Journal of Energy, Material, and Instrumentation Technology
Vol 5 No 4 (2024): Journal of Energy, Material, and Instrumentation Technology

Pengaruh Hidrolisis Asam pada Pembuatan Nanoselulosa dari Swietenia mahagoni

Gultom, Rysa Sonya Reni Paulin (Unknown)
Manurung, Posman (Unknown)
Karo Karo, Pulung (Unknown)
Suciyati, Sri Wahyu (Unknown)



Article Info

Publish Date
30 Nov 2024

Abstract

The extraction of the mahogany pulp as the main ingredient for the preparation of nanocellulose was carried out using the acid hydrolysis method. Sulfuric acid (H2SO4) was used to hydrolyze the primary constituent and sodium hydroxide (NaOH) was utilized in the delignification process. The purpose of this study is to identify the properties of nanocellulose made from mahogany hardwood on fluctuations in H2SO4 concentrations, particularly on concentration 19, 29, 39, and 45%. A Fourier Transform Infrared (FTIR) spectrophotometer, Scanning Electron Microscopy (SEM) and X-ray diffraction (XRD) were used to analyze the sample product, which is cellulose nanocrystal powder. The XRD results stated that the diameter of the nanocellulose crystal size ranged from 3-6 nm, while the SEM results showed that the sample's morphology resembled a stacked arrangement of stones. Meanwhile, the results of the FTIR indicated that the functional groups produced consisted of hydroxyl, aliphatic, aromatic rings, aryl carbonyls, and pyranose. Based on the tests, the best sample is obtained as a concentration variation of H2SO4 39%, which produces a diameter of 3.6 nm with a crystallinity index as high as 80.48%.

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Journal Info

Abbrev

jurnal

Publisher

Subject

Control & Systems Engineering Electrical & Electronics Engineering Energy Materials Science & Nanotechnology Physics

Description

Ruang lingkup penulisan dalam jurnal ini meliputi: 1. Fisika Teori Mekanika Klasik Elektromagnetik Termodinamika Mekanika Statistik Mekanika Kuantum Teori Relativitas Kuantum Gravitasi Astrofisika Kosmologi 2. Fisika Bumi (Geofisika) Geothermal Geolistrik Seismik Geomagnet 3. Fisika Material ...