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Jurnal Kimia Terapan Indonesia

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Published by Lembaga Ilmu Pengetahuan Indonesia

ISSN : 08532788 EISSN : 25277669 DOI : -

Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Materials Science & Nanotechnology

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Search results for , issue "Vol 18, No 02 (2016)" : 5 Documents clear

Simple Purification of Vetiver Oil by Multiglass Plate System for Quality Improvement Evi Yanto; Egi Agustian; Anny Sulaswatty
Jurnal Kimia Terapan Indonesia Vol 18, No 02 (2016)
Publisher : Research Center for Chemistry - LIPI

Vetiver oil is one of essential oil from Indonesia which no synthetic substitute is available. The drawback of vetiver oil from Indonesia is smoky odor and dark appearance. To increase added value of Indonesian vetiver oil, therefore it is need method with cheap production, simple and easy to operate. Multiglass plate system (MGS) is one method to increase added value of vetiver oil. The aim of this research is to improve the vetiver oil quality in terms of appearance, odor and the physicochemical properties by MGS method and also optimize the operation condition on the vetiver oil yield and total vetiverol contents. The process parameters used on this research are to optimize the flow rate, angular and amount of glass plate. As a result, was obtained the optimum condition in 0.38 ml/sec of flow rate, 3o of glass plate angular and 5 of glass plate to increase 15% of total vetiverol contents, while the yields decreased until 5.6%. Refined vetiver oil by MGS are almost meet fulfill with Indonesia National Standard number 06-2386-2006 except total vetiverol contents and odor. Even though, the total vetiverol content increased and the odor became slightly smoky compare to raw material. Based on the results, MGS method can give higher purification of vetiverol of increase vetiver oil quality with easy to handle, low cost operation and also can moved to anywhere due to portable unit and mobile system.

Nickel Supported Natural Zeolite as a Bifunctional Catalysts for Conversion of Citronella Oil Crude to Menthols Ralentri Pertiwi; Silvester Tursiloadi; Indri Badria Adilina; Kiky Corneliasari Sembiring; Yuya Oaki
Jurnal Kimia Terapan Indonesia Vol 18, No 02 (2016)
Publisher : Research Center for Chemistry - LIPI

Characterization and catalytic activity of modified natural zeolite for the conversion of citronella oil to menthol was investigated. In this research, natural zeolite was prepared by acid activation with HCl and impregnated with Ni metal. The addition of Ni metal of around 12.5 nm in diameter provided a bifunctional catalyst for two steps of citronella oil conversion i.e. cyclization and hydrogenation. The process was performed in a one-pot reaction system by stirring at 200oC with pressure of 20 bar H2 for 3h. The reaction products changed slightly with varieties of reaction temperature and amount of catalysts employed. Results showed that Ni/NZB-HT catalyst was the best catalyst which was able to convert citronella oil to menthol with a selectivity of 50% menthol and 100% conversion of citronellal.

Carbonization of Palm Oil Empty Fruit Bunch (EFB) in Hydrothermal Processes to Produce Biochar Rakhman Sarwono; Silvester Tursiloadi; Kiky Corneliasari Sembiring
Jurnal Kimia Terapan Indonesia Vol 18, No 02 (2016)
Publisher : Research Center for Chemistry - LIPI

ABSTRACT Empty fruit bunch (EFB) of palm oil is a waste from the palm oil industries which in a large amount, those waste is not properly utilized yet. EFB is a lignocelluloses waste as a polymer with big molecule such as cellulose, lignin, and hemicelluloses that can be degraded into smaller molecules in hydrothermal carbonization (HTC) process. The HTC process of EFB will result three fractions such as gas, organic water soluble and biochar as solid residue or bio-char-water-slurry. EFB degradation is influenced by the operation conditions such as temperature, pressure, catalysts, reaction time, stirring and ratio liquid and solid. The HTC process involved many routes of reaction such as liquefaction, hydrolysis, dehydration, decarboxylation, condensation, aromatization, and polymerization. In this experiment 60 ml closed vessel was used as the HTC reactor to degrade of EFB. EFB concentration of 6.44% resulted 62% of conversion. Reaction time of 6 hours resulted 62 % of conversion. Increasing the reaction time and temperature increase the conversion of EFB. Liquid products of organic water soluble has cleared yellow color, after several hours the color become darkness that is further reaction still occurs in that solution. Solid products is biochar as brown coal, that can be easily separated and processed into powder, pellet or briquette form with outstanding storage and transport characteristics. For further economic development, biochar with excellent transport characteristics, the possibility of exporting this commodity to the world’s energy market is possible. Key words: EFB, hydrothermal, carbonization, conversion, biochar

Identification and Characterization of Bacterial Lipase from Plateu Soil in West Java Vivitri Dewi Prasasty; Vinella Winata; Muhammad Hanafi
Jurnal Kimia Terapan Indonesia Vol 18, No 02 (2016)
Publisher : Research Center for Chemistry - LIPI

Lipases are known as glycerol ester hydrolases that catalyze the hydrolysis of triglycerides into free fatty acids and glycerol. Lipases are found in human, animal, plant, and microorganisms. The aim of this research is to identify lipase producers and characterize bacterial lipase from West Java plateau soil. Plateau soil bacteria samples were isolated on lipase screening medium containing Rhodamine B. Olive oil was used as a substrate in screening and production medium bacterial lipases. From 16 bacterial isolate of lipase producers, 14 were identified as Bacillus sp. and the others were identified as Pseudomonas alcaligenes. All isolates were taken into production step to determine their lipase activities. Moreover, top 3 lipase activities out of 16 lipase activities were chosen to find the optimum pH and temperature. Both characterizations showed pH optimum and temperature optimum from each lipase. These optimum condition were used in heat stability characterization for each lipase samples. The result showed that lipase from isolate COK 2 in optimum pH 4 and temperature 50oC was the most stable lipase due to this sample has good and stable activity for 1 to 5 hours incubation time. Lipase sample from isolate COK 2 has good efficiency for lipase productivity in acid condition and high temperature. Results of this investigation could encourage utilization of these activity enhancers for various industrial applications.

The Analysis of Pulsed Electromagnetic Field Effect on Solution Conductivity Novan Agung Mahardiono; Hanif Fakhrurroja; V. Luvita; Sudaryati Cahyaningsih
Jurnal Kimia Terapan Indonesia Vol 18, No 02 (2016)
Publisher : Research Center for Chemistry - LIPI

This paper presents the observation of magnetization process variableswhich influenced the conductivity of FeSO4, MnSO4, MgCl2 and CaCl2solution. Some of the survey results revealed that there was a decrease inthe rate of particle formation of FeSO4, MnSO4, MgCl2 and CaCl2 of theions in the sample of the magnetized hard water. This study compared theconductivity of FeSO4, MnSO4, MgCl2 and CaCl2 solution before and afterthe pulsed electromagnetic field with a concentration level of 0.1 M wasgiven. Electromagnetic Water Treatment (EW) was used to generate theelectromagnetic pulse wit 9.3 mT pulsed electromagnetic filed. Tools Themeasurement of solution conductivity level conducted using BenchConductivity Meter was calibrated by Control Company with certificatenumber 4163-4997748 and traceable to the National Institute of Standardsand Technology. The measurement was conducted by observing the timefunction of solution conductivity of FeSO4, MnSO4, MgCl2, and CaCl2.The results showed that pulsed electromagnetic fields affected theconductivity of FeSO4 and CaCl2 solution by74% and 67%, respectively.Meanwhile, the lower conductivity was observed from MnSO4 and MgCl2solution with 6% due to process of magnetization which caused theinstability of the ionic bonding in the solution.

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