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EKSTRAKSI MINYAK BIJI JENGGER AYAM (Celosia argentea var. cristata) DAN KARAKTERISASI DAN KANDUNGANNYA Hartati Soetjipto; Novenda Pramesti Ayuningtyas; November Rianto Aminu
Jurnal Kimia dan Kemasan Vol. 42 No. 2 Oktober 2020
Publisher : Balai Besar Kimia dan Kemasan

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24817/jkk.v42i2.6138

Abstract

Tujuan dari penelitian ini adalah memperoleh rendemen minyak biji jengger ayam (Celosia argentea var. cristata) dengan metode ekstraksi berkelanjutan menggunakan pelarut heksana serta menentukan komposisi kimia minyak biji jengger ayam menggunakan metode Gas Chromatography-Mass Spectrometry (GC-MS) sebelum dan setelah pemurnian. Hasil rendemen minyak biji jengger ayam sebelum dan setelah pemurnian adalah 6,79 ± 0,27% dan 1,88 ± 0,01%. Tujuh asam lemak teridentifikasi dalam minyak kasar, sedangkan empat asam lemak teridentifikasi setelah minyak dimurnikan. Asam palmitat 3,38%; skualen 89,67%; dan asam linoleat 6,58% merupakan asam lemak dominan dalam minyak biji jengger ayam hasil pemurnian.
POTENSI KENIKIR (COSMOS CAUDATUS) SEBAGAI LARVASIDA NYAMUK AEDES AEGYPTI INSTAR IV November Rianto Aminu; Alfon Pali; Sri Hartini
Jurnal Biologi Tropis Vol. 20 No. 1 (2020): Januari - April
Publisher : Universitas Mataram

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (534.381 KB) | DOI: 10.29303/jbt.v20i1.1489

Abstract

Abstrak: Resistensi temephos (abate) sebagai larvasida telah terjadi di Jawa Tengah sejak tahun 2007 dan ditahun 2017 Jawa Tengah tercatat sebagai provinsi dengan jumlah kasus DBD terbanyak ketiga secara nasional. Oleh karena itu, penelitian ini bertujuan untuk memanfaatkan ekstrak daun kenikir (Cosmos caudatus) sebagai larvasida pengganti temephos. Proses penelitian dimulai dengan ekstraksi fraksinasi, kemudian dilanjutkan dengan screening fitokimia dan uji larvasida menggunakan metode yang direkomendasikan oleh WHOPES dengan mengamati mortalitas larva nyamuk A. aegypti pada jam ke 24, 48 dan 72 pada berbagai konsentrasi larutan uji (600, 800, 1000, 1200, 1400, 1600, dan 1800 ppm). Data mortalitas larva dianalisis dengan menggunakan Rancangan Acak Kelompok (RAK) subsampling. Perbandingan antar perlakuan diuji dengan uji Beda nyata Jujur (BNJ) dengan tingkat kebermaknaan 5%. Analisa probit pada data mortalitas menghasilkan nilai dosis efektif LC50. Hasil penelitian menunjukan diantara ketiga fraksi, ekstrak kenikir fraksi heksan memiliki efek larvasida terbaik (mortalitas 71,67%) dengan LC50 sebesar 1762 ppm pada waktu paparan 72 jam. Golongan senyawa kimia yang menyebabkan efek larvasida ini adalah alkaloid, terpenoid, dan flavonoid. Walaupun ekstrak fraksi heksan tanaman ini memiliki efek larvasida, potensi pengembangan tanaman ini sebagai pengganti temepos kecil dikarenakan nilai LC50 yang tinggi pada waktu paparan yang lama.Kata kunci: Larvasida; temephos; resistensi; Cosmos caudatus; potensiAbstract: Temephos resistance as larvicide has occurred in Central Java since 2007 and in 2017 Central Java was recorded as the 3rd highest dengue cases in Indonesia. Hence, this study attempts to use extract of Cosmos caudatus as temephos substitute. The study start with fraction extraction of dried C. caudatus leaf followed by phytochemical screening of the extract and larvicide assay was carried out using method recommended by WHOPES by observing the mortality of A. aegypti larvae at 24, 48, and 72 hours on various extract concentration (600, 800, 1000, 1200, 1400, 1600, and 1800 ppm). The mortality data was analyzed using Randomized Block Design (RBD) subsampling (P<0,05). Probit analysis on mortality data result in the LC50. The result showed the most effective fraction is hexane fraction (mortality 71,67%) with LC50 ­1762 ppm at 72 hours exposure time. The active compound in the hexane fraction were alkaloid, terpenoids, and flavonoids. Even though the hexane fraction extract has the most larvicidal effect, this extract has low potential to developed as replacement to temephos because the LC50 was high and longtime exposure  Keywords: Larvicide; temephos; resistance; Cosmos caudatus; potential
Studi Kinetika dan Isoterm Adsorpsi Ion Fe (III) dan Mn (II) pada Karbon Aktif Batang Eceng Gondok Cucun Alep Riyanto; Bereka Meidelivia Raharjianti; November Rianto Aminu
Jurnal Riset Teknologi Industri Vol.15 No.1 Juni 2021
Publisher : Balai Riset dan Standardisasi Industri Samarinda

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.26578/jrti.v15i1.6633

Abstract

Batang Eceng Gondok (BEG) (Eichhornia crassipes) mengandung senyawa lignoselulosa yang dapat dimanfaatkan sebagai bahan baku pembuatan karbon aktif dengan biaya rendah dan terbarukan. Penggunaan karbon aktif dari BEG sebagai adsorben berpotensi menurunkan konsentrasi logam berat, seperti ion Fe(III) dan Mn(II). Tujuan penelitian ini adalah menentukan pemodelan kinetika dan isoterm adsorpsi karbon aktif BEG pada ion Fe(III) dan Mn(II), serta menentukan efisiensi penurunan kadar ion Fe(III) dan Mn(II) menggunakan karbon aktif BEG pada air sumur di desa Guyangan Kabupaten Jepara. Metode sintesis karbon aktif BEG dilakukan dengan proses karbonisasi pada suhu 400℃ selama 60 menit lalu dilanjutkan aktivasi kimia menggunakan H3PO4 30% pada rasio impregnasi karbon: H3PO4 (1:4, b/b) selama 24 jam serta aktivasi fisika pada suhu 600℃ selama 60 menit. Hasil penelitian menunjukkan bahwa adsorpsi karbon aktif BEG pada ion Fe(III) dan Mn(II) mengikuti pemodelan isoterm Redlich-Peterson dengan nilai R2 berturutan adalah 0,9386 dan 0,9982. Pemodelan kinetika adsorpsi karbon aktif BEG pada ion Fe(III) dan Mn(II) mengikuti pemodelan Pseudo Orde Dua dengan nilai kapasitas adsorpsi masing-masing sebesar 32,7869 mg/g dan 1,4166 mg/g. Nilai % efisiensi adsorpsi ion Fe(III) dan Mn(II) menggunakan karbon aktif BEG pada air sumur di desa Guyangan Kabupaten Jepara sebesar 23,37% dan 79,25%. Kata kunci : adsorpsi, batang eceng gondok, isoterm, karbon aktif, kinetika  
Composition of Fatty Acids and Squalene Content of Wild Spinach (Amaranthus dubius Mart) Seed Oil Soetjipto, Hartati; Krisdayanti, Mitra; Aminu, November Rianto
Makara Journal of Science Vol. 25, No. 2
Publisher : UI Scholars Hub

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

This study aims to determine the yield of wild spinach seed oil obtained by continuous extraction methods using Soxhlet apparatus for 10.5 hours in n-hexane solvent, the physio-chemical properties, and the composition of wild spinach seed oil using the Gas Chromatography-Mass Spectrometry (GC-MS) method. Refinement of wild spinach seed oil was done by degumming and neutralization. The yield of wild spinach seed oil extraction before refinement was 4.36 ± 0.29% (w/w) while after refinement was 0.68 ± 0.033% (w/w). Physio-chemical properties of wild spinach seed oil after refinement was as follows: water content 0.37%; peroxide value 9.5 meq/kg; acid value of 0.53 mg KOH/g oil; saponification value 208.9 mg KOH/g oil. The results of GC-MS analysis showed that the wild spinach seeds were composed of 5 main components: dodecanoic acid (0.28%); tetradecanoic acid (0.08%); palmitic acid (1.31%); squalene (94.9%); and linoleic acid (3.34%).
Linoleic Acid Isolation from Watermelon Seeds Oil (Citrullus lanatus L) with Urea Inclusion Method Divina Anindya Della; Hartati Soetjipto; November Rianto Aminu
EduChemia (Jurnal Kimia dan Pendidikan) Vol 7, No 2 (2022)
Publisher : Department of Chemical Education Faculty of Teacher Training and Education Universitas Su

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30870/educhemia.v7i2.15128

Abstract

Nutritional problems still become a crucial issue in Indonesian public health. Fulfillment of nutritional balance is expected to improve life quality. In humans, one of the nutrients that play a role in the growth of brain and nervous system functions is PUFA, such as omega-6 and omega-3. Besides, fulfillment of nutritional balance can prevent some diseases; especially linoleic acid used to prevent some diseases. Linoleic acid is an omega-6 and essential fatty acid. Linoleic acid is the main essential fatty acid because it is the precursor for GLA, DGLA, and AA. Omega-6 works with omega-3 and some omega-3 benefits are supported or can arise by omega-6 presence. Studies reveal that watermelon contains high linoleic acid. This study aimed to determine the optimum temperature and ratio of fatty acids: urea for the isolation of linoleic acid from watermelon seed oil. The method used was urea inclusion with a variety of temperatures (-6oC, 6oC, 18oC) and the ratio of fatty acid: urea (1:1; 1:3; 1:5). The results showed the optimum watermelon seed oil linoleic acid isolate at 18oC and the ratio of fatty acids: urea 1:5 with linoleic acid purity (%) of 82.53%.
Pengolahan Kompos: Upaya untuk Mengatasi Masalah Limbah Rumah Tangga November Rianto Aminu; Anthony Sudibya; Ida Ratnasari; Gavrila Debora Manampiring; Ni Ketut Prihatin
Magistrorum et Scholarium: Jurnal Pengabdian Masyarakat Vol 1 No 1 (2020)
Publisher : Universitas Kristen Satya Wacana Salatiga

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (596.201 KB) | DOI: 10.24246/jms.v1i12020p97-106

Abstract

Pengabdian kepada Masyarakat dilaksanakan di Desa Kalikurmo, Kecamatan Beringin Kabupaten Semarang. Kegiatan yang dilaksanakan adalah penyuluhan dan pelatihan pembuatan pupuk kompos dari limbah sisa makanan masyarakat. Metode pembuatan pupuk kompos menggunakan metode Takakura. Pembuatan kompos ini diharapkan dapat menambah nilai tambah limbah pertanian dan rumah tangga untuk menggantikan kebutuhan pupuk kimiawi dengan dapat membuat sendiri sekaligus menjaga kesuburan tanah di Desa Kalikurmo.
Pelatihan Daring Pembuatan Produk ‘Hand Sanitizer’ untuk Guru-guru di Sekolah SMP dan SD Laboratorium Satya Wacana Hartati Soetjipto; November Rianto Aminu; Yohanes Martono; Devina Intan Sari; Widhi Nugroho Meindra; Tiffany Febetania Widodo; Diyonisio Kevin Elisando
Magistrorum et Scholarium: Jurnal Pengabdian Masyarakat Vol 1 No 3 (2021)
Publisher : Universitas Kristen Satya Wacana Salatiga

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (613.671 KB) | DOI: 10.24246/jms.v1i32021p474-483

Abstract

Kegiatan Pengabdian kepada Masyarakat ini dilaksanakan dalam rangka membantu sekolah mitra dalam menerapkan protokol 3M yang salah satunya adalah menjaga kebersihan tangan. Kegiatan ini ditujukan untuk melatih petugas sekolah mitra dalam pembuatan produk Hand Sanitizer (HS) dan memberikan produk HS sebagai bahan persediaan untuk menerapkan protokol 3M di sekolah. Sebagai sekolah mitra adalah SMP dan SD Kristen Satya Wacana. Institusi sekolah merupakan salah satu tempat yang berisiko tinggi terjadi paparan virus Covid-19 sehingga penting untuk membantu penegakan protokol kesehatan dengan terjaminnya ketersediaan produk HS. Metode pelaksanaan kegiatan ini melalui pelatihan daring pembuatan produk dan pemberian produk HS kepada sekolah mitra sebagai bahan persediaan. Kegiatan ini memberikan bekal ketrampilan petugas sekolah dalam pembuatan produk HS dan menjamin ketersediaan produk HS dalam penerapan protokol kesehatan.
Pemberdayaan Masyarakat Desa Jlarem Kecamatan Gladagsari Kabupaten Boyolali (Fasilitasi Pembelajaran Kimia Siswa dan Penyuluhan Pertanian) Cucun Alep Riyanto; Sarawinda Hutagalung; November Rianto Aminu; Jumiyati Jumiyati; Pandu Krisnawan; Nur Ayu Hidayati; Ratu Anggriani Tangke Parung; Samuel Yoga Saputra; Elizabeth Elizabeth; Maria Githania Maya Krisnawati; Yos Saputra Halomoan
Magistrorum et Scholarium: Jurnal Pengabdian Masyarakat Vol 3 No 1 (2022)
Publisher : Universitas Kristen Satya Wacana Salatiga

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (716.383 KB)

Abstract

Community service is undertaken effectively to implement knowledge outside of lectures and train students' hard and soft skills as well. Community service was conducted in rural Jlarem, Gladagsari District, Boyolali Regency. The issues raised in this community service are related to the education of children and society’s agricultural knowledge. Therefore, this community service aims respectively to create programs that can improve learning methods for students and increase the people's insight in terms of managing agriculture and farm products in rural Jlarem. This community service is to address learning difficulties due to virtual learning activities during the COVID-19 pandemic and the scarcity of fertilizers and plant pests that are occurring in rural Jlarem. The method used in education was regularly tutoring with materials that have been prepared and followed by fun experiment s. Meanwhile, the agriculture tutorial was conducted by combining the presentation of the material by speakers and the following discussion. The satisfaction value is conducted by assessing questionnaires that are distributed to participants. The result of this community service is the implementation of learning guidance, and an agricultural extension program acquired a 3.6 GPA predicate of user activity respectively succeed.
Determination of Shelf Life of Herbal Products from the Combination of Stevia rebaudiana, Curcuma zanthorrhiza and Honey (Stekurmin MD) through the Accelerated Shelf Life Test (ASLT) Method Yohanes Martono; Fidelia Novitasari; November Rianto Aminu
Jurnal Kimia Sains dan Aplikasi Vol 23, No 9 (2020): Volume 23 Issue 9 Year 2020
Publisher : Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (51.378 KB) | DOI: 10.14710/jksa.23.9.325-332

Abstract

Stekurmin MD is a syrup preparation formulated from the extract of Stevia rebaudiana leaves, temu lawak (Curcuma zanthorrhiza), and honey. One of the active compounds in Stekurmin MD products is phenolic and flavonoid compounds in which the active phenolic and flavonoid compounds can be degraded during the storage period. This study aimed to determine the shelf life of Stekurmin MD products based on the degradation of phenolic compounds and flavonoids. The Accelerated Shelf Life Test (ASLT) method was used in determining the shelf life kinetics of this product. Phenolic and flavonoid concentrations were determined using the UV-Vis spectrophotometric method with the gallic acid standard for phenolic and quercetin standard for flavonoids. Degradation of phenolic and flavonoid compounds was determined every 7 days during 35 days of storage at 25, 35, 45, and 55°C ± 2°C. In natural ingredients, there is a multi-mechanism reaction. The shelf life of Stekurmin MD products based on the degradation of phenolic and flavonoid active ingredients at room temperature were 39.909 days and 23.53 hours, respectively.
Efek Larvasida Ekstrak Tegates erecta Fraksi Heksan dan Aseton terhadap Larva Nyamuk Aedes aegypti Instar 3 dan 4 November Rianto Aminu; Hartati Soetjipto; A Ign Kristijanto
JURNAL KIMIA MULAWARMAN Vol 20 No 2 (2023)
Publisher : Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/jkm.v20i2.772

Abstract

Resistance to temephos as a larvicide of A. aegyptimosquitoes has occurred in Indonesia. Therefore, it is necessary to look for other active compounds that can act as larvicides, but also environmentally friendly. This study used leaf and roots extract of T. erectahexane and acetone fraction as larvicide. The process begins with drying followed by extracting samples (leaves and roots of T. erecta) each with hexane and acetone solvents. Test solutions were made with a concentration of 0, 0.0075, 0.015, 0.03, and 0.1% (w/v) of the extract produced. Larvicide test was carried out referring to WHOPES by observing the mortality of instar larvae 3 and 4 in each extract. The results obtained showed the mortality percentage of larvae increased with increasing concentration and exposure time in both types of larvae. The lowest LC 50 was obtained from the root extract of hexane fraction (37 ppm) for 3rd instar larvae and acetone fraction (61 ppm) for instar 4 larvae. Keywords: Larvae, A. aegypti, T. erecta. Fraction