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Jurnal Sains Materi Indonesia
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Core Subject : Science,
Jurnal Sains Materi Indonesia (Indonesian Journal of Materials Science), diterbitkan oleh Pusat Teknologi Bahan Industri Nuklir - BATAN. Terbit pertama kali: Oktober 1999, frekuensi terbit: empat bulanan.
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Articles 865 Documents
Adsorption of Phenol and Iron In Wastewater Using a Mixture of Active Carbon and Zeolite Modified with Chitosan Ratnawati Ratnawati; Rian Hidayat; M. Cece Ariwirdana; Kudrat Sunandar; Wahyudin Wahyudin
Jurnal Sains Materi Indonesia Vol 24, No 1: OCTOBER 2022
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2022.24.1.6691

Abstract

Phenol (C6H5OH) and iron (Fe2+) contained in electroplating industrial wastewater are toxic even at small concentrations. One of the effective methods to remove these compounds is adsorption because the method is easy and simple. Activated carbon and zeolite are types of adsorbents that are often used in wastewater treatment, but both types of adsorbents are not selective in certain chemicals. In this study, modification of zeolite and activated carbon with chitosan was carried out to adsorb waste containing phenol and Fe2+. The variations used were pH (7 and 9) and the adsorbent composition to study its effect on the adsorption of phenol in the presence of Fe2+. Adsorption was carried out in a bed with circulating waste for 2 hours. Feed at pH 9 with adsorbent mixed of zeolite-chitosan composite (Z-Ch) and activated carbon-chitosan composite (AC-Ch) in a ratio of 1:1 gave the optimal results. Under these conditions, 94% and 97% of phenol and Fe2+ were adsorbed, respectively.
Influence of Glucose, Urea and Bacteria Concentration On Nata De Cassava Preparation Using Liquid Tapioca Waste Medium Muhammad Ghozali; Yenny Meliana; Witta Kartika Restu; Evi Triwulandari; Mochamad Chalid
Jurnal Sains Materi Indonesia Vol 24, No 1: OCTOBER 2022
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2022.24.1.6669

Abstract

In this research, Nata de Cassava as the obtained bacterial cellulose was synthesized by Acetobacter xylinum using the liquid tapioca waste as the media. This research aimed to investigate the influence of concentration from carbon and nitrogen sources and then the type of bacteria used toward the obtained Nata de Cassava. The liquid tapioca waste was heated in a beaker glass at 70-80 °C and then added 5-10 % (w/v) of sugar and 0.1-0.5 % (w/v) of urea. The mixed solution was poured into a container and then cooled. Furthermore, 10-20 % (v/v) of Acetobacter xylinum was added and incubated at room temperature. After ten days, the Nata de cassava was harvested, sterilized, and immersed in ethanol, then dried in an oven at 60 °C. The results of FTIR, XRD and SEM analysis showed that Nata de Cassava had been successfully synthesized. The composition that produced the highest Nata de Cassava yield of 2.41% was the composition using 15% of A. xylinum, 10% of glucose and 0.1% of urea in the fermentation medium. In addition, the composition that produced the highest carbon conversion ratio of 26.15% was the composition that used 10% of A. xylinum, 5% of glucose and 0.2% of urea in the fermentation medium.
Influence of Applied Potential on The Structural and Optical Properties of Cu2O Thin Films Grown by Electrochemical Deposition Akhiruddin Maddu
Jurnal Sains Materi Indonesia Vol 24, No 1: OCTOBER 2022
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2022.24.1.6709

Abstract

Cu2O thin films have been deposited on indium-tin-oxide (ITO) coated glass substrate by electrochemical method or electrodeposition. The effect of deposition potential on the microstructure and optical properties of Cu2O thin films was studied. Electrodeposition for two Cu2O thin films was carried out at –0.5V and –0.6V relative to the standard calomel electrode (SCE) as a reference electrode. Cu2O thin films were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), and UV-Visible spectroscopy. The diffraction pattern indicated the cubic structure of the Cu2O crystal has been well grown. The lattice parameters of Cu2O films slightly increased as the potential of electrodeposition increased. The crystallite size of Cu2O films significantly increased as the applied potential increased. Cu2O thin films showed a smooth and flat surface morphology based on SEM images. The optical transmittance of the Cu2O thin films drastically decreased as the applied potential increased due to the film thickness increasing. The bandgap energy of Cu2O films based on the Tauc plot increased as the applied potential increased, that is 2.0 eV for the film deposited at -0.5V and 2.13 eV deposited at -0.6V.
The Effect of Conventional and Sonochemical Synthesis Methods on Gd2O3 Nanoparticles Properties Muflikhah Muflikhah; W. Z. Lubis; R. P. Caesariyanti; Mujamilah Mujamilah
Jurnal Sains Materi Indonesia Vol 24, No 1: OCTOBER 2022
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2022.24.1.6674

Abstract

Paramagnetic Gd2O3 nanoparticles have been widely used as a contrast agent in bioimaging such as Magnetic Resonance Imaging (MRI). In this study, Gd2O3 nanoparticles were prepared using conventional and sonochemically precipitation methods, without any stabilizers. Gadolinium nitrate was used as a precursor and ammonium hydroxide as precipitating agent. The synthesized Gd2O3 nanoparticles were characterized using X-Ray Diffractometer (XRD), Particle Size Analyzer (PSA), Scanning Electron Microscope (SEM), and Vibrating Sample Magnetometer (VSM). It was found that Gd2O3 nanoparticles obtained in both methods have a cubic phase. The saturation magnetization (Ms) values of conventional and sonochemical samples were 1.63 emu/g and 1.44 emu/g respectively. The morphology of both samples shows agglomerated spherical shape in the nanometer range. The nanoparticles size of Gd2O3 that was confirmed by the Dynamic Light Scattering technique show samples from the sonochemical method has narrower size distribution (higher homogeneity) compare to samples from the conventional method. It was also found that the sonochemical synthesis technique is faster (time-saving), simple, convenient, and environmentally benign.
Sensing Properties of ZnO-SWCNT Hybrid Nanostructure Coated on Flexible Substrate for CO2 Gas Detection Aisyah Nur Estri
Jurnal Sains Materi Indonesia Vol 24, No 1: OCTOBER 2022
Publisher : Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.17146/jsmi.2022.24.1.6679

Abstract

We report sensing properties of functionalized single walled carbon nanotubes (f-SWCNTs) deposited on the flexible substrate of silicon (Si)  and polyethylene tereptaphalate (PET).  Deposition of f-SWCNT  on Si rubber and PET surface was conducted by applying different manner  of  spray coating and dip coating  techniques, respectively. Surface modification of f-SWCNT by ZnO nanostructure layer were applied by hydrothermal process.The research study  were conducted to know the effect of substrate material and ZnO structure on the f-SWCNT surface which embedded in those flexible polymer substrates. The results reveal that f-SWCNT on Si substrate (f-SWCNT/Si) do not have a good  response in gas sensing performance. In meanwhile  f-SWCNT on PET substrates (f-SWCNT/PET) is more sensitive about 1.6% with 3s in response.  ZnO structure layer modifying the surface structure of f-SWCNT enhance the sensitivity and responsiveness of the sensor with sensitivity of 4.1 % in 2s response after CO2 injection. Effect of bending treatment of the sensor and its stability were further investigated. Morphological surface of f-SWCNT network and crystal structure of ZnO and f-SWCNT were also observed by scanning electron microscope (SEM) and X-ray diffraction, respectively

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