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Widiawati, Nina
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Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Environmental Science Materials Science & Nanotechnology Physics

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High Temperature Oxidation Behavior of ODS Ferritic Stainless Steel Fe-16Cr-4Al-1Ni-0.4Y2O3 Wafda, Hakimul; Prajitno, Djoko Hadi; Basuki, Eddy Agus; Syafiq, Ahmad; Widiawati, Nina; Andi Mustari, Asril Pramutadi
Indonesian Journal of Chemistry Vol 24, No 5 (2024)
Publisher : Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/ijc.95284

Abstract

This study investigates the isothermic oxidation behavior of the new ODS alloy Fe-16Cr-4Al-1Ni-0.4Y2O3 (% by weight) at 700, 800 and 900 °C, with exposure times of 5, 20, 50, and 100 h at each temperature. The purpose is to obtain new data on its high-temperature parabolic oxidation constant for assessing oxidation resistance. The methods used include isothermal oxidation testing, XRD, SEM-EDS characterization, and analysis of oxidation kinetics by monitoring changes in oxide thickness using microscopy and SEM-EDS. The oxide products formed on the sample surface are Fe2O3, Fe3O4, AlFe2O4, and (Fe,Cr)2O3. Al and Cr oxides are located under the dominant Fe oxide layer on the surface of the sample. The oxidation test results showed that the most protective sample was obtained at a temperature of 700 °C for 100 h with an oxide thickness of 263.99 μm. The kinetics analysis correlates strongly with the parabolic equation (R2 ≈ 1). The oxidation rate constants at temperatures of 700, 800, and 900 °C were 681.76, 2957.5, and 12300 μm2 h−1, respectively. The activation energy required by the oxidation reaction in this alloy is 136.5 kJ mol−1. This research enhances understanding and potential applications of the Fe-16Cr-4Al-1Ni-0.4Y2O3 alloy in high-temperature environments.
Corrosion Behavior of Modified F/M Steel with Ti and Dispersed Oxides: Y2O3 and ZrO2 Under High Temperature in Static Liquid Lead Setyo Hadi, Dhimas; Wafda, Hakimul; Pramutadi Andi Mustari, Asril; Trisnawan, Veri; Widiawati, Nina; Miftasani, Fitria; Hadi Prajitno, Djoko
Science and Technology Indonesia Vol. 10 No. 3 (2025): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26554/sti.2025.10.3.877-888

Abstract

This study investigates the corrosion resistance of Oxide Dispersion Strengthened (ODS) steel in a lead environment, which is crucial for Lead-Cooled Fast Reactors (LFR), a type of Generation IV nuclear reactor. To improve corrosion resistance, two types of oxides-yttrium oxide (Y2O3) and zirconium oxide (ZrO2)-were added individually and in combination to the ODS steel. The samples were synthesized via powder metallurgy and characterized using optical microscopy, X-ray diffraction (XRD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDX), and Vickers hardness testing. Corrosion testing was conducted in static liquid lead at 550°C for 75 hours. The results showed that the addition of Y2O3 and ZrO2 significantly refines grain structure, increases hardness, and promotes the formation of stable, protective oxide layers. Particularly, the dual-oxide (Y2O3+ ZrO2) sample exhibited the most uniform and effective oxide barrier, indicating improved resistance to lead corrosion. These findings demonstrate that dual-oxide dispersion is a promising strategy for improving the durability of structural materials in LFR applications.
Co-Authors Ahmad Syafiq Andi Mustari, Asril Pramutadi Basuki, Eddy Agus Djoko Hadi Prajitno Hadi Prajitno, Djoko Miftasani, Fitria Pramutadi Andi Mustari, Asril Setyo Hadi, Dhimas Trisnawan, Veri Wafda, Hakimul