Jurnal Material Kedokteran Gigi
Vol 6 No 1 (2017): JMKG Vol 6 No 1 Maret 2017

Analisis Mikrostruktur Partikel Zirkoniakalsia-silika (ZrO 2 -CaO-SiO ) Dari Pasir Zirkon Alam Indonesia Menggunakan Metode Spray Pyrolysis

Elin Karlina (Departemen Ilmu dan Teknologi Material Kedokteran Gigi Fakultas Kedokteran Gigi Universitas Padjadjaran)
Nina Djustiana (Departemen Ilmu dan Teknologi Material Kedokteran Gigi Fakultas Kedokteran Gigi Universitas Padjadjaran)
I Made Joni (Nanotechnology and Graphene Research Center Universitas Padjadjaran)
Renny Febrida (Departemen Ilmu dan Teknologi Material Kedokteran Gigi Fakultas Kedokteran Gigi Universitas Padjadjaran)
Camellia Panatarani (Nanotechnology and Graphene Research Center Universitas Padjadjaran)
Akhyar Dyni Zakyah (Departemen Ilmu dan Teknologi Material Kedokteran Gigi Fakultas Kedokteran Gigi Universitas Padjadjaran)



Article Info

Publish Date
01 Mar 2017

Abstract

Indonesian Natural Sand, Zircon, is an Indonesia’s natural resource that contains zirconia, silica, titania and alumina. In Dentistry, zirconia as one of the content in natural zircon sand, have the potential to be the material for filler composites. The purpose of this research was to analyze the Zirconia-Calcium-Silicate Particle (ZrO2CaO-SiO2) synthesized from Indonesia natural sand, zircon, in microstructural way. Methods: By synthesizing ZirconiaCalcium-Silicate particle (ZrO2-CaO-SiO2) from Indonesia natural zircon sand, using spray pyrolysis method. A precursor solution that is used consists of zirconil nitrate (Zr (NO3) 2), sodium silicate (Na2SiO3), and calcium hydroxide (Ca (OH) 2). Variations in the temperature of the reactor that are used were 4000C, 4500C, and 5000C with a feed rate of 6 L / min and a piezoelectric frequency of 1.7 MHz. Result showed that the better content in zirconia-calcium-silicate is the one that was synthesized at a temperature of 4500C, based on the results of EDS, SEM and XRD. The composition that is obtained in the zirconia-calcium-silicate particle has a ratio of 1: 14: 4 with the size of 500-1000nm, and has a tetragonal crystal zirconium silicate structure and dicalcium monoclinic silicate. From this research it can be concluded that the result that was synthesized at a temperature of 4500C is adequate to use as a filler based on the characterization result of SEM and XRD.

Copyrights © 2017






Journal Info

Abbrev

jmkg

Publisher

Subject

Dentistry Materials Science & Nanotechnology

Description

Jurnal Material Kedokteran Gigi (JMKG) is a media publication of scientific research and studies of dental materials both in the form of research, case reports, and literature review. Acceptable topics include all aspects of dentistry materials, from new material research, test characteristics, ...