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All Journal Jurnal Riset Teknologi Pencegahan Pencemaran Industri Journal of Energy, Material, and Instrumentation Technology JURNAL REKAYASA KIMIA & LINGKUNGAN
Karo Karo, Pulung
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Chemical Engineering, Chemistry & Bioengineering Chemistry Control & Systems Engineering Electrical & Electronics Engineering Energy Engineering Environmental Science Materials Science & Nanotechnology Physics

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Utilization of Iron Ore Slag in The Manufacture of Calcium Silicate Boards Hendronursito, Yusup; Amin, Muhammad; Al Muttaqii, Muhammad; Karo Karo, Pulung; Yulia, Andini; Candra Birawidha, David; Isnugroho, Kusno
Jurnal Riset Teknologi Pencegahan Pencemaran Industri Vol. 12 No. 2 (2021)
Publisher : Balai Besar Standardisasi dan Pelayanan Jasa Pencegahan Pencemaran Industri

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21771/jrtppi.2021.v12.no2.p25-33

Abstract

This study aims to determine the iron ore slag effect as an additive in particleboard based on the SNI 7705:2011 standard. Iron ore slag comes from the waste processing of iron ore into sponge iron. The iron ore slag is reduced to a size of 200 mesh. Particleboard made with the composition of slag and silica is 0:40, 8:32, 16:24, 20:20, 24:16, 32:8, and 40:0 wt%. Meanwhile, other materials were made permanent, namely PCC cement and lime 16 wt%, coconut fiber 3wt%, and water 3 wt%. They are pressed with 3 tons of pressure for 1 hour using a hydraulic press. Drying at room temperature for one day, under the hot sun for two days, then in an oven at 110 oC for 8 hrs. Analysis of the chemical composition of X-ray fluorescence and X-ray diffraction crystalline phase, SEM-EDS micro-photographs, physical tests including density and porosity, and mechanical compressive strength tests. The dominant composition of SiO2 and CaO affects the formation of silicon dioxide (SiO2), calcium silicate (CaSiO3), and dicalcium silicate (Ca2SiO4) phases. Silica has a positive effect on the compressive strength of particleboard but is different from Ca, which has an impact on reducing the compressive strength. The sem morphology shows that coconut fiber cannot withstand heating at 190 oC and results in agglomeration. The addition of 20% ore slag and silica has met the calcium silicate board SNI 7705-2011. These results can be used to develop slag waste from iron ore processing into much more useful objects.
Pengaruh Hidrolisis Asam pada Pembuatan Nanoselulosa dari Swietenia mahagoni Gultom, Rysa Sonya Reni Paulin; Manurung, Posman; Karo Karo, Pulung; Suciyati, Sri Wahyu
Journal of Energy, Material, and Instrumentation Technology Vol 5 No 4 (2024): Journal of Energy, Material, and Instrumentation Technology
Publisher : Departement of Physics, Faculty of Mathematics and Natural Sciences, University of Lampung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23960/jemit.v5i4.184

Abstract

The extraction of the mahogany pulp as the main ingredient for the preparation of nanocellulose was carried out using the acid hydrolysis method. Sulfuric acid (H2SO4) was used to hydrolyze the primary constituent and sodium hydroxide (NaOH) was utilized in the delignification process. The purpose of this study is to identify the properties of nanocellulose made from mahogany hardwood on fluctuations in H2SO4 concentrations, particularly on concentration 19, 29, 39, and 45%. A Fourier Transform Infrared (FTIR) spectrophotometer, Scanning Electron Microscopy (SEM) and X-ray diffraction (XRD) were used to analyze the sample product, which is cellulose nanocrystal powder. The XRD results stated that the diameter of the nanocellulose crystal size ranged from 3-6 nm, while the SEM results showed that the sample's morphology resembled a stacked arrangement of stones. Meanwhile, the results of the FTIR indicated that the functional groups produced consisted of hydroxyl, aliphatic, aromatic rings, aryl carbonyls, and pyranose. Based on the tests, the best sample is obtained as a concentration variation of H2SO4 39%, which produces a diameter of 3.6 nm with a crystallinity index as high as 80.48%.
Selective Reduction of High Alumina-Lateritic Nickel Ore (0.5 Ni-44Fe-16Al2O3) Nurjaman, Fajar; Wahyuningsih, Wahyuningsih; Karo Karo, Pulung; Ginting, Ediman; Shofi, Achmad; Handoko, Anton Sapto
Jurnal Rekayasa Kimia & Lingkungan Vol 14, No 2 (2019): Jurnal Rekayasa Kimia & Lingkungan (December, 2019)
Publisher : Chemical Engineering Department, Syiah Kuala University, Banda Aceh, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.23955/rkl.v14i2.14561

Abstract

In this present study, the effect of reductant dosage, temperature and holding time on selective reduction process of high alumina-lateritic nickel ore have been investigated clearly. The lateritic nickel ore was reduced with 5 until 15 wt. % anthracite and 10 wt. % sodium sulfate at reduction temperature of 950C, 1050C and 1150C for 60, 90, and 120 minutes. Magnetic separation process was then conducted to separate the concentrate and tailing. The analysis of reduced nickel ore is performed by the Atomic Absorption Spectroscopy, X-Ray Diffraction, and Secondary Electron Microscopy. The optimal process resulted from the reduction of nickel ore with 10 wt. % anthracite at the temperature of 1050C for 120 minutes which resulted in 0.84% nickel in concentrate. The troilite was not found in reduced ore. The iron grade increased along the increased of reduction temperature. The longer of holding time in selective reduction process increased the nickel grade but it decreased the iron grade.
Co-Authors Al Muttaqii, Muhammad Anton Sapto Handoko, Anton Sapto Candra Birawidha, David Ediman Ginting Fajar Nurjaman Gultom, Rysa Sonya Reni Paulin Isnugroho, Kusno Muhammad Amin Posman Manurung Shofi, Achmad Sri Wahyu Suciyati Wahyuningsih Wahyuningsih Yulia, Andini Yusup Hendronursito, Yusup