Jurnal Fisika FLUX
Vol 21, No 2 (2024): Jurnal Fisika Flux: Jurnal Ilmiah Fisika FMIPA Universitas Lambung Mangkurat

Crystal Structure Parameter Analysis of Reduced Graphene Oxide (rGO) from Coconut Shell Charcoal

Hikmah, Utiya (Unknown)
Azizah, Aghea Tahta Wahyu (Unknown)
Hastuti, Erna (Unknown)



Article Info

Publish Date
30 Jun 2024

Abstract

In this research, reduced graphene oxide (rGO) material from coconut shell charcoal was synthesized using the modified Hummer method. The reduction process of Graphene Oxide (GO) to rGO uses the reducing agent L-Ascorbic Acid (LAA) and is assisted by microwave radiation. The samples obtained were then characterized using XRD to analyze the crystal structure parameters of the rGO samples obtained. Based on the XRD results, the data obtained was then analyzed using the Scherrer and modified Scherrer equations to determine the crystal size in the sample. In addition, the Williamson-Hall equation is also used to analyze crystal size and lattice strain. This article also analyzes XRD data using the Rietveld method using Rietica software. The output from the Rietica software obtained lattice parameter values a ≠ b ≠ c and angle α = β = γ = 90° which indicates an orthorhombic crystal lattice structure. In the refinement process, Rietica's software affects the suitability parameters in the form of R and GOF indicator values. The sample obtained was also measured for the electrical conductivity value of the rGO sample using an LCR meter.

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Journal Info

Abbrev

f

Publisher

Subject

Earth & Planetary Sciences Education Materials Science & Nanotechnology Physics

Description

Jurnal Fisika FLUX is a peer-reviewed, open access journal that publishes original research articles, review articles, as well as short communication in all areas of physics including applied physics, which includes: physics instrumentation and computation, biophysics, geophysics, physics materials, ...