AJARCDE (Asian Journal of Applied Research for Community Development and Empowerment)
Vol. 10 No. 3 (2026)

Synthesis of Calcium Carbonate from Carbide Lime Waste (Ca(OH)2) Using a Bubble Column Reactor with the Carbonation Method

Imanda Rahmawaty (Chemical Engineering Department, Faculty of Engineering and Science, Pembangunan Nasional "Veteran" Jawa Timur University, Surabaya, Indonesia.)
Rafi Rajendra (Chemical Engineering Department, Faculty of Engineering and Science, Pembangunan Nasional "Veteran" Jawa Timur University, Surabaya, Indonesia.)
Ketut Sumada (Chemical Engineering Department, Faculty of Engineering and Science, Pembangunan Nasional "Veteran" Jawa Timur University, Surabaya, Indonesia.)
Ni Ketut Sari (Chemical Engineering Department, Faculty of Engineering and Science, Pembangunan Nasional "Veteran" Jawa Timur University, Surabaya, Indonesia.)
Nurul Widji Triana (Chemical Engineering Department, Faculty of Engineering and Science, Pembangunan Nasional "Veteran" Jawa Timur University, Surabaya, Indonesia.)



Article Info

Publish Date
11 Sep 2026

Abstract

The acetylene gas industry generates substantial carbide lime waste (Ca(OH)2, which poses environmental challenges but offers potential as a calcium source for precipitated calcium carbonate (PCC) production. This study synthesized PCC from carbide lime waste using a Bubble Column Reactor (BCR) and optimized the carbonation process using Response Surface Methodology (RSM). The effects of Ca(OH)2 concentration (3–7%) and CO2 flow rate (3–7 L/min) on PCC purity, product mass, and yield were evaluated. The products were characterized using acid–base titration, SEM–EDX, and X-ray diffraction (XRD). SEM–EDX analysis showed that the carbide lime waste contained 44.64 wt% calcium, confirming its suitability as a calcium source. Both Ca(OH)2 concentration and CO2 flow rate significantly influenced PCC production. The optimum condition was achieved at 7% Ca(OH)2 and a CO2 flow rate of 5 L/min, producing PCC with 99.88% purity and 82.85% yield, meeting the purity requirement for paper-grade filler. These findings demonstrate the potential of carbide lime waste valorization as a sustainable waste-to-resource strategy integrating industrial waste reduction, value-added material production, and CO2 utilization. Contribution to Sustainable Development Goals (SDGs):SDG 9 — Industry, Innovation and InfrastructureSDG 12 — Responsible Consumption and ProductionSDG 13 — Climate Action

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Journal Info

Abbrev

ajarcde

Publisher

Subject

Agriculture, Biological Sciences & Forestry Earth & Planetary Sciences Education Energy Environmental Science

Description

AJARCDE (Asian Journal of Applied Research for Community Development and Empowerment) publishes papers on innovative applications, development of new technologies, and efficient solutions in agriculture, engineering, computing, economic, social, information technology, food, energy, and scientific ...