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Reaktor
Published by Universitas Diponegoro
ISSN : 08520798     EISSN : 24075973     DOI : https://doi.org/10.14710/reaktor.xx.x.xx-xx
Core Subject : Science, Engineering,
Chemical Engineering, Chemistry & Bioengineering Control & Systems Engineering Energy Materials Science & Nanotechnology
Reaktor invites contributions of original and novel fundamental research. Reaktor publishes scientific study/ research papers, industrial problem solving related to Chemical Engineering field as well as review papers. The journal presents paper dealing with the topic related to Chemical Engineering including: Transport Phenomena and Chemical Engineering Operating Unit Chemical Reaction Technique, Chemical Kinetics, and Catalysis Designing, Modeling, and Process Optimization Energy and Conversion Technology Thermodynamics Process System Engineering and products Particulate and emulsion technologies Membrane Technology Material Development Food Technology and Bioprocess Waste Treatment Technology
Arjuna Subject : Teknik (semua kategori) - Teknik (Lain-Lain)
Articles 8 Documents
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Search results for , issue "Volume 16 No.3 September 2016" : 8 Documents clear
Efek Aditif LPM dan HPM Terhadap Konsumsi Bahan Bakar Spesifik (Brake Specific Fuel Consumption (BSFC)) dan Emisi Jelaga Mesin Diesel Injeksi Langsung Berbahan Bakar Campuran Solar dan Jatropha dengan Cold EGR (Exhaust Gas Recirculation) S Syaiful; S Sobri
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (408.504 KB) | DOI: 10.14710/reaktor.16.3.116-122

Abstract

Diesel engines have been widely used as a mode of public transport and private vehicles because of several advantages compared to gasoline engines including greater power, fuel economy, high reliability and durability of the engine and lower CO emissions. However, diesel engines release more NOx and soot emissions into the atmosphere. This is a serious problem with the strict regulations regarding exhaust emissions. Besides problems of depletion of fossil fuel reserves require various parties to seek alternative fuels derived diesel fuel. Therefore, this work is intended to reduce soot emissions by adding LPM (low purity methanol) or wet methanol and HPM (high purity methanol) into a mixture of jatropha and diesel fuels. From this research, it is also desirable to observe the effect of methanol additive to the specific fuel consumption. Experiment method was conducted to obtain the correlation between the percentage of methanol to a brake specific fuel consumption (BSFC) and soot emissions. Methanol (LPM and HPM) was varied in the range of 5 to 15% by volume. Jatropha is in the range of 10% to 30%. The rate of EGR (exhaust gas recirculation) expressed by OEV (opening EGR valve) was varied at the opening of 0 to 100%. Engine load was varied from 25 to 100% at intervals of 25%. The engine speed was kept constant of 2000 rpm. The results show that the use of fuel mixture increases evenly BSFC of 5.2% and soot emissions of 65%. Keywords: LPM and HPM, BSFC, soot emissions, jatropha, cold EGR and diesel engine  Abstrak Mesin diesel telah banyak digunakan sebagai moda transportasi umum dan kendaraan pribadi oleh karena beberapa kelebihannya dibandingkan dengan mesin bensin diantaranya daya yang lebih besar, hemat bahan bakar, kehandalan dan ketahanan mesin yang tinggi (high realibility and durability), dan emisi CO yang lebih rendah. Akan tetapi mesin diesel melepaskan lebih banyak emisi NOx dan jelaga ke atmosfir. Hal ini menjadi permasalahan serius dengan semakin ketatnya regulasi menyangkut emisi gas buang. Selain itu permasalahan menipisnya cadangan bahan bakar fosil menuntut berbagai pihak untuk mencari bahan bakar alternatif pengganti solar. Oleh karena itu, penelitian ini bermaksud untuk mereduksi emisi jelaga dengan menambahkan LPM (low purity methanol) atau wet methanol dan HPM (high purity methanol)kedalam campuran bahan bakar jatropha dan solar. Dari penelitian ini juga diinginkan untuk mengamati pengaruh aditif metanol terhadap konsumsi bahan bakar spesifik. Metode eksperimen dilakukan untuk mendapatkan keterkaitan antara prosentase metanol terhadap brake specific fuel consumption (BSFC)dan emisi jelaga. Metanol (LPM dan HPM) divariasikan pada rentang 5% sampai 15%. Jatropha adalah pada rentang 10% sampai 30%. Laju EGR (exhaust gas recirculation) yang dinyatakan oleh OEV (opening EGR valve) divariasikan pada bukaan 0% sampai 100%. Beban mesin divariasikan dari 25% sampai 100% dengan interval 25%. Putaran mesin dipertahankan konstan 2000 rpm. Hasil-hasil penelitian menunjukkan bahwa penggunaan bahan bakar campuran rata-rata meningkatkan BSFC 5,2% dan menurunkan emisi jelaga sampai 65%.
Pre-treatment dan Fermentasi Hidrolisat Kulit Buah Kakao menjadi Asam Laktat menggunakan Lactobacillus Plantarum Dodi Irwanto; Wiratni Wiratni; Rochmadi Rochmadi; Siti Syamsiah
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (350.831 KB) | DOI: 10.14710/reaktor.16.3.123-127

Abstract

Abstract COCOA POD HUSK PRE-TREATMENT AND HYDROLYZATE FERMENTATION INTO LACTIC ACID USING LACTOBACILLUS PLANTARUM. Lactic acid is a raw material that is widely used in food industry as preservatives in meat, vegetables or canned fish. In the pharmaceutical industry is used as raw material for the manufacture of drugs. Lactic acid can be made from natural materials such as lignocellulosic waste one of them is cocoa shell waste. Indonesia is number three cocoa-producing country in the world. 70% cacao fruit components such as pod husk are composed of cellulose, hemicellulose and lignin, so it has the potential to be converted into lactic acid. In this study been the conventional method to determine the overall process in order to know what parts need to be further developed to become a method more effective and efficient. The conventional method is done through several processes, namely the delignification, hydrolysis and fermentation using microorganisms. This study aims to determine the extent of the potential for cocoa pod husk waste to be converted into lactic acid. The results showed that the pod husks delignification with sodium hydroxide solution reaches optimum at a concentration of 6% which results in lower levels of lignin from 30.46 to 24.64%. The process of acid hydrolysis of the pod husks achieve optimum conditions at a concentration of 2.0%, a temperature of 120°C and a 30 minute production of glucose at 32g/L. Glucose is the result of acid hydrolysis produces lactic acid by 13.268g/L. Keywords: lactic acid; delignification; fermentation; hydrolysis; cocoa pod husks   Abstrak Asam laktat adalah salah satu bahan baku yang banyak dimanfaatkan pada industri makanan sebagai bahan pengawet daging, sayuran atau ikan kalengan. Dalam industri farmasi digunakan sebagai bahan baku pembutan obat-obatan. Asam laktat dapat dibuat dari bahan alam berupa limbah lignoselulosa yang salah satunya adalah limbah kulit kakao. Indonesia merupakan negara penghasil kakao nomor tiga di dunia. Komponen buah kakao 70% berupa kulit buah yang terdiri dari selulosa, hemiselulosa dan lignin, sehingga berpotensi untuk dikonversi menjadi asam laktat. Pada penelitian ini dipilih metode konvensional untuk mengetahui proses secara keseluruhan sehingga diketahui bagian mana yang perlu dikembangkan lebih lanjut untuk menjadi metode yang lebih efektif dan efisien. Metode konvensional dilakukan melalui beberapa proses, yakni delignifikasi, hidrolisis, dan fermentasi menggunakan mikroorganisme. Penelitian ini bertujuan untuk mengetahui sejauh mana potensi limbah kulit buah kakao untuk dikonversi menjadi asam laktat. Hasil penelitian menunjukkan bahwa delignifikasi kulit buah kakao dengan larutan sodium hidroksida mencapai kondisi optimum pada konsentrasi 6% yang menyebabkan penurunan kadar lignin dari 30,46% menjadi 24,64%. Proses hidrolisis asam terhadap kulit buah kakao terdelignifikasi mencapai kondisi optimum pada konsentrasi 2,0%, suhu 120°C dan waktu 30 menit yang menghasilkan glukosa sebesar 32g/L. Glukosa hasil hidrolisis asam menghasilkan asam laktat sebesar 13,268g/L. Kata kunci: asam laktat; delignifikasi; fermentasi; hidrolisis; kulit buah kakao 
Potensi Biogas dan Pupuk dari Limbah Lumpur Kertas Cindy Rianti Priadi; Iftita Rahmatika; Chihiya Fitria; Dwica Wulandari; Setyo Sarwanto Moersidik
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (362.946 KB) | DOI: 10.14710/reaktor.16.3.141-146

Abstract

BIOGAS ENERGY AND FERTILIZING POTENTIAL FROM PAPER SLUDGE Paper sludge contains potential as energy and fertilizer due to the high amount of C, N and P. The aims of this study were to investigate resource recovery potential through biogas production from paper sludge only and with cow manure as co-substrate for 30-45 days in batch anaerobic digestion reactor. In addition, the fertilizer potential from digestate was also tested in Vetiveria zizanioides. Co-digestion with cow manure yielded higher methane gas up to 380 CH4/g VS due to a more optimum C/N ratio. Vetiver plants grown on digestate relatively showed the high growth performance after 4 weeks. The heavy metal accumulation from digestate was still in tolerable amount since the growth rate was not significantly different with the plant grown in fertilizer. Therefore, resource recovery technology can be an option to recover C, N and P in paper sludge to achieve sustainable waste management.  Keywords: ananerobic digestion; biogas;  fertilizer; paper sludge AbstrakLumpur dari Air Limbah industri kertas memiliki C, N dan P yang tinggi sehingga berpotensi menghasilkan energi dan menjadi pupuk, Penelitian ini bertujuan untuk meneliti pemulihan sumber daya (resource recovery) melalui produksi biogas dari lumpur kertas tanpa dan dengan ko-substrat kotoran sapi selama 30-45 hari dalam reaktor batch anaerobic digestion. Selanjutnya potensi pupuk dari digestat juga diuji dengan tumbuhan akar wangi (Vetiveria zizanioides). Setelah 45 hari, lumpur kertas dengan kotoran sapi menghasikan gas metana yang lebih besar, yaitu 380 CH4/g VS. Tanaman akar wangi yang ditanam dengan dengan digestat R2 tumbuh relatif tinggi setelah 4 minggu. Akumulasi logam berat juga masih dalam batas aman karena laju pertumbuhannya yang masih sebanding dengan tanaman yang diberi pupuk. Oleh karena itu, pemulihan sumber daya dapat diterapkan untuk memanfaatkan C, N dan P yang terkandung dalam lumpur kertas sebagai usaha pengelolaan limbah berkelanjutan.  Kata Kunci: biogas; digestasi anaerobik; lumpur kertas; pupuk 
Halal Perspective of Microbial Bioprocess Based-Food Products Muhamad Kurniadi; Andri Frediansyah
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (317.657 KB) | DOI: 10.14710/reaktor.16.3.147-160

Abstract

Halal food industries are growing rapidly in line with the growing number of World’s Muslim populations. The demand of halal food products by the non-Muslim’s countries have also increase as the increasing of the general public understanding of the strickly processed to achive halal status. Halal food is more than just a food product. It is also protect people from poisons, intoxication and hazardous substances exposure. Microbial bioprocess based-food products is one of alternative to create a variety of good quality and nutritious food products. These products can be fermented food, nutraceutical, whole microbes, probiotic and synbiotic. The presence of several microbes in gastric intestinal tract will also maintain mictobiota of human gut. Microbial agent is also important on producing the aroma, taste and color. It is also important on modifiying of food materials. As Muslim, people should follow the halal dietary laws. Halal food means any process to be a food product that is permissible of lawful by Islamic laws. It is defined in the holy Quran and the Sunnah of Prophet Muhammad. In general, the microbial based-food products are categorized into halal, haram and doubtful. To achieve the lawful status, six of main critical points in the use of microbes in food processing need to be considered. Microbial metabolite such as ethanol is one of crucial factor in order to achieve halal status of food products. In order to achieve the global halal market, several strategies must be applied to microbial bioprocess based-food industries.Keywords: microbe, halal, industry, bioprocess, critical point
Bagian belakang Vol 16 No. 3 September 2016 Widayat, W
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (251.711 KB)

Abstract

Bagian belakang yang berisi indeks judul, subyek dan author
Kinetika Release Mikrokapsul Oleoresin Jahe Merah Jayanudin Jayanudin; R Rochmadi; Meri Yulvianti; Ahmad Imanudin; Tri Rina Sari
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (730.468 KB) | DOI: 10.14710/reaktor.16.3.128--140

Abstract

Abstract RELEASE KINETICS OF RED GINGER OLEORESIN MICROCAPSULES. Red ginger oleoresin microcapsule is used to protect the active component of medicine against the negative effect of the environment, thus the microcapsule can be applied in the pharmaceutical industries. Kinetic release is used to determine the rate of red ginger oleoresin microcapsule release in human body system. The models used for this purpose are zero order, first order, Higuchi, and Korsmeyer-Peppas. These models were completed by using graphical method to get the determination coefficient (R2). The aims of this research are to determine the effect of Tripolyphosphate (TPP) concentration towards microcapsule release, to determine the red ginger oleoresin microcapsule kinetic release, and to characterize the morphology and particle sizes of red ginger oleoresin microcapsule using the Scanning Electron Microscopy (SEM). The encapsulation method was started by emulsifying process of chitosan-alginate, with various ratios of Chitosan-Alginate such as 1:2, 1:1, 2:1, and 20 gram red ginger oleoresin, and also the addition of TPP, with various concentrations for as much as 3%, 4 %, and 5%, as the crosslinking agent. The emulsion was forwarded to the spray dryer machine to produce the red ginger oleoresin microcapsule. Then, the microcapsule was treated with the mixture of KH2PO4 and NaOH (pH 6.8) for 1 hour, and sample was taken for every 10 minutes for the dissolution test. The result showed that the increase of TPP concentration will reduce the release velocity of the active compound. Kinetic model with the highest value of R2 was the Korsmeyer-Peppas model. Keywords: alginate; encapsulation; release kinetics; chitosan red ginger oleoresin;   Abstrak Mikrokapsul digunakan untuk melindungi oleoresin jahe merah yang sensitif terhadap pengaruh lingkungan, sehingga dapat diaplikasikan dalam bidang farmasi. Kinetika release digunakan untuk menentukan kecepatan release mikrokapsul oleoresin jahe merah, model yang digunakan adalah model order nol, order satu, model Higuchi, dan Model Korsmeyer-Peppas. Penyelesaian model-model ini menggunakan metode grafis dengan menentukan koefisien determinasi (R2). Tujuan penelitian ini adalah menentukan pengaruh konsentrasi sodium tripolifosfat (TPP) dan rasio berat antara kitosan dan alginate sebagai penyalut terhadap kinetika release dan karakterisasi morfologi mikrokapsul oleoresin jahe merah.  Metode enkapsulasi dimulai dengan pembentukan emulsi dari penyalut kitosan-alginat dengan rasio 1:2; 1:1; 2:1 dan 20 gram oleoresin jahe merah, penambahan TPP 3%, 4% dan 5% untuk cross-link. Emulsi dialirkan ke spray dryer untuk menghasilkan mikrokapsul oleoresin jahe merah. Uji disolusi menggunakan medium basa dengan mencampurkan KH2PO4 dan NaOH (pH 6,8) sampel diambil tiap 10 menit selama 1 jam. Hasil penelitian yang telah dilakukan didapat peningkatan konsentrasi TPP akan menurunkan kecepatan releasenya, model model kinetika dengan nilai R2 terbesar adalah model Korsmeyer-Peppas. Kata kunci: alginat; enkapsulasi; kinetika release; kitosan; oleoresin jahe merah
Pengembangan Biolarvasida Jentik Nyamuk Aedes aegypti Berbahan Aktif Ekstrak Beluntas (Pluchea indica Less.) Agus Rochmat; Mitha Fuji Adiati; Zahrotul Bahiyah
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (222.67 KB) | DOI: 10.14710/reaktor.16.3.103-108

Abstract

Abstract POTENSIAL DEVELOPMENT OF EXTRACT BELUNTAS (Plucea indica Less.) as BIOLARVACIDE TO MOSQUITO Aedes aegypti LARVAE. The eradication of Aedes aegyptY mosquito is difficult because they have the ability to adapt the environment which makes it very tough. Although, there are not disturbances due to natural phenomena or human intervention. Termination of the mosquito life cycle is an alternative to reduce the mosquito population. The antimicrobial of beluntas extract is expected to have the ability biolarvacide on mosquito larvae. The biolarvasicide of beluntas leaf extracts was determined LC50 values and strengthened by identification of the active compound. The biolarvacide tested was conducted on the larvae of Aedes aegypti with variations extract concentrations of 50, 100, 250, 500 and 1000 ppm for 24 hours observation. The experimental results found that yield of ethanol extract, extract n-hexane and ethyl acetate extract: 3.8742%, 1.2054% and 1.8627%. While the value of LC50 to extract n-hexane and ethyl acetate respectively amount to 46.09 ppm and 108.79 ppm. LC50 value obtained belong biolarvacide active and positive control using abate value LC100 Abate at a concentration of 100 ppm. The ability biolarvacide ethyl acetate fraction only make the mosquito larvae die, anwhile the fraction of n-hexane can degrade the cells larvae destroyed. The ability biolarvacide beluntas extract was corroborated by the results of GC-MS analysis which showed contains active compounds beluntas such as quinic acid, hydrazinecarboxamide, benzene acetic acid, and 1,2-benzendicarboxylic acid which is a compound of larvicides. Keywords: biolarvacide; beluntas; LC50, GC-MS  Abstrak Pemberantasan nyamuk Aedes aegypti sulit dilakukan karena mereka memiliki kemampuan adaptasi lingkungan yang membuat sangat tangguh, meski ada gangguan  akibat  fenomena  alam ataupun  intervensi manusia. Pemutusan siklus hidup nyamuk merupakan alternative dalam mengurangi populasi nyamuk. Sifat antimikroba ekstrak nyamuk diharapkan dapat memiliki kemampuan biolarvasida pada jentik nyamuk. Kemampuan biolarvasida ekstrak daun beluntas ditentukan melalui nilai LC50 dan diperkuat dengan identifikasi kandungan senyawa aktif. Uji biolarvasida ini dilakukan terhadap larva nyamuk Aedes aegypti dengan variasi konsentrasi ekstrak 50, 100, 250, 500 dan 1000 ppm selama 24 jam pengamatan. Hasil percobaan diketahui bahwa: rendemen untuk ekstrak etanol, ekstrak n-heksana dan ekstrak etil asetat masing-masing sebesar 3,8742 %, 1,2054 % dan 1,8627 % sementara nilai LC50 untuk ekstrak n-heksan dan etil asetat masing-masing sebesar 46,09 ppm dan 108,79 ppm. Nilai LC50 yang diperoleh termasuk golongan biolarvasida aktif dan kontrol positif menggunakan abate memiliki nilai LC100 Abate pada konsentrasi 100 ppm. Kemampuan biolarvasida fraksi etil asetat hanya membuat larva nyamuk mati sementara fraksi n-heksana dapat mendegradasi sel larva hingga hancur. Kemampuan biolarvasida aktif ekstrak beluntas ini dikuatkan dengan hasil analisa GC-MS yang menunjukkan bahwa kandungan senyawa aktif ekstrak daun beluntas seperti quinic acid, hydrazinecarboxamide, benzene acetic acid, dan 1,2-benzendicarboxylic acid yang merupakan senyawa larvasida.
POTENSI KATALIS PADAT ASAM GAMMA ALUMINA TERSULFATASI PADA REAKSI ESTERIFIKASI MINYAK BIJI KARET Maria Ulfah; S Subagjo
Reaktor Volume 16 No.3 September 2016
Publisher : Dept. of Chemical Engineering, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (399.365 KB) | DOI: 10.14710/reaktor.16.3.109-115

Abstract

POTENTIAL OF SULFATET ALUMINA-HETEROGENEOUS ACID CATALYST IN ESTERIFICATION RUBBER SEED OIL.  Two tipe of  catalysts have been synthesed and evaluated ( free fatty acid conversion) in esterification of rubber seed oil. The first and the second catalyst have content SO3 8,821 % and 40,715 %, respectly. The optimum condition of reaction studied : volume ratio methanol/oil  0,9-1,8 v/v;  catalyst concentration 1,67-10 % wt/v; time of reaction 1-7 hours and temperature of reaction 50-70 oC. This study  showed, the second catalyst  more active than the first catalyst. Maximum conversion from esterification reaction of rubber seed oil of the first and the second catalyst are 75 % and  97 %, respectly. The optimum condition of reaction achieved at volume ratio methanol/oil  1,8 v/v;  catalyst concentration 1,67 % wt/v; time of reaction 7 hours and temperature of reaction 70 oC.   Keywords: sulfated alumina, free fatty acid, eterification, rubber seed oil.AbstrakDua tipe katalis alumina tersulfatasi telah disintesis dan dievaluasi kinerjanya (berupa konversi Asam Lemak Bebas, ALB) pada reaksi esterifikasi asam lemak bebas minyak biji karet. Katalis tipe 1 dan tipe 2 berturut-turut memiliki kandungan SO3 8,821 % dan 40,715 %.  Kondisi optimasi reaksi yang dipelajari: rasio volume metanol/minyak 0,9-1,8 v/v; konsentrasi katalis 1,67-10 % b/v; waktu reaksi 1-7 jam dan temperatur reaksi 50-70 oC.  Hasil penelitian menunjukkan katalis tipe 2 lebih aktif dari tipe 1. Konversi ALB maksimum  dari reaksi esterifikasi minyak biji karet  dengan katalis tipe 1 dan tipe 2  berturut-turut 75 % dan 97 %.  Kondisi  optimum reaksi tersebut dicapai pada rasio volume metanol/minyak 1,8; konsentrasi katalis/minyak 1,67 % b/v; lama reaksi 7 jam dan temperatur reaksi 70 oC. Kata kunci: alumina tersulfatasi, asam lemak bebas, esterifikasi, minyak biji karet

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