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All Journal Indonesian Journal of Material Research
Yulizah Hanifah
Graduate School, Faculty of Mathematics and Natural Sciences, Sriwijaya University, Palembang, 30139, Indonesia
Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Electrical & Electronics Engineering Energy Engineering

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Preparation of Layered Double Hydroxide-Polyoxometalate Based Composite Yulizah Hanifah; Amri Amri
Indonesian Journal of Material Research Vol. 1 No. 2 (2023): July
Publisher : Magister Program of Material Science Graduate School of Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/ijmr.20231210

Abstract

Material NiAl-K3[α-PW12O40], NiAl-K4[α-SiW12O40], ZnAl-K4[α-SiW12O40] and ZnAl-K3[α-PW12O40] were created. FTIR, XRD and SEM were used to characterize the substance. The findings of the successfully completed synthesis showed that peak diffraction angle for NiAl-LDH were at 11.58°, 23.18°, 35.01°, 39.41°, 46.70°, 60.94°, and 62.26° and diffraction at 10.29°, 20.07°, 34.02°, and 60.16° for ZnAl-LDH. The composite material LDH-polyoxometalate NiAl-PW12O40 that was at angles 10.76°, 26.59°, 30.8° and 63.1° and 8.61°, 25.27°, 33.8°, 66.34° for ZnAl-plyoxometalate. The typical polyoxometalate band on the composite material’s FTIR spectrum proved tha intecalation of the substance. SEM examination revealed the aggregat for nearly all intercalated and synthesized materials.
Co-Authors Amri Amri