SINGKONG (Manihot Esculenta L) DENGAN ASAM ASETAT MENGGUNAKAN KATALIS ASAM Tri Eva Lidiawati; Chairul Saleh; Alimuddin Alimuddin
PROSIDING SEMINAR KIMIA SEMINAR NASIONAL KIMIA 2018
Publisher : PROSIDING SEMINAR KIMIA

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A study on the synthesis of ethyl acetate from fermented cassava peel (Manihot esculenta L) with acetic acid using acid catalyst has been done. Determination of the ratio of ethanol content with the addition of yeast bread and yeast tape, also to know the rendement of ethanol and ethyl acetate contained in cassava skin. Cassava leaf flour is hydrolyzed by using concentrated hydrochloric acid (HCl) then tested by reducing sugar content by nelson somogyi method and analyzed by using UV-Vis spectrophotometry. The hydrolysis result is divided into two parts and added yeast tape and bread yeast is also added nutrient NPK each and fermented for 5 days. The fermentation results were distilled off and analyzed using Chromatography Gas (GC). The obtained ethanol is reacted with acetic acid and sulfuric acid catalyst in the esterification reaction to obtain ethyl acetate. The esterification results were analyzed by IR spectroscopy. Ethanol obtained from Chromatography Gas (GC) analysis of 13% and esterification results from IR spectroscopic analysis showed the presence of ester (ethyl acetate) formed. Keywords: Cassava Leather, Fermentation, Esterification, Ethyl Acetate.
REVIEW JURNAL: POTENSI DAUN NIPAH DALAM OBAT TRADISIONAL SEBAGAI AKTIVITAS ANTIINFLAMASI Angellina Putri Petrisia; Chairul Saleh; Djihan Ryn Pratiwi
PROSIDING SEMINAR KIMIA Vol 1 No 2 (2023): Prosiding SNKT II 2022
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Nipah (Nypa fruticans Wurmb) is a mangrove plant from the Palmae tribe that grows along rivers that are affected by tides. The abundance of nipa palm in mangrove forests is quite high, so it has great potential to be developed. This review aims to discuss the potential anti-inflammatory activity of nipah leaves as traditional medicine, so that they can add value to nipah leaves and can be useful in the health sector. The literature search was carried out through Google Scholar and Scholar research papers related to the ability of anti-inflammatory activity in nipah leaves and other Arecaceae families. Nipah leaf extract contains secondary metabolites, namely flavonoids, phenolics, tannins, steroid saponins and triterpenoids. Flavonoids can function as inhibitors of cyclooxygenase and lipoxygenase enzymes so that they can be used to treat anti-inflammatory. Based on the literature, it can be concluded that nipah leaves are potentially effective as traditional medicine in treating inflammation or inflammation. Keywords: Nipah (Nypa fruticans Wurmb), anti-inflammatory and flavonoids
AKTIVITAS ANTIBAKTERI EKSTRAK METANOL DAUN KENITU (Chrysophyllum cainito L.) TERHADAP Salmonella thypi ATCC 422 Ade Dinaran; Chairul Saleh; Djihan Ryn Pratiwi
PROSIDING SEMINAR KIMIA Vol 1 No 2 (2023): Prosiding SNKT II 2022
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Kenitu (Chrysophyllum cainito L.) is one of the plants that has the potential to cure fever, diarrhea and inflammation of the respiratory tract. This study aimed to determine the minimum inhibitory concentration value of kenitu leaf methanol extract (Chrysophyllum cainito L.) against Salmonella thypi bacteria ATCC 422. The minimum inhibitory concentration value of kenitu (Chrysophyllum cainito L.) against Salmonella thypi ATCC 422 bacteria was 0.625 %. The presence of antibacterial activity of kenitu leaf methanol extract (Chrysophyllum cainito L.) contains secondary metabolite compounds of alkaloid, phenolic and steroid groups. Keywords: Chrysophyllum cainito L., antibacterial, minimum inhibitory concentration, Salmonella thypi ATCC 422
EKSTRAKSI DAN PREPARASI GLUKOMANAN UMBI PORANG (Amorphophallus muelleri Blume) SEBAGAI EDIBLE FILM Juntia Kirana Pratiwi; Subur P. Pasaribu; Chairul Saleh; Aman Sentosa Panggabean
PROSIDING SEMINAR KIMIA Vol 1 No 2 (2023): Prosiding SNKT II 2022
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Glucomannan extracted from porang tubers (Amorphophallus muelleri Blume) can be used as a raw material for made edible films. In this research, extraction of glucomannan with graded ethanol method resulted in a yield of 10% and the composition of the edible film forming solution used was 6% glucomannan porang tubers and 25% (w/w) glycerol. The resulted edible film was clear and transparent with the characteristics tested are water content, thickness and water vapor transmission respectvely 20.16%, 0.15 m2 and 22.89 g/m2/hour. Based on the results of SEM analysis showed that the surface of the edible film of glucomannan porang tubers, the morphology of the surface was somewhat smooth but still less homogeneous. So, efforts are still needed to improve the characteristics so that to acording the required standards Keywords: Preparation, edible film, glucomannan, porang tubers
UJI AKTIVITAS ANTIINFLAMASI DARI EKSTRAK METANOL DAUN KENITU (Chrysopyllum cainito L.) SECARA IN VITRO Nur Hidayah; Chairul Saleh; Djihan Ryn Pratiwi
PROSIDING SEMINAR KIMIA Vol 1 No 2 (2023): Prosiding SNKT II 2022
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

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Antiinflammatory activity tests of extract and fractions of kenitu Leaves (Chrysopyllum cainito L) in vitro were carried out. This research aimed to determine the anti-inflammatory activity of crude extract methanol of kenitu leave with protein denaturation inhibition method by using BSA (Bovine serum albumin). Diclofenac sodium was used as positive control and the negative control used the appropriate solvent. Based on phytochemical screening test, methanol extracts are known to contain secondary metabolites including flavonoids, alkaloids and phenolics. The results of the anti-inflammatory activity test of methanol extract have moderate anti-inflammatory potential with an IC50 value of 196,29 ppm. Keywords: Chrysopyllum cainito L, Secondary metabolites, Anti-inflammatory, 50% inhibition concentration.
Co-Authors Ade Dinaran Ade Trisna P. Alimuddin Alimuddin Aman Sentosa Panggabean Angellina Putri Petrisia Citra Uli Sitompul Daniel Daniel Daniel Tarigan Djihan Ryn Pratiwi Edi Novian Jaya Fath Ali Akbar Fiktor Boni Pasilala Josua K. Panannangan Juntia Kirana Pratiwi Nur Hamid Nur Hidayah Rabiatul Adhawiyah Al-Idrus Rudi Kartika, Rudi Subur P Pasaribu Tasik Sinta Tri Eva Lidiawati Widyanto Saptawan Priambodo Yohana Pebrina Pasaribu