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Prawiranegara, Barata Aditya
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Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Engineering Mechanical Engineering

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Hydrocarbon-Impacted Soils Supported Mn for Organic Pollutant Oxidation Saputra, Edy; Fadli, Ahmad; Prawiranegara, Barata Aditya; Amri, Amun; Heltina, Desi; Bahri, Syaiful; Sandhyavitri, Ari; Restuhadi, Fajar; Abid, Hussein Rasool; Azhar, Muhammad Rizwan; Utama, Panca Setia
Journal of Applied Materials and Technology Vol. 4 No. 2 (2023): March 2023
Publisher : AMTS and Faculty of Engineering - Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31258/Jamt.4.2.90-98

Abstract

Hydrocarbon-impeded soil (HIS) is solid waste from spills or leaks during industrial activities that negatively impact the environment. This study aims to utilize HIS as catalyst support on MnO2 to degrade RhB (RhB) solution using Peroxymonosulfate (PMS) and to determine the optimum conditions for the catalyst to degrade RhB. The catalyst was synthesized by reacting HIS, calcined with KMnO4 with various catalyst supports with high and low Total contain Petroleum Hydrocarbon (TPH). The process degradation of Rhodamine Solution was carried out with various catalysts, PMS, and RhB concentrations. The catalyst was characterized using X-ray diffraction (XRD), Nitrogen gas adsorption-desorption (BET), and Scanning Electron Microscope-Energy Disperse Spectroscope (SEM-EDX). In this study,  the best catalyst performance was MnO2@H-TPH, which could activate PMS to degrade RhB with dye removal of 98% in about 180 min, at conditions 10 g/L RhB, 0.1 g/L catalyst, and 3 g/L PMS with the activation energy of 16.3 kJ/mol.
Metal-Free Activated Carbon Catalytic for Degradation of Organic Contaminants by Peroxydisulfate Activation Prawiranegara, Barata Aditya; Setia Utama, Panca; Amri, Amun; Nurhayati; Muhdarina; Awaluddin, Amir; Saputra, Edy
Journal of Applied Materials and Technology Vol. 5 No. 1 (2023): September 2023
Publisher : AMTS and Faculty of Engineering - Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31258/Jamt.5.1.20-26

Abstract

Green chemistry has become trending recently, and the discovery of environmentally friendly catalysts is mandatory. Activated carbons (ACs) are one of the most environmentally friendly yet cheap materials that have the potential for catalyst application. Three commercially available ACs from Pancasari, Norit, and Chemical Supply were used as metal-free catalysts for advanced oxidation process (AOP) phenol removal in water in the presence of oxidants peroxydisulfate (PDS), and hydrogen peroxide (H2O2). It was found that ACs were effective to be used as catalysts for activating those oxidants to oxidize phenol in AOP reactions. In this study, the surface area of the catalyst significantly improved the phenol removal efficiency. ACs Pancasari (ACP) with the highest surface area has the best degradation performance of phenol removal with up to 99% removal efficiency in 60 minutes under the condition of [phenol] = 30 mg L-1, [ACP] = 0.2 g L-1, [PDS] = 3.3 mmol L-1, and T = 25oC. it was also found that the degradation process was significantly influenced by reaction temperature. Nevertheless, in this study, ACs display the potential as catalysts in the AOP process for wastewater treatments.
Synthesis of ?-MnO2@Mn2O3 and ?-MnO2 nanoparticles using tartaric/maleic acid and their enhanced performance in the catalytic oxidation of pulp and paper mill wastewater Sugesti, Heni; Prawiranegara, Barata Aditya; Utama, Panca Setia; Saputra, Edy
Journal of Applied Materials and Technology Vol. 6 No. 1 (2024): September 2024
Publisher : AMTS and Faculty of Engineering - Universitas Riau

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.31258/Jamt.6.1.30-36

Abstract

Two MnOx, namely ?-MnO2@Mn2O3 and ?-MnO2 catalyst, were successfully synthesized using two different organic acids, tartaric and maleic acid, as a reduction in the redox process of KMnO4. The obtained catalysts are used in the AOP degradation reaction for paper mill effluent. The organic content in the effluent is analogous to the COD number in the effluent. The degradation process is depicted as a decrease in the COD number. The catalyst properties were characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and N2 sorption. The obtained materials were then studied for PMS activation using Oxone® as a sulfate radical source for COD removal reactions. The ?-MnO2@Mn2O3, which is compromised by Mn (IV) and Mn (II, III), by using 0.3 gL-1 ?-MnO2@Mn2O3 has the best efficiency with almost 75% COD removal, higher than the ?-MnO2 catalyst. The activation energy of the ?-MnO2@Mn2O3 is measured up to 11.4 kJ mol-1.
Co-Authors Abid, Hussein Rasool Ahmad Fadli Amir Awaluddin Amun Amri Ari Sandhyavitri Azhar, Muhammad Rizwan Desi Heltina Edy Saputra Fajar Restuhadi Muhdarina Nurhayati Setia Utama, Panca Sugesti, Heni SYAIFUL BAHRI Utama, Panca Setia