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Journal : IPTEK Journal of Proceedings Series

Microstructure and Adhesion Properties Post-Annealed Metallic Coating of Fecrbmnsi on Tube and Internal Structure Coal-Fired Boiler Agung Purniawan; Hengki Irawan; Sigit Tri Wicaksono
IPTEK Journal of Proceedings Series No 1 (2017): The 2nd International Conference on Civil Engineering Research (ICCER) 2016
Publisher : Institut Teknologi Sepuluh Nopember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j23546026.y2017i1.2200

Abstract

Iron-chrome based metallic coating is generally used to increase the life-time tube and internal structure of coal-fired boiler. The most common method used is thermal spray coating. The advantages of this method are simple in application, repair, and low cost. The post-heat treatment coating on metallic coating applied by the thermal spray method can affect to adhesion properties, the number of porosity and microstructure of coating material. The objective of this study is to analyze the influence of post-annealing on the metallic coating FeCrBMnSi applied by Twin Wire Arc-Spraying (TWAS) method on microstructure and adhesion properties which is applied on tube and internal structure of coal-fired boiler. Post-annealing was  performed after coating application in vacuum furnace with variety of temperature at 500oC, 600oC and 700o and holding time about 3 hours. Scanning Electron Microscopy (SEM) and Energy Dispersive X-Ray Spectroscopy (EDS) were used to analyze the morphology of microstructure, the uniformity of the deposit layer, and the percentage of  porosity. X- Ray Diffraction (XRD) was used  to determine phase formation and composition phase. Then, Pull Off Test was performed for adhesion test that is referred to ASTM D4541. The results shows that increasing post-annealed temperature cause microstructure of coating more crystalline,  percentage of porosity decreased from 3% As-sprayed to 1,4% at 700oC post-annealing temperature and it has an effect on the adhesion properties of coating which increase up to 25%.
Deposition of Titanium Aluminium Nitride Thin Layer on High Speed Steel Substrate by Radio Frequency Sputtering Sigit Tri Wicaksono; I G.N.B. Dwistha Prayukti; Agung Purniawan; Tri Mardji Atmono
IPTEK Journal of Proceedings Series No 1 (2017): The 2nd International Conference on Civil Engineering Research (ICCER) 2016
Publisher : Institut Teknologi Sepuluh Nopember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j23546026.y2017i1.2201

Abstract

High Speed Steel (HSS) has been widely used in manufacturing industry as one of cutting tool materials because of its good mechanical properties yet with a low price. However, since this material has a low thermal resistance property, it will limit its application when used in dry cutting process. Several methods have been used to improve the cutting performance of HSS in dry cutting. One of them was by growing a thin layer of hard coating on the contact surface of the cutting tool material. In this research, Titanium Aluminium Nitride layer were deposited on AISI M41 High Speed Steel substrate by using Radio Frequency (RF) Sputtering method. The aims of this study were to analyze the effect of variations of Aluminium surface area ratios (10, 20, 30, and 40 %) on the Titanium target and also to analyze the effect of deposition time (15, 30, and 45 minutes) on the composition, phase characterization and morphology of the thin layer that formed. The formation of TiAlN and AlN crystalline compounds were observed by X-Ray Diffraction method. A dense layer with a thickness range from 1.4 to 5.2 µm was observed by using a Scanning Electron Microscopy. It was known that the deposition time affect the thickness and also the roughness of the layer. The topography images by Atomic Force Microscopy showed that the deposition time of 45 minutes produce the finest layer with the surface roughness of 10.8 nm.
Scratch Area Effect in Coating to Protection Current Needing in ICCP System for AISI 1045 Steel in Sea Water Environment Dewanti Dewanti; Tubagus Noor Rohmannudin; Sigit Tri Wicaksono
IPTEK Journal of Proceedings Series Vol 1, No 1 (2014): International Seminar on Applied Technology, Science, and Arts (APTECS) 2013
Publisher : Institut Teknologi Sepuluh Nopember

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.12962/j23546026.y2014i1.288

Abstract

Every metal always going back to its oxide form. Steel which are oxidized having lower quality than steel which are not. Oxidizing steel will going faster if it is placed in corrosive environment. Sea water is one of the environment that support the oxidizing process. Coats are using to protect the steel in sea water. But sometimes there is some failure in coating process so the coat will have scratch damage area. The objective of this experiment is to know how much current needed to protect AISI 1045 steel which have been coated with polyethylene and given scratch area with shape variations, in sea water environment. This experiments is the continuation from the past experiences which is using sacrifice anode, on the other hand, this experiences using Impressed Current Cathodic Protection. Data which are taken from this experiment is the differentiation of potential that measured with electrode reference Cu/CuSO4, and the current measured by avometer. With ICCP system, we know that the corrosion rate in rectangular-shape scratch is faster than circle-shape scratch, and the larger the area of scratch, the larger current needed to protect the coated steel.