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All Journal Buletin Peternakan VALENSI CHEMISTRY PROGRESS Bulletin of Chemical Reaction Engineering & Catalysis EduChemia: Jurnal Kimia dan Pendidikan Bulletin of Chemical Reaction Engineering & Catalysis
Siti Nurbayti
Program Studi Kimia Fakultas Sains Dan Teknologi UIN Syarif Hidayatullah Jakarta
Chemical Engineering, Chemistry & Bioengineering Chemistry Education Materials Science & Nanotechnology Veterinary Other

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Synthesis of ZnO-Fe3O4 Magnetic Nanocomposites through Sonochemical Methods for Methylene Blue Degradation Nanda Saridewi; Sri Komala; Agustino Zulys; Siti Nurbayti; Latifah Tulhusna; Adawiah Adawiah
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 3 Year 2022 (September 2022)
Publisher : Department of Chemical Engineering - Diponegoro University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.3.15492.650-660

Abstract

Textile industry waste can pollute the aquatic environment because it contains dye contaminants with very stable properties that are difficult to degrade naturally. However, dye contaminants degradation can be carried out by photodegradation using ZnO-Fe3O4 magnetic nanocomposite photocatalysts. This study aims to synthesize ZnO-Fe3O4 magnetic nanocomposite through a sonochemical method. Then measure their photocatalytic activity in methylene blue degradation. The best ZnO-Fe3O4 magnetic nanocomposite is made of ZnO:Fe3O4 mass ratio of 4:1 with a crystal size of 31.058 nm, a hexagonal crystal phase and a particle size of 173.23 nm. The ZnO-Fe3O4 magnetic nanocomposites (4:1) provides optimum degradation capacity of methylene blue under halogen lamp irradiation of 99.56 mg/g at pH 13. Furthermore, the ZnO-Fe3O4 magnetic nanocomposites had good stability in 10 cycles reaction with a degradation capacity of 99.24-99.75 mg/g. The photocatalytic degradation of methylene blue by ZnO-Fe3O4 occurs through the formation of free radical species with hydroxyl radicals as the dominant species that play an important role in the degradation process. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Synthesis and Antibacterial Activity of 1,3,5,7-Tetrahydroxy-9,10-Anthraquinone and Anthrone Derivatives Siti Nurbayti; Didin Mujahidin; Yana Maolana Syah
Jurnal Kimia Valensi Jurnal Kimia VALENSI Volume 8, No. 2, November 2022
Publisher : Syarif Hidayatullah State Islamic University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15408/jkv.v8i2.25279

Abstract

In this research, the synthesis of 1,3,5,7-tetrahydroxy-9,10-anthraquinone (1) and two anthrone derivatives, 1,3,5,7-tetrahydroxy-10H-anthracene-9-one (2) and 1-hydroxy-3,5,7,9-tetramethoxyanthracene (3) has been done. Compound 1 was synthesized by a symmetrical condensation reaction of 3,5-dihydroxybenzoic acid in concentrated sulfuric acid. Reduction of the carbonyl group in compound 1 with SnCl2/HCl-HOAc affords compound 2. Compound 3 was prepared by modifying the hydroxy groups of compound 2 by a methylation reaction. The synthesized compounds were identified using nuclear magnetic resonance spectroscopy (NMR) and a high-resolution mass spectrometry (HR-ESI-MS). The antibacterial activity test of the synthesized compounds against four pathogenic bacteria, Bacillus subtilis, Staphylococcus aureus, Escherichia coli, and Salmonella typhi, was carried out using the microdilution method. Compound 3 showed moderate activity against B. subtilis, E. coli and S. typhi with a MIC value of 37.5 µg/mL. Moderate activity was also shown by compound 2 against S. aureus, while compound 1 showed weak activity with a MIC value of 75 µg/mL against the four test bacteria.
Optimization of Biofuel Production from Used Cooking Oil Using Natural Zeolite Catalyst Isalmi Aziz; Siti Nurbayti; Reza Falepi
EduChemia (Jurnal Kimia dan Pendidikan) Vol 7, No 2 (2022)
Publisher : Department of Chemical Education Faculty of Teacher Training and Education Universitas Su

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30870/educhemia.v7i2.13892

Abstract

Petroleum is still the primary energy used in the world. Its diminishing production is the trigger to find alternative energy to replace it. Biofuel is an alternative energy that has the potential to replace petroleum because it is renewable, environmentally friendly, and easy raw material. Waste such as used cooking oil can be used as raw material for making biofuels. The low price can reduce the cost of biofuel production. The conversion of oil into biofuel can be done using catalytic cracking with natural zeolite as a catalyst. This study aims to determine the optimum conditions for making biofuel from used cooking oil and determine its physical and chemical properties. The catalytic cracking process is carried out using an autoclave reactor. Used cooking oil and natural zeolite were introduced into the reactor, and the reaction was carried out by varying the time (1, 2, 3 hours), temperature (325, 350, 375oC), catalyst concentration (3, 5, 7%), and catalyst size. The product is distilled to produce biofuel (liquid), gas, and residue. The optimization results show that 3 hours, a temperature of 375oC, a catalyst concentration of 7%, and a catalyst size of 180µm are the optimum conditions for catalytic cracking with 44.94% biofuel yield. The resulting biofuel contains 73.48% hydrocarbons and 26.52% fatty acids. The hydrocarbon composition consists of 19.32% gasoline, 12.82% kerosene, and 35.11% diesel. The density of the biofuel produced is 0.8835g/mL, the flashpoint is 68oC, and the pourpoint is 27oC.
Synthesis of ZnO-Fe3O4 Magnetic Nanocomposites through Sonochemical Methods for Methylene Blue Degradation Nanda Saridewi; Sri Komala; Agustino Zulys; Siti Nurbayti; Latifah Tulhusna; Adawiah Adawiah
Bulletin of Chemical Reaction Engineering & Catalysis 2022: BCREC Volume 17 Issue 3 Year 2022 (September 2022)
Publisher : Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.9767/bcrec.17.3.15492.650-660

Abstract

Textile industry waste can pollute the aquatic environment because it contains dye contaminants with very stable properties that are difficult to degrade naturally. However, dye contaminants degradation can be carried out by photodegradation using ZnO-Fe3O4 magnetic nanocomposite photocatalysts. This study aims to synthesize ZnO-Fe3O4 magnetic nanocomposite through a sonochemical method. Then measure their photocatalytic activity in methylene blue degradation. The best ZnO-Fe3O4 magnetic nanocomposite is made of ZnO:Fe3O4 mass ratio of 4:1 with a crystal size of 31.058 nm, a hexagonal crystal phase and a particle size of 173.23 nm. The ZnO-Fe3O4 magnetic nanocomposites (4:1) provides optimum degradation capacity of methylene blue under halogen lamp irradiation of 99.56 mg/g at pH 13. Furthermore, the ZnO-Fe3O4 magnetic nanocomposites had good stability in 10 cycles reaction with a degradation capacity of 99.24-99.75 mg/g. The photocatalytic degradation of methylene blue by ZnO-Fe3O4 occurs through the formation of free radical species with hydroxyl radicals as the dominant species that play an important role in the degradation process. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). 
Co-Authors Adawiah Adawiah Agustino Zulys Arif Rahman Arif Rahman Hakim Badrul Ulum Badrul Ulum Christie Adi Octavia Didin Mujahidin Fira Luthfiana Isalmi Aziz Juwita Suwandari La Ode Sumarlin Latifah Tulhusna Lisa Adhani Lisa Adhani Muhammad Akbar Tafdila Nana Mulyana Nanda Saridewi, Nanda Putri Amanda Reza Falepi Solly Aryza Sri Komala Suharyono Soharyono Syifa Fauziah Teguh Wahyono Wahyu Permata Yana Maolana Syah