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Journal : Al-Kimia

Pengujian Aktivitas Antibakteri Minyak Atsiri Jahe (Zingiber Officinale Roscoe) Terhadap Bakteri Staphylococcus Aureus dan Escherichia Coli Sufriyana Ali; Maswati Baharuddin; Sappewali Sappewali
Al-Kimia Vol 1 No 2 (2013): December
Publisher : Study Program of Chemistry - Alauddin State Islamic University of Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (347.992 KB) | DOI: 10.24252/al-kimia.v1i2.1629

Abstract

Testing the antibacterial activity of the Essential Oil of Ginger (Zingiber officinale Roscoe) against bacteria Staphylococcus aureus and Escherichia coli. Purpose of this study is to determine the bacterial growht and activity test active compounds in ginger essential oils that can be used as an antibacterial to inhibit the growth of bacteria. This research uses a method soxhletation with solvent n- hexane to obtain the essential oil of ginger, making the media NA, rejuvenation bacteria, the manufacture of bacterial inoculum and suspension test. Antibacterial activity test using paper disc diffusion method in the form and method of dilution and analysis using GC-MS instrument. Antibacterial activity test result using paper disc method with a concentration of 25%,  50%, 75% and 100% in S. aureus (12, 34; 19, 42; 17, 34; 21, 7) mm and E. coli (10, 56; 13, 76; 16, 5; 23, 6) mm, while the result of the minimum inhibitory concentration (MIC) using ginger essential oil dilution method in S. aureus not found and E. coli at a concentration of 100%. The results of the analysis of essential oil components by GC-MS showed the active compounds in the form of compounds containing hydroxyl groups such as nerol, β- eusdesmol, borneol and compounds containing phenolic groups like zingerone.
Modifikasi Biodiesel Melalui Reaksi Oksidasi Menggunakan Gelombang Ultrasonik Aisyah Aisyah; Sappewali Sappewali; Nurlina Nurlina
Al-Kimia Vol 1 No 2 (2013): December
Publisher : Study Program of Chemistry - Alauddin State Islamic University of Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (280.822 KB) | DOI: 10.24252/al-kimia.v1i2.1633

Abstract

Biodiesel is an alternative energy fuel that is sustainable and environmentally safe. However, biodiesel has a higher cloud point than fuel diesel because it contains several saturated fatty acids such as oleic acid, linoleic and linolenic acid so that biodiesel tend to solidify at a temperature higher than the freezing point of diesel. This study aims to modify biodiesel from candlenut oil (Aleurites moluccana) through oxidation reaction by KMnO4 using ultrasonic equipment. The products obtained were analyzed using FTIR and GCMS instrument. FTIR analysis showed that spectral data of the four modified samples which run in 20, 30, 40 and 50 minutes practically similar. The methyl ester products are characterized by typical bands at specific frequencies such as stretch of C = O; C-C; C-H (sp3) and = C-H (sp2). Fragmentation patterns by GCMS showed that the oxidation reaction in 20, 30, 40 and 50 minutes did not undergo bond disconnection. The components produced is methyl palmitate, methyl linoleate, methyl oleate, heksadekanoat acid, 9, 12 and 9,17oktadekadienal oktadekadienoat acid.
Isolasi dan Identifikasi Bakteri Pendegradasi Fenol yang Bersumber Dari Danau Tempe Kabupaten Wajo Sulawesi Selatan Fitriana Fitriana; Maswati Baharuddin; Sappewali Sappewali
Al-Kimia Vol 4 No 2 (2016): December
Publisher : Study Program of Chemistry - Alauddin State Islamic University of Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (847.388 KB) | DOI: 10.24252/al-kimia.v4i2.1694

Abstract

Water pollution in Tempe Lake was consequence by people activity in around of  Tempe Lake, such as domestic waste and agriculture waste. One of the dangerous pollutions which was resulted from the waste was phenol pollution. Phenol waste reduction efforts on Tempe Lake could be solved by biodegradation process using bacteria. This research aimed to: 1) Get the bacteria which was able to degrade phenol on samples sourced from Tempe Lake, Wajo South Sulawesi and 2) Identify the type of bacteria that can degrade phenol sourced from Lake Tempe, Wajo South Sulawesi. The Metods used in the research was making of media, isolation and purification of bacteria, identification of bacteria and testing the ability of phenol degradation. Bacterial identification tests include staining gram and biochemical tests (TSIA, SIM, MR-VP, urea, citric and sugar fermentation). The degradation test was performed using UV-Vis spectrophotometry with colorimetric method using follin reagent. The results showed that the bacterial identified as the genus Enterobacter spp and Klebsella spp which were gram negative bacteria. Test  of phenol degradation at 48 hour incubation using UV-Vis shows that bacterial isolates C1F was able to degrade phenol 500 ppm to 3,091 ppm, bacterial isolate S1F was able to degrade phenol 500 ppm to 5,1153 ppm and bacterial isolate H2F was able to degrade phenol 500 ppm to 7,7834 ppm.
Sintesis dan Karakterisasi Hidroksiapatit Dari Tulang Ikan Tuna (Thunnus Albacores) Dengan Xrf, Ftir, Dan Xrd St Chadijah; Hardiyanti Hardiyanti; Sappewali Sappewali
Al-Kimia Vol 6 No 2 (2018): December
Publisher : Study Program of Chemistry - Alauddin State Islamic University of Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24252/al-kimia.v6i2.5067

Abstract

Hydroxyapatite (Hap) were inorganic compounds with constituent of bones and teeth has the molecular formula Ca5(PO4)3OH. Synthesis of hydroxyapatite can be done with  hydrothermal method  with calcium precursors tuna fish bone calcination process to obtain calcium compounds in the form   of calcium oxide. Calsium wich has been obtained added  phosphate precursor NH4H2PO4 0.547 M. On research conducted long stirring time variation and its effect on rendement and the resulting crystallites products. As for the variation of the long time of stirring used are 1, 2, 3, 4 and 5 hours. The optimum time of formation of hydroxyapatite obtained within 3 hours stirring from which content was 96.4156%. The material was analyzed by FTIR,XRF and XRD. Results showed their characterization by FTIR indicated the presence of OH groups,PO4  and CO3.  Based on the resulting diffraction of  XRF and XRD analysis, crystallite size obtained each of 41,9753  within 2 hours of stirring structure was hexagonal.
Analisis Sifat Fisika Kimia Tanah dan Uji Daya Hambatnya terhadap Bakteri Air Liur AnjingLiar Sjamsiah Sjamsiah; Arifuddin Arifuddin; Mashuri Masri; Sappewali Sappewali; Indah Islamiah; Hardiyanti Hamrullah; Elmika Nesti
Al-Kimia Vol 7 No 1 (2019): JUNE
Publisher : Study Program of Chemistry - Alauddin State Islamic University of Makassar

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24252/al-kimia.v7i1.7940

Abstract

This study aims to analyze the physical and chemical properties of soil from paddy fields, garden lands and city area also determine the soil inhibitory test of dog saliva bacteria. The results showed that these three soil types have different physical chemical properties and have different inhibitory zones against dog saliva bacteria. The physical chemistry of soil from paddy fields, garden lands and city area (0 cm) are as follows: for color; dark chocolate; grayish brown; and blackish ash, for texture: clay; clay; and sandy clay, for moisture content: 7.14; 6.53; 2.13. for pH close to neutral around 6.52-7.03; Total N is low (0.08-0.23); organic C compounds are classified as moderate; nutrient content of Ca/Mg is classified as moderate (9.55 /1.70 - 14.89/2.22); cation exchange capacity is classified as high (25.32-29.03) in paddy fields and gardens and compounds. The inhibitory zone of the highest dog saliva bacteria is in garden soil (3.7 cm), then paddy soil (2.86 cm) and land in the city area (1.6 cm).