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All Journal PROSIDING SEMINAR KIMIA KOVALEN: Jurnal Riset Kimia Jurnal Kimia Mulawarman JURNAL ATOMIK
Lianasari, Ika Yekti
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Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Energy Environmental Science

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Journal : JURNAL ATOMIK

 1 
PEMBUATAN DAN KARAKTERISASI ADSORBEN KITOSAN–SILIKA DAN PENGAPLIKASIAN TERHADAP ADSORPSI ION Cd2+ Nisa, Muflihatu Khoiratun; Lianasari, Ika Yekti; Koesnarpadi, Soerja
JURNAL ATOMIK Vol 7 No 1 (2022)
Publisher : Jurusan Kimia FMIPA UNMUL

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The Research has been conducted on the synthesis of chitosan-silica adsorbents from chitosan and silica derived from TEOS (Tetraethyl Orthosylicate). The chitosan-silica was made by mixing chitosan solution and silica soles that were previously chitosan we were added with acetic acid and silica solution we were added with aqueous solution, ethanol and HCl(p). The result from characterization of FT-IR chitosan-silica adsorbents indicates the presence of OH, NH2, Si-O, Si-O-Si, chitosan adsorbents that only have OH and NH2 groups and silica adsorbents that only have OH, Si-O and Si-O-Si groups. Application of chitosan, silica and chitosan-silica adsorbents to adsorp Cd2+ ion. Cd2+ ion concentration after adsorption was determined by atomic absorption spectrophotometer (AAS). Adsorption Cd2+ ion in chitosan-silica successfully indexed Cd2+ by 98.67% while for chitosan adsorbents by 97.87% and while silica adsorbents by 79.45%. The Sem results showed that when adsorbents before soaking with Cd2+ it was seen that the morphology of the surface of the pores adsorbent there is still a cavity then when after soaking with Cd2+ pores filled by ions Cd2+.
PENENTUAN VARIASI KOMPOSISI DAN pH OPTIMUM ADSORBEN KITOSAN-Fe3O4 BERDASARKAN PERSEN PENYERAPAN ION Pb2+ Lianasari, Ika Yekti; Koesnarpadi, Soerja; Pratiwi, Djihan Ryn; Munandar, Aris
JURNAL ATOMIK Vol 8 No 1 (2023)
Publisher : Jurusan Kimia FMIPA UNMUL

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Previously, the synthesis of Chitosan-Fe3O4 adsorbent from magnetite (Fe3O4) made from ferrous ammonium sulfate (III) and ferrous ammonium sulfate (II) in a ratio of 3:1 was carried out. The adsorbent is adjusted with the ratio of magnetite and chitosan composition 1:1; 1:2 and 2:1 with the help of glutaraldehyde as a crosslinker. The results showed that the ratio of the ideal composition is 1:1 with % absorption that is 94.97% in 24 hour, and the optimum pH is obtained at pH 5 with % absorption of 92.18% for Pb2+ ions.
PEMANFAATAN ARANG AKTIF DARI LIMBAH SERBUK GERGAJI KAYU BANGKIRAI (Shorea Laevifolia Eudert) SEBAGAI ADSORBEN ZAT WARNA RHODAMIN B Agustina, Linda; Sitorus, Saibun; Lianasari, Ika Yekti
JURNAL ATOMIK Vol 6 No 2 (2021)
Publisher : Jurusan Kimia FMIPA UNMUL

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Penelitian yang telah dilakukan mengenai pemanfaatan arang aktif dari limbah serbuk gergaji kayu bangkirai sebagai adsorben zat warna Rhodamin B. Arang aktif dikarakterisasi menggunakan Scanning Electron Microscopy (SEM). Didapatkan hasil karakterisasi SEM sebelum dikontakkan dengan Rhodamin B pada perbesaran 2.000 kali dan 5.000 kali bentuk morfologi permukaan seragam dan merata sedangkan sesudah dikontakkan dengan Rhodamin B pada perbesaran 2.000 kali dan 5.000 kali bentuk morfologi permukaan tidak seragam dan merata. Rhodamin B diadsorpsi oleh arang aktif dan diukur dengan menggunakan Spektrofotometer UV-Vis pada panjang gelombang maksimum 554 nm. Didapatkan hasil kondisi optimum pada proses adsorpsi Rhodamin B sebanyak 25 mL adalah pada massa adsorben 0,2 gram, konsentrasi Rhodamin B 3 ppm dan waktu adsorpsi 45 menit dengan % teradsorpsi sebesar 96,37%.
ADSORPSI ION LOGAM Pb2+ DENGAN ARANG AKTIF MAHKOTA NANAS (Ananas comosus (L.) Merr) TERMODIFIKASI KITOSAN Arsyakia, Tarisa; Koesnarpadi, Soerja; Lianasari, Ika Yekti
JURNAL ATOMIK Vol 10 No 1 (2025)
Publisher : Jurusan Kimia FMIPA UNMUL

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30872/ja.v10i1.1436

Abstract

Pineapple (Ananas comosus (L.) Merr) is one of the most widely produced plants in Indonesia. Pineapple crown can be classified as solid waste that has an impact on the environment. Another problem of environmental pollution is heavy metals such as lead. In this study, modification was carried out by adding chitosan to the activated charcoal prepared from pineapple crown powder waste. The purpose of this study was to determine the characterization of chitosan-modified pineapple crown activated charcoal using Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM), determine the optimum adsorption conditions based on variations in pH, contact time and concentration of Pb2+ metal and determine the percent absorption and adsorption capacity. The results of FT-IR characterization of pineapple crown charcoal, chitosan and chitosan-modified activated charcoal indicated the presence of O-H (streching), N-H, C-H (streching), C=C aromatic and C-H (bending) groups, and in pineapple crown charcoal and chitosan-modified pineapple crown activated charcoal also indicated C-O-C groups while chitosan indicated C-N groups. In the results of SEM characterization, pineapple crown charcoal has a smooth, chitosan has a rough and chitosan-modified activated charcoal has a slightly rough surface and is still tightly bound to each other. The optimum conditions for adsorption of chitosan-modified activated charcoal on Pb2+ metal ions at pH 4 with a contact time of 60 minutes and a concentration of 75 mg/L. The results of the adsorption capacity test at each pH variation, contact time and concentration of Pb2+ metal ions were 2.4154 mg/g, 14,89 mg/g and 15,1732 mg/g.
Co-Authors Alimuddin Aman Sentosa Panggabean Aris Munandar Arsyakia, Tarisa Bohari Bohari Bohari Yusuf Bohari Yusuf Djihan Ryn Pratiwi, Djihan Ryn Farlianti, Resma Lita Linda Agustina Nisa, Muflihatu Khoiratun Putri, Amelia Putri, Marlisa Roro Rumengan, Nur Khamillah Saibun Sitorus Soerja Koesnarpadi Subur P Pasaribu Terra, Patrycia Zulliani