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All Journal METANA Elkawnie Journal of Natural Science and Integration Chemistry Indonesian Journal of Chemical Research Biopedagogia Dirasah: Jurnal Pendidikan Islam
Amalia, Hilda Ayu Melvi
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Religion Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Education Engineering Environmental Science Other

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Journal : Chemistry Indonesian Journal of Chemical Research

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Synthesis of Glucopyranosyl Acetic from Sago Flour as Raw Material for the Synthetic Polymers Dali, Arniah; Dali, Nasriadi; Dali, Seniwati; Amalia, Hilda Ayu Melvi
Indonesian Journal of Chemical Research Vol 8 No 3 (2021): Edition for January 2021
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598/ijcr.2021.8-dal

Abstract

Synthesis of glucopyranosyl acetic from sago flour as raw material for the synthetic polymers has been successfully carried out. The synthesis product is obtained through two reaction stages, namely the hydrolysis and esterification reactions. Sago flour is hydrolyzed with 25% HCl and neutralized with 45% NaOH. Glucose hydrolysis of sago starch and acetic anhydride was esterified using a zinc chloride catalyst. Synthesis product was obtained as a white solid substance (57.31% recovery), a melting point of 110 - 111oC, and Rf 0.79 on TLC (SiO2, n-hexane: ethyl acetate = 9:1 v/v). The results of the analysis of synthesis products with FTIR and GC-MS spectrometers showed that the synthesis product was glucopyranosyl acetic or 2,3,4,6-tetra-O-acetyl glucopyranose.
Extraction of The Chemical Components of Dengen Leaves (Dillenia serrata Thunb) by MAE Method and Activity Test as Antioxidant and Toxicity Wela, Nasriadi Dali; Dali, Seniwati; Chairunnas, Armadi; Amalia, Hilda Ayu Melvi; Puspitasari, Sri Ayu Andini
Indonesian Journal of Chemical Research Vol 10 No 2 (2022): Edition for September 2022
Publisher : Jurusan Kimia, Fakultas Sains dan Teknologi, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2022.10-wel

Abstract

Research on the extraction of chemical components of Dengen (Dillenia serrata Thumb) leaves using the MAE (microwave-assisted extraction) method and activity as an antioxidant and toxicity test has been carried out. This study aimed to extract the chemical components of Dengen leaves using the MAE method and to test the antioxidant activity and toxicity of the ethanol extract of Dengen leaves. The chemical components of Dengen leaves were extracted by the MAE method and obtained ethanol extract with a yield of 47%. Dengen leaves ethanol extract was partitioned with n-hexane and ethanol as solvents and obtained yields of 5% (n-hexane) and 65% (ethanol). The chemical components of Dengen leave ethanol extract were identified by phytochemical screening. The results of phytochemical screening showed the presence of secondary metabolites of alkaloids, flavonoids, saponins, polyphenols, terpenoids, and steroids. The antioxidant activity test of the ethanol extract of Dengen leaves was carried out using the DPPH (2,2-diphenyl-1-picrihydrazil) method and obtained the value of IC50 = 100,363 ppm (strong antioxidant). A toxicity test of the ethanol extract of Dengen leaves was carried out using the BSLT (Brine Shrimp Lethality Test) method and obtained the value of LC50 = 18.3443 ppm (very toxic).
Co-Authors Awan, Rusdi Bidasari bidasari, Bidasari Chairunnas, Armadi Dali, Arniah Hasana, Fitratul Moh. Yahya Obaid, Moh. Yahya Nasriadi Dali Nunuk Hariani Soekamto Puspitasari, Sri Ayu Andini Rizalia, Syarif Rosmini Rosmini Seniwati Dali Sukmawati Sukmawati Sulaiman Sulaiman Syarifuddin, Syamsidar Haji Yunita, Ferni Zakaria Zakaria