Al-Kimia
Vol 11 No 2 (2023): DESEMBER

Characterization of Hydroxyapatite of Chicken Eggshells Composite with Gelatin as Methylene Blue Absorbent

Nurfadillah (Unknown)
Ramadani, Kurnia (Unknown)
Firnanelty (Unknown)
Chadijah, Sitti (Unknown)
Aisyah, Aisyah (Unknown)
Ilyas, Asriani (Unknown)
Nur, Arfiani (Unknown)
Adawiah, Syarifah Rabiatul (Unknown)
Andriani, Titik (Unknown)



Article Info

Publish Date
28 Dec 2023

Abstract

Chicken egg shells contain an inorganic element (CaCO3) which has potency to be a source of calcium hydroxide (Ca(OH)2) which is then reacted with diammonium hydrogen phosphate ((NH4)2HPO4) as a phosphate precursor for hydroxyapatite synthesis. This study aims to determine the characterization of hydroxyapatite from eggshells and determine the absorbability of hydroxyapatite-gelatin composites against methylene blue. Synthesis of hydroxyapatite used precipitation method. The calcination results obtained calcium hydroxide (Ca(OH)2) content in the shell of 68.3%. Analysis of hydroxyapatite with Fourier Tranform Infra-Red (FT-IR) there was a wavenumber of 3434 cm-1 perform hydroxyl groups (-OH-), 1421 cm-1 carbonate groups (-CO3-2) and 1035 cm-1, 604 cm-1, 471 cm-1 phosphate groups (-PO4-2), and analysis by x-ray diffraction revealed that pure hydroxyapatite crystals had formed at an angle of 2Ɵ = 34,08 with crystallinity of 100%. The peaks that appear on the XRD diffractogram are adjusted to the Joint Committee on Power Diffraction Standards (JCPDS) No. 09-0432. The synthesis of HAp-gelatin composites obtained typical groups such as, amine groups from gelatin and phosphate groups and carbonates from Hap. The results of methylene blue absorption using hydroxyapatite-gelatin composites have obtained optimum conditions at a ratio of 2: 4 for 240 minutes with an efficiency of 63%. Based on these data, it reveals that the longer the time given, the greater the methylene blue absorbed

Copyrights © 2023






Journal Info

Abbrev

al-kimia

Publisher

Subject

Chemistry

Description

Al-Kimia is a journal of chemistry that published by Department of Chemistry, Faculty of Science and Technology UIN Alauddin Makassar. The journal is published twice a year on January-June and July-December. This journal encompasses original research articles in all aspects of chemistry and related ...