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INDONESIA
Jurnal Sains Materi Indonesia
Published by BRIN Publishing
ISSN : 14111098     EISSN : 2614087X     DOI : https://doi.org/10.55981/jsmi
Core Subject : Science, Engineering,
Engineering Industrial & Manufacturing Engineering Materials Science & Nanotechnology
Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science, JUSAMI) is an international peer-reviewed journal that publishes significant and important research from all areas of materials science and engineering. The topics discussed in JUSAMI are research & development results in materials science and engineering, technological innovations and applications in industry based on materials such as polymers, ceramics, composites, metals, noble metals, metal alloys, oxides, or carbon, which are related to mechanical, magnetic, physical, optical, dielectric or electronic properties (superconductivity, semiconductivity, superionic conductivity, etc.) with discussion including synthesis, modification and development of methods; testing and characterization; simulation and modeling; nuclear engineering and its applications in materials science, etc.
Arjuna Subject : Ilmu Material (semua kategori) - Ilmu Material (Lain-Lain)
Articles 94 Documents
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Synthesis and Characterization of LaF3:Ce Scintillator Material Engkir Sukirman; Yustinus Purwamargapratala; Bambang Sugeng; Wahyudianingsih Wahyudianingsih; Indra Gunawan; Syahfandi Ahda; Agus Sudjatno; Arbi Dimyati
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.185

Abstract

Synthesis and Characterization of LaF3:Ce Scintillator Material.Synthesis and characterization of the LaF3:Ce scintillator have been carried out. Synthesis was carried out using the co-precipitation method. In this study, the raw materials used were NaF, LaCl3•7H2O, and Ce(NO3)3•6H2O with ethanol and distilled water as a solvent; while surfactants were used oleic acid. In this study, the compound LaF3:0.2Ce was synthesized. The sample was characterized by using an X-Ray Diffractometer (XRD), a Scanning Electron Microscope (SEM), and a Spectrofluorometer. The analyzed data showed that the 82.6 weight fraction of LaF3:0.2Ce phase has precipitated accompanied by the formation of NaCl and C2Ce phases of 5.1 and 12.3 weight fraction, respectively. The NaCl phase is a by-product of the chemical reaction: xLaCl3•7H2O + zCeCl3•7H2O + 3NaF → LaxCezF3 + 3NaCl + 7H2O which could be removed from the precipitate solution by an appropriate separation method, while the C2Ce one appeared as a result of heating the sample at 400ºC. The LaF3:Ce scintillator sample shows the phenomenon of a bluish glow with a lifetime, t = 6 × 10-10 seconds even in the presence of a foreign phase. The existence of NaCl and C2Ce as a local environment still makes LaF3:0.2Ce has normal lifetime characteristics.
Effect of 2-Methylimidazole Composition as Low-Temperature Application in Phenol-Formaldehyde, Glycidyl Ether Epoxy Coating Rinush Fedrikdo Paltgor; Rini Riastuti; Rizal Tresna Ramdhani; Muhammad Yunus
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.267

Abstract

The addition of materials to pile pipe at low temperatures is very challenging. Thereby, an optimum operating level is needed to produce a quality coating. Furthermore, 2-methylimidazole (2MI) was added into a phenol-formaldehyde, glycidyl ether polymer fusion bonded epoxy (FBE) coating at different concentrations of 1, 2, and 3 %wt. Thermal analysis was then carried out using differential scanning calorimetry (DSC), where the addition of 2MI decreased the curing temperature to 134.76°C due to the reduced activation energy. Potentiodynamic polarization showed the best corrosion rate of 0.00991 mm/year with a current density of 0.847μA/cm2 after adding 1 %wt 2MI. Electrochemical impedance spectroscopy (EIS) was carried out to determine the charge transfer resistance and maximum coating capacitor capacitance after adding 1 %wt 2MI, namely 9.9 kΩ and 8.45×10-5 F, respectively. The cathodic disbondment test (CD-Test) showed that the disbondment radius of the coating under the influence of the cathodic protection current was 4.32mm. Mechanical analysis by pull-off adhesion test showed a value of 7.28 MPa after the addition of 2MI 2 %wt but decreased to 6.63 MPa at 3 %wt. Therefore, the optimum addition is 1 %wt 2MI for low-temperature applications of 170 –175°C in piles with high coating performance and compliance with predetermined standards.
Preparation of Polyurethane-Modified Epoxy Coating Materials Based on Vegetable Oil Derivated Ester Muhammad Ghozali; Witta Kartika Restu; Evi Triwulandari; Lutfi Rizky Fauzi
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.271

Abstract

This study utilize vegetable oil derivatives as a polyol in polyurethane. A modification of epoxy using polyurethane was done using ester derivative of vegetable oils as polyols, which was polyethylene glycol monooleate (PEGMO). The PEGMO was synthesized via an esterification reaction. The synthesis of polyurethane-modified epoxy using polyethylene glycol monooleate ester (PME-PEGMO) was conducted by reacting epoxy, tolonate and PEGMO. Analysis results of FTIR and H-NMR showed a new absorption peak derived from the urethane bond. The mechanical and thermal properties were characterized by a universal testing machine (UTM) and thermogravimetry analysis (TGA), respectively. According to the analysis results, it is shown that the addition of polyethylene glycol monooleate ester-based polyurethane on epoxy improved the mechanical properties of the epoxy, from 69.61 kgf/cm2 to139.80 kgf/cm2. However, it decreased the thermal stability of the epoxy. At 500°C, the mass of epoxy was remaining 28%, while the PME-PEGMO was only 13%.
Characterization of Glass Fiber / Epoxy with Various Silicone Resin Addition Composite’s Compressive and Flexural Strength Muhamad Hananuputra Setianto; Herry Purnomo; Mochamad Chalid
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.277

Abstract

Glass fiber/epoxy composite was developed and used widely in manyapplications. Development on fiber and matrix of composite material was done to improve itsproperties. Improvement of the composite’s matrix can be done/by adding a modifier. Silicone resinis one kind of modifier that can be added to epoxy to improve its properties. Silicone resin willimprove the thermal stability of epoxy, but the effect on mechanical properties, especially whencombined with glass fiber, has not been done. In this study, a composite of glass fiber/epoxy with 0,10, 20, and 30 weight-% silicone resin addition was tested by compressive and flexural loadingmethods. Compressive strength and maximum strain tend to decrease with the increase of siliconeresin added. The highest compressive strength and strain were reached by a glass fiber and epoxycomposite without any modification at the value 240.63 MPa and 0.5%. Flexural strength willdecrease, but maximum strain will increase when more silicone resin is added to the matrix on theflexural test. The biggest flexural strength at 293.73 MPa was possessed by the composite withoutfurther modification, and a maximum strain of 5% was owned by the composite with 20% and 30%silicone resin addition.
Porous Carbon Black Microsphere from Palm Oil Black Liquor Jayadi Jayadi; Akhiruddin Maddu; Yessie Sari; Wahyu Bambang Widayatno; Agus Sukarto Wismogroho; Cherly Firdarini; Marga Asta Jaya Mulya
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.686

Abstract

The aim of this research is to synthesize porous carbon black microspheres from palm oil black liquor through an in-house spray pyrolysis system. The in-house spray pyrolysis (SP) system was developed using a horizontal furnace. To test the developed SP equipment, the temperature profiles within the developed spray pyrolysis chamber were examined at 3 different setting temperatures (800, 900, and 1000 °C). These temperatures were also applied for synthesizing the carbon black microspheres, with and without nitrogen as carrier gas. The morphology of carbon black produced by using SP equipment was tested by a 3D Optical Microscope and FE-SEM. The optimum temperature obtained in this study is 1000 ºC according to the characterization of carbon black microspheres produced. The FE-SEM analysis indicated the presence of spherical carbon having microstructures. This indicates that the in-house spray pyrolysis machine has been successfully developed for synthesizing carbon black microspheres.
Synthesis and Characterization of a Polystyrene-based Scintillator for Gamma Detection Marliyadi Pancoko; Hafni Lissa Nuri; Azwar Manaf; Arbi Dimyati; Abdul Jami
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.704

Abstract

This study aimed to create and examine plastic scintillators made from a polystyrene matrix, which are widely used in radiation detection due to their favorable properties such as rapid decay time, low cost, resistance to moisture, and ease of fabrication. The scintillators were doped with p-terphenyl (PTP) and 1,4-bis[2-(phenyloxazolyl)]-benzene (POPOP) using an injection method with an extruder machine. The materials were then characterized using various techniques. Fourier Transform Infrared Spectroscopy (FTIR) revealed the presence of aromatic chains which are essential for the scintillation process. Differential Scanning Calorimetry (DSC) analysis showed stable thermal properties with a glass transition temperature of approximately 100ºC. Scanning Electron Microscopy (SEM) showed that the surface of the polymer is amorphous with small bumps and protrusions likely caused by the PTP and POPOP dopants. The optical evaluation indicated that the sample could absorb UV photons up to 340 nm and emit photons in the wavelength range of 400-500 nm with a peak at 421 nm. Gamma spectra analysis indicated that the plastic scintillators performed well in gamma detection and could be used in a Radiation Portal Monitor (RPM).
Post-Consumer Recycling of Polymers for Sustainable 3D Printing Filament Material Siti Mutia Mawaddah; Mochamad Chalid; Sandrina Aras Maulidina; Cut Kayla Ashanti; Adam Febriyanto Nugraha
Jurnal Sains Materi Indonesia Vol. 25 No. 1 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.707

Abstract

3D printing technology is rapidly developing in the manufacturing industry in producing complex and easily adjustable three-dimensional objects using the help of controls from computers. Behind its advantages, the 3D printing process requires filaments from virgin polymers which generally have a high price and adversely affect the environment. Post-consumer polymer recycling is a substitute material solution from virgin polymers and is environmentally friendly so as to support the realization of a circular economy. Studies on 3D printing filaments from post-consumer polymers have been discussed in this article, especially for filaments derived from acrylonitrile butadiene styrene (ABS), polylactic acid (PLA), and polyethylene terephthalate (PET). In addition, this article also reviews the sources of recycled raw materials, difficulties during the process, mechanical properties, thermal properties and efforts to improve the quality of 3D printing products. The results show that recycling post-consumer polymers for 3D printing filament applications is a promising approach to reducing the environmental impact of 3D printing while still retaining the mechanical properties and printability of filaments. This article provides insight into several studies that address the development of 3D printing using post-consumer polymer materials.
Effect of Ammonia on the Synthesis of NMC541 Cathode Materials with the Sol-Gel Method Yustinus Purwamargapratala; Jihan Fakhriyah Safitri; Eduardus Budi Nursanto; Heri Jodi; Evvy Kartini; Anne Zulfia
Jurnal Sains Materi Indonesia Vol. 24 No. 2 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.757

Abstract

The research studied about the effect of ammonia on the synthesis of lithium-ion battery cathode materials LiNi0.5Mn0.4Co0.1O2 (NMC541) through a sol-gel method by modifying the mole ratio of ammonia to metal forming ratios (0.5; 1.0; 1.5; and 2.0). The precipitation formed at pH 11 and at temperature of 80oC. Characterization was carried out on samples resulting from pyrolysis (pyrolysis result), with calcination for once and twice at 850oC for 3 hours, X-ray diffraction pattern characterization, morphological characterization using scanning electron microscope (SEM), and conductivity characterization using an impedance capacitance conductance (LCR) meter. The result of the synthesis is in the form of spherical particles. The addition of ammonia affected the particle size distribution and stoichiometry of the metal forming NMC541, eventhough it was not significant. The ammonia to metal ratio of 1.5 (Sample N1.5-K) resulted in the distribution with the optimum particle homogeneity. The morphology of the pyrolysis and 3 hours-850oC calcined samples was dominated by spherical particles and agglomeration. Particle growth in the material is affected by heat treatment time. Samples with ammonia to metal ratio of 2.0 (N2.0-K) have the closest stoichiometry to NMC541. The total conductivity of the sample at a measurement frequency of 42Hz-1MHz is in the value range of 10-7–10-5 S.cm-1. The particle size is also affected by the calcination temperature. The effect of using ammonia in the synthesis process is not directly related to the electrical properties. However, it is related to the purity of NMC541. Samples of N1.5-K pyrolyzed result and samples of N1.0-K (3 hour 850 oC calcined) have optimum conductivity values. Agglomeration as a calcination effect lowers the conductivity value. The addition of 3 hours of calcination time does not significantly increase the conductivity value
Effect of Cold Rolling and Flash Annealing on Microstructure and Mechanical Behaviour of Austenitic Manganese Steel (Fe-1.15C-13Mn) Abdul Hanin Al Hakam; Faried Miftahur Ridlo; Rifqi Aulia Tanjung; Lia Amalia Damar; Permana Andi Paristiawan
Jurnal Sains Materi Indonesia Vol. 24 No. 2 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.758

Abstract

Austenitic manganese steel (AMS) is widely used in the mineral and mining industry under high workload condition due to its remarkable work-hardening capacity under impact. However, AMS typically has an austenitic matrix with carbides precipitated resulting in low hardness and brittle properties, which impaired its wear performance. In this study, cold deformation followed by flash annealing were conducted to improve the mechanical behavior of AMS. The experimental was carried out by solution treatment (ST), cold rolling (CR) with deformation degrees of 10% and 20%, and flash annealing (FA) at 915°C with holding times of 90 and 150 seconds. The microstructure evolution and mechanical behavior were studied. The ST produced a completely austenitic microstructure which was free of carbide, resulting in a decrease in strength and hardness, as well as improved ductility. After cold deformation, both of strength and hardness were substantially improved, followed by loss in ductility. Optical microstructures reveal the formation of deformation twin (DT) and annealing twin (AT) after cold deformed. Higher intensity of DT results in AMS with considerable strength and hardness but decrease in ductility. After FA process, cold deformed structures undergo microstructural restoration, which manifests by recovery stage at 90 s and recrystallisation stage at 150 s annealing time. At the same FA time, higher degree of deformation led to increase the hardness, while at the same degree of strain, longer annealing time led to a decrease of hardness. Moreover, both of higher degree of strain and longer annealing time during flash annealing were contributed to grain refinement, even though did not affected to the increase of tensile and hardness. In addition, 20% cold rolling followed by 150 s annealing time (CR20FA150) could be considered as an effective method to obtain the most optimum combination of strength and ductility with finer grain.
Investigation On Oxidation Behavior of Nuclear Graphite IG-110 At Elevated Temperature Herlina; Abu Khalid Rivai; Sigit Khalid Rivai
Jurnal Sains Materi Indonesia Vol. 24 No. 2 (2023): Jurnal Sains dan Materi Indonesia
Publisher : BRIN Publishing (Penerbit BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/jsmi.2023.759

Abstract

IG-110 is one of nuclear graphite types for high temperature gas cooled reactor. One of the issues of the graphite in the reactor system is the interaction with air or/and water which can reduce the integrity of the material. In this study, the sample of IG-110 has been tested at high temperature in an air environment. The oxidation test was done using a magnetic suspension balance to analyze the changes in weight with direct monitoring. The test was carried out at a temperature of 630°C. Morphological and microstructural analysis were observed and tested using scanning electron microscope (SEM) and X-ray diffractometer (XRD). The oxidation rate of the sample was relatively low. Rougher sheets shape, larger pores, and slight cracks were observed for the tested sample which indicate the traces of oxidation of the samples with no any critical damage occurred in the sample. Lattice parameters, density, crystal size, and d-space of the sample after oxidation test slightly change, which show the reversible characteristic of the sample from the temperature viewpoint.

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