Jurnal Penelitian Pendidikan IPA (JPPIPA)
Vol 11 No 10 (2025): October

Effect of Temperature and Holding Time Variations in the Annealing Process of Ni-Hard Material on Machinability

Soetopo, Antonius Adi (Unknown)
Hidayat, Reza Yadi (Unknown)
Billy Heriawan (Unknown)
Muslim, Dede Buchori (Unknown)
Mudji, Paulus (Unknown)



Article Info

Publish Date
25 Oct 2025

Abstract

Ni-Hard cast iron was selected for the pump cover material because of its exceptional abrasion resistance afforded by a Ni–Cr-alloyed, martensitic matrix with hard carbides. This alloy (e.g. ASTM A532 Ni-Hard 4) typically has hardness in the 50–58 HRC range. However, this extreme hardness makes conventional machining difficult, often causing rapid tool wear and poor surface finish. In contrast, conventional cast irons like FC25 machine easily but fail prematurely under abrasive service. Thus, to balance wear resistance and machinability, we heat-treated Ni-Hard. Annealing experiments (400–600 °C and 800–1000 °C) were carried out, followed by hardness testing and machining trials. We find that high-temperature annealing (1000 °C, 4–6 h) effectively softens the Ni-Hard (to ~39–32 HRC), enabling conventional milling with minimal tool failure. Lower-temperature anneals produced little softening and even carbide precipitation. These results agree with literature on high-Cr iron annealing. The softened microstructure (spheroidized carbides, ferrite/austenite matrix) and substantially improved machinability validate Ni-Hard’s suitability after annealing for abrasive slurry pump components.

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Journal Info

Abbrev

jppipa

Publisher

Subject

Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Physics

Description

Science Educational Research Journal is international open access, published by Science Master Program of Science Education Graduate Program University of Mataram, contains scientific articles both in the form of research results and literature review that includes science, technology and teaching ...