Biodegradable film is an environmentally friendly plastic replacement packaging. Areca fruit peel has the potential to make biodegradable film because it contains high cellulose, which is 34.18%. This study aims to determine the effect of glycerol addition on the characteristics of areca nut peel-based biodegradable film, to determine the effect of CMC on the characteristics of areca nut peel-based biodegradable film, and to determine the interaction of glycerol and CMC to produce the best characteristics of areca nut peel-based biodegradable film. The study was arranged in RAKL with 2 factors and 3 replications. The first factor was the addition of glycerol with concentrations of 0.5% (G1), 1% (G2), and 1.5% (G3), and the second factor was the addition of CMC consisting of concentrations of 1% (C1), 2% (C2), and 3% (C3). Areca fruit peels were dried, mashed, filtered, soaked using 2.5% NaOH, hydrolyzed using 2% H2O2, and mixed with other ingredients. The data obtained were analyzed for variance and further tested with the Least Significant Difference Test (BNT) at the 5% level. The best research results were obtained in the interaction of 1% glycerol and 3% CMC treatment with a tensile strength of 71.87 MPa, percent elongation value of 26.27%, a thickness of 0.32 mm, water vapour permeability of 7.41 g/m2/hour, and biodegradability for 28 days.
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