Journal of Material Processing and Characterization (JMPC)
Vol 1, No 2 (2020): Articles

The Effect of Varying Water to Powder Ratios on the Microhardness and Microstructure of Mineral Trioxide Aggregate

Rethy Den (Department of Mechanical and Industrial Engineering, Universitas Gadjah Mada, Yogyakarta, Indonesia)
Rini Dharmastiti (Department of Mechanical and Industrial Engineering, Universitas Gadjah Mada, Yogyakarta, Indonesia)
Nuryono Nuryono (Department of Chemistry, Universitas Gadjah Mada, Yogyakarta, Indonesia)
Leny Yuliatun (Department of Chemistry, Universitas Gadjah Mada, Yogyakarta, Indonesia)
Widjijono Widjijono (Department of Dental Biomaterial Science, Universitas Gadjah Mada, Yogyakarta, Indonesia)



Article Info

Publish Date
07 Aug 2021

Abstract

The composition of water and powder in a mixture is one of the common problems in application as clinicians typically estimate the ratio chairside. The purpose of this study was to investigate the effect of varying water-to-powder ratios on the microhardness and microstructure of mineral trioxide aggregate (MTA). ROOTDENT MTA was investigated. One gram of cement was mixed with 0.28, 0.33, and 0.40 grams of distilled water and was stored for 1, 7, and 28 days in the water. Samples were subjected to x-ray diffraction (XRD), scanning electron microscopy (SEM), and microhardness tests. Tricalcium silicate, dicalcium silicate, zirconium dioxide, calcium carbonate, and calcium hydroxide were detected by XRD. SEM showed the presence of amorphous, porous capillary channel and capillary structure on the surface of the specimens. The SEM image for each water-to-powder ratio of the surface of the material was indistinguishable from the other. The highest microhardness was exhibited by the MTA specimen with the 0.33 water-to-powder ratio submerged in the water for 28 days.

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Journal Info

Abbrev

jmpc

Publisher

Subject

Engineering Industrial & Manufacturing Engineering Mechanical Engineering

Description

Journal of Materials Processing and Characterization (JMPC) is an international, open-access and peer-reviewed journal aimed to facilitate researchers in disseminating their research works in the field of processing and characterization of engineering materials as well as biomaterials for biomedical ...