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All Journal Urania Jurnal Ilmiah Daur Bahan Bakar Nuklir Rekayasa Mesin Majalah Kedokteran Gigi Indonesia
Ihwanul Aziz
PSTA BATAN
Dentistry Materials Science & Nanotechnology Mechanical Engineering

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Titanium oxide coating and acid etching on platelet activation in dental implants Maharani, Adella Syvia; Ismiyati, Titik; Aditama, Pramudya; Abdullah, Johari Yap; Aziz, Ihwanul
Majalah Kedokteran Gigi Indonesia Vol 10, No 1 (2024): April
Publisher : Faculty of Dentistry, Universitas Gadjah Mada

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22146/majkedgiind.94366

Abstract

Titanium is the most widely used dental implant material, but it requires surface treatment to improve osseointegration. While coating implants with TiO2, residue can arise, which may lead to contamination. To address this, 10% HF etching is added. This study investigated the effect of TiO2 coating using sputtering and HF etching on platelet activation in titanium dental implants. Laboratory experiments were conducted on titanium implants (Ø = 4 mm; length = 12 mm) treated with TiO2 coating and 10% HF etching. Twenty-four samples were divided into four groups (n = 6): Group I (TiO2), Group II (TiO2 + HF 5 min), Group III (TiO2 + HF 10 min), and Group IV (TiO2 + HF 20 min). Platelet activation was assessed using CD41 and CD62P expression markers. Data analysis employed one-way ANOVA and post hoc LSD test (p = 0.05). Platelet activation ranged from 20.31 ± 1.78% to 35.90 ± 3.81%. One-way ANOVA revealed a significant effect (p < 0.05) of both TiO2 coating and acid etching on activation. LSD post hoc test showed significant differences (p < 0.05) between all groups except for the 10 and 20-minute etching periods. TiO2 coating with 10 minutes of HF etching resulted in the optimal activation level.
PELAPISAN PERMUKAAN BAJA TAHAN KARAT AISI 304 DENGAN KHROM OKSIDA MENGGUNAKAN METODA SPUTTERING Sungkono, Sungkono; Setiawan, Jan; isfandi, Isfandi; Aziz, Ihwanul
Urania : Jurnal Ilmiah Daur Bahan Bakar Nuklir Vol 25, No 2 (2019): Juni, 2019
Publisher : website

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (332.581 KB) | DOI: 10.17146/urania.2019.25.2.5433

Abstract

PELAPISAN PERMUKAAN BAJA TAHAN KARAT AISI 304 DENGAN KHROM OKSIDA MENGGUNAKAN METODE SPUTTERING. Baja tahan karat digunakan sebagai bahan struktur reaktor daya tipe LWR, AGR dan LMFBR. Permasalahan bahan struktur yang timbul adalah ketahanan korosi rendah dan swelling dalam lingkungan iradiasi tinggi. Salah satu cara yang digunakan adalah melapisi permukaan kelongsong baja tahan karat dengan khrom oksida. Tujuan penelitian adalah mendapatkan karakter mikrostruktur, kekerasan mikro, dan senyawa yang terbentuk pada lapisan permukaan baja tahan karat AISI 304. Metode  yang digunakan adalah pelapisan permukaan SS 304 dengan metode DC-sputtering. Proses pelapisan menggunakan bahan pelapis berupa target khrom, argon sebagai gas sputter, yang didoping gas oksigen dengan konsentrasi bervariasi dari 0 – 50 %volume, arus 10 – 20 mA, dan waktu 1 - 3 jam. Karakterisasi lapisan meliputi pengamatan mikrostruktur menggunakan mikroskop optik, kekerasan dengan microhardness Vickers tester, dan senyawa dalam lapisan dengan X-ray difractometer. Hasil penelitian menunjukkan bahwa mikrostruktur base metal tersusun dari fasa austenit dan endapan karbida, antarmuka logam-lapisan terlihat jelas, serta lapisan kompak dan homogen dengan ketebalan cenderung naik dalam rentang   0 – 30 %volume, menurun pada 30 – 40 %volume, dan bertambah tebal pada 40 – 50 %volume gas O2  Kekerasan lapisan bertambah tinggi hingga doping gas oksigen 30 %volume, kemudian menurun hingga 50 %volume gas O2. Pada konsentrasi dopan tetap dengan arus 10 – 20 mA dan waktu proses 1 – 3 jam diketahui kekerasan lapisan permukaan SS 304 bertambah tinggi seiring dengan bertambah besarnya arus dan waktu sputtering. Pada konsentrasi dopan 30 %volume O2, arus 10 mA dan waktu 2 jam, lapisan yang terbentuk mengandung CrO2 Kata kunci: Karakterisasi, lapisan permukaan, bahan struktur, SS 304, mikrostruktur, kekerasan, senyawa lapisan.
EFFECT OF ANNEALING ON MICROSTRUCTURE AND HARDNESS OF FeNiCo ALLOYS SYNTHESIZED BY MECHANICAL ALLOYING Sutrisna, Sutrisna; Pamuji, Didit Setyo; Prasetiyo, Angger Bagus; Ababil, Ismail Zulpria; Aziz, Ihwanul
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1690

Abstract

Alloys based on Fe-Ni-Co are categorized as special nickel-based superalloys with braod application as magnetic sensors in electric motors, recording devices as well as for vehicle engine parts. The purpose of this study was to determine the physical and mechanical properties of Fe-Ni-Co materials synthesized by mechanical alloying method, then subjected to annealing temperature variation i.e 800oC, 900oC, and 1000oC for 1 hour. Test methods carried out by XRD-spectra to identify the phase, SEM and EDS mapping to determine the microstructure and composition together with micro hardness test to represent the mechanical properties of this FeNiCo alloys. The results of the XRD test showed that Co atoms and some Fe dissolved into the Ni crystal lattice tended to form a solid solution of g-Ni(Fe,Co). Microstructural observations at 900 OC after milling for 16 hours showed a fine and homogeneous grain structure. The highest hardness value was 421.5 kg/mm2 at 16 hours milling. The Fe-Ni-Co alloy exhibited a homogeneous microstructural distribution with a fine grain structure and high densification.
EFFECT OF ANNEALING ON MICROSTRUCTURE AND HARDNESS OF FeNiCo ALLOYS SYNTHESIZED BY MECHANICAL ALLOYING Sutrisna, Sutrisna; Pamuji, Didit Setyo; Prasetiyo, Angger Bagus; Ababil, Ismail Zulpria; Aziz, Ihwanul
Jurnal Rekayasa Mesin Vol. 15 No. 1 (2024)
Publisher : Jurusan Teknik Mesin, Fakultas Teknik, Universitas Brawijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.21776/jrm.v15i1.1690

Abstract

Alloys based on Fe-Ni-Co are categorized as special nickel-based superalloys with braod application as magnetic sensors in electric motors, recording devices as well as for vehicle engine parts. The purpose of this study was to determine the physical and mechanical properties of Fe-Ni-Co materials synthesized by mechanical alloying method, then subjected to annealing temperature variation i.e 800oC, 900oC, and 1000oC for 1 hour. Test methods carried out by XRD-spectra to identify the phase, SEM and EDS mapping to determine the microstructure and composition together with micro hardness test to represent the mechanical properties of this FeNiCo alloys. The results of the XRD test showed that Co atoms and some Fe dissolved into the Ni crystal lattice tended to form a solid solution of g-Ni(Fe,Co). Microstructural observations at 900 OC after milling for 16 hours showed a fine and homogeneous grain structure. The highest hardness value was 421.5 kg/mm2 at 16 hours milling. The Fe-Ni-Co alloy exhibited a homogeneous microstructural distribution with a fine grain structure and high densification.
Co-Authors Ababil, Ismail Zulpria Abdullah, Johari Yap Adella Syvia Maharani Angger Bagus Prasetiyo Didit Setyo Pamuji isfandi, Isfandi Jan Setiawan Pramudya Aditama Sungkono Sungkono Sutrisna Sutrisna Titik Ismiyati