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All Journal INDONESIAN JOURNAL OF APPLIED PHYSICS Communications in Science and Technology Jurnal Ilmu Fisika Bulletin of Chemical Reaction Engineering & Catalysis
Prasetya, Nurdiyantoro Putra
Universitas Sebelas Maret
Astronomy Chemical Engineering, Chemistry & Bioengineering Chemistry Earth & Planetary Sciences Energy Engineering Materials Science & Nanotechnology Physics

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Variation of Indigofera tinctoria’s Immersion Time on Dye Solution and its effect on DSSC efficiency Fahru Nurosyid; Parahita Faqih; Zulaldi Yahya Dewangga; Nurdiyantoro Putra Prasetya
INDONESIAN JOURNAL OF APPLIED PHYSICS Vol 10, No 01 (2020): April
Publisher : Department of Physics, Sebelas Maret University

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (625.275 KB) | DOI: 10.13057/ijap.v10i01.21902

Abstract

The utilization of Indigo tinctoria as a DSSC sensitizer has been done to study the effect of I. tinctoria’s immersion time on DSSC efficiency. One of the most essential components in DSSC is a sensitizer or dye. In this work, the dye has been used in DSSC is the natural indigo dye from I. tinctoria leaves. The extraction was done by dissolving 50 grams of I. tinctoria leaves in 500 mililiters aquades and soaking in various time: 12, 24, 36, and 48 hours. The optical properties of dye solution was characterized by UV-Vis spectrophotometer and the current-voltage of DSSC was characterized by Keithley I-V Meter. The highest absorbance is 2.7 of 48h dye solution, but the best efficiency of DSSC is 5.39 x 10-3 % that owned 24 h cell.
Photocatalytic Properties of Co-precipitated Bismuth Cobalt Ferrite Abi Catur Saputri; Nurdiyantoro Putra Prasetya; Utari Utari; Budi Purnama
Jurnal Ilmu Fisika Vol 14 No 2 (2022): September 2022
Publisher : Universitas Andalas

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.25077/jif.14.2.116-123.2022

Abstract

Bismuth substituted cobalt ferrite nanoparticle is studied for photocatalytic in this paper.  Bismuth cobalt ferrite has been synthesized by the coprecipitation method and low-temperature annealing treatment. The characterization results showed that the XRD spectral pattern is consistent with ICDD 221086. The crystallite size of bismuth cobalt ferrite increases with increasing annealing temperature. FTIR results confirm the available metal-oxide at number wave around 570/cm and 475/cm which is the appearance of octahedral and tetrahedral sites owing cobalt ferrite. The photocatalyst test was carried out by varying the catalyst mass and UV irradiation time. The absorption spectrum decreases with increasing catalyst mass. The increase in UV irradiation time causes the formation of more holes (h+) and electrons (e-). So that the hydroxide reaction occurs that produces free radicals. The results of this study indicate that cobalt ferrite-based nanoparticles have potential as photocatalyst materials.
Annealing temperature modify of crystalline structure, magnetic properties and antibacterial performance in nickel substituted cobalt ferrite nanoparticles utilizing natural-fine-sediment Bestari, Laksmita Farah; Iqlimatussholihah, Lathifah; Prasetya, Nurdiyantoro Putra; Kusumandari; Utari; Riyatun; Purnama, Budi
Communications in Science and Technology Vol 9 No 2 (2024)
Publisher : Komunitas Ilmuwan dan Profesional Muslim Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21924/cst.9.2.2024.1495

Abstract

This study details the nickel-substituted cobalt ferrite nanoparticle employing natural fine sediment (NiCFO-fs) annealing temperature dependency of crystalline and magnetic characteristics. The NiCFO-fs nanoparticles were prepared by the coprecipitation method with varying annealing temperatures (200-500°C with increment of 100°C for five hours). As a comparison, Ni-CFO was also synthesized using pure analytical chemicals (NiCFO-pa). The XRD results showed that the whole Ni-CFO nanoparticles established an inverse spinel face center cubic (fcc) order according to space group Fd-3m for both NiCFO-fs and NiCFO-pa. There was no additional peak, indicating that Ni2+ cations successfully substituted in cobalt ferrite nanoparticles. In case of NiCFO-fs nanoparticle samples, a crystallite size (D) decreased with the increasing annealing temperature (Ta), namely 45.72 nm, 37.35 nm, 25.95 nm, and 20.51 nm. In contrast to NiCFO-pa, the D increased with the increase of the Ta, i.e., 19.67 nm, 20.74 nm, 21.99 nm, and 23.33 nm. Meanwhile, FTIR results showed the presence of metal-oxygen bonds at 551-586 cm-1 and 384-391 cm-1 at tetrahedral (k1) and the octahedral (k2) sites for both NiCFO-fs and NiCFO-pa nanoparticles samples. The VSM result showed that a narrow hysteresis curve was observed for the NiCFO-fs sample compared to NiCFO-pa. The NiCFO-fs nanoparticles owing the smallest coercive field (HC) of 79.5 Oe were attained for the Ta of 300°C. In case of NiCFO-fs samples, magnetization saturation (MS) decreased with the increase of the Ta in contrast to NiCFO-pa samples. Here, the redistribution of two and three plus ions in the sub-lattice k1 and k2 locations should be encouraged by the Jahn-Teller phenomenon through strain-induced magnetism. The findings of the antibacterial test indicated that the potential of NiCFO based on natural materials (fine sediment) was higher than that of NiCFO based on pure analytical chemicals. This result was also supported by the emergence of ZOI magnitudes for all NiCFO-fs materials compared to NiCFO-pa that was only at Ta = 300°C.
Lanthanum-substituted Cobalt Ferrite Established by the Co-precipitation Process: Annealing Temperature Adjustment of Structural, Magnetic, and Dye Removal Characteristics Rahmawati, Ramadona; Musadewi, Adiana; Prasetya, Nurdiyantoro Putra; Suharno, Suharno; Budiawanti, Sri; Rahardjo, Dwi Teguh; Riyatun, Riyatun; Utari, Utari; Iriani, Yofentina; Nuryani, Nuryani; Purnama, Budi
Bulletin of Chemical Reaction Engineering & Catalysis 2023: BCREC Volume 18 Issue 4 Year 2023 (December 2023)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.19638

Abstract

Co-precipitation process was used for the synthesis of lanthanum-substituted cobalt ferrite nanoparticles at several annealing temperatures (Ta), i.e., 200 °C, 300 °C, and 400 °C, for 5 h. XRD spectral depicted that the produced nanoparticles sample indicates a single phase of fcc inverse spinel conforming to ICDD No 22-1086. The crystallite size (D) calculation at the strongest peaks shows the increase in enhancing the Ta i.e., 18.99 nm, 19.90 nm, and 23.21 nm for 200 °C, 300 °C, and 400 °C, respectively. The FTIR results showed absorption band at the tetrahedral site, v1 ~575 cm−1 and the octahedral site, v2 ~474 cm−1. The absorption bands indicate that the lanthanum ions have successfully replaced the Fe3+ cations in the original cobalt ferrite structure. According to the hysteresis loop, the coercive field's (HC) magnitude falls from 700 Oe down to 550 Oe as Ta increases. This result is consistent with the anisotropy constant which decreased from 0.77×104 erg/cm3 to 0.56×104 erg/cm3. The obtained nanoparticles also showed superior performance (much larger than 95%) for dye removal of Congo red. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
Co-Authors Abi Catur Saputri Bestari, Laksmita Farah Budi Purnama Budi Purnama Dwi Teguh Rahardjo Fahru Nurosyid Iqlimatussholihah, Lathifah Kusumandari Musadewi, Adiana Nuryani Nuryani Parahita Faqih Rahmawati, Ramadona Riyatun Riyatun, Riyatun Sri Budiawanti Suharno Suharno Utari Utari Utari Utari Utari Yofentina Iriani Zulaldi Yahya Dewangga