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All Journal Jurnal RISET Geologi dan Pertambangan INTEKNA Chimica et Natura Acta LEMBARAN PUBLIKASI MINYAK DAN GAS BUMI
Anggoro Tri Mursito
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Agriculture, Biological Sciences & Forestry Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Computer Science & IT Earth & Planetary Sciences Economics, Econometrics & Finance Electrical & Electronics Engineering Energy Environmental Science Materials Science & Nanotechnology Other

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Journal : Jurnal RISET Geologi dan Pertambangan

 1 
The Characteristics of Padamarang Magnesite under Calcination and Hydrothermal Treatment Mutia Dewi Yuniati; Feronika Cinthya Mawarni Putri Wawuru; Anggoro Tri Mursito; Iwan Setiawan; Lediyantje Lintjewas
JURNAL RISET GEOLOGI DAN PERTAMBANGAN Vol 29, No 2 (2019)
Publisher : Indonesian Institute of Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14203/risetgeotam2019.v29.1016

Abstract

Magnesite (MgCO3) is the main source for production of magnesium and its compound. In Indonesia, magnesite is quite rare and can be only found in limited amount in Padamarang Island, Southeast Sulawesi Provence. Thus the properties of magnesite and the reactivity degree of the obtained product are of technological importance. The aim of this work was to analyze the characteristics of Padamarang magnesite under calcination and hydrothermal treatment processes. The processes were carried out at various temperatures with range of 150-900°C for 30 minutes. The solids were characterized with respect to their chemical and physical properties by using scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDX), Fourier-transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD). SEM image indicates that magnesite was formed from thin and flat hexagon sheets. The FTIR and XRD analysis disclose that MgO formed at temperature above 300°C, where as the magnesite sample also lost its mass around 50%. These results demonstrate that Padamarang magnesite decomposes to magnesium oxide and carbon dioxide at high temperature.Magnesit (MgCO3) merupakan sumber utama untuk produksi magnesium dan senyawa-senyawanya. Di Indonesia, magnesit cukup jarang dan hanya dapat ditemukan dalam jumlah yang terbatas di Pulau Padamarang, Propinsi Sulawesi Tenggara. Oleh karena itu sifat magnesit dan derajat reaktivitas dari produk-produk magnesit penting untuk diketahui. Penelitian ini bertujuan untuk menganalisis karakteristik magnesit Padamarang dengan perlakuan kalsinasi dan hidrothermal.  Proses dilakukan pada temperatur yang bervariasi dari 150-900°C selama 30 menit. Sifat kimia dan fisika dari magnesit dikarakterisasi dengan menggunakan scanning electron microscopy dengan energy-dispersive X-ray spectroscopy (SEM-EDX), Fourier-transform infrared spectroscopy (FTIR), dan X-ray diffraction (XRD). Gambar dari analisis SEM menunjukkan bahwa magnesit terbentuk dari lembaran-lembaran heksagonal yang tipis dan datar. Hasil analisis dengan FTIR dan XRD menunjukkan bahwa MgO terbentuk pada temperatur diatas 300°C, dimana sampel magnesit juga kehilangan massanya sekitar 50% pada suhu tersebut. Hal ini menunjukkan bahwa Magnesit Padamarang terdekomposisi menjadi magnesium oksida dan karbon dioksida pada temperatur tinggi.
RAPID EX SITU COLLECTION AND THERMAL BEHAVIOR ANALYSIS OF VOLATILE ORGANIC MATTERS BY THERMAL EXTRACTION CONE CHAMBER FOR HIGH UN-BURNT CARBON COAL FLY ASH Anggoro Tri Mursito
JURNAL RISET GEOLOGI DAN PERTAMBANGAN Vol 15, No 1 (2005)
Publisher : Indonesian Institute of Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (757.489 KB) | DOI: 10.14203/risetgeotam2005.v15.188

Abstract

A thermal extraction cone chamber system has been modified to measure differential thermal functions and products where overall volatile organic matters are lost to the environment during heating. The aims of the research are to analyze and measure the thermal behavior of high un-burnt carbon coal fly ash derived from textile industrial power in Bandung. Efforts are being made to find the solution in large-scale utilization for alternative energy based on their by product. The sample analysis show that volatile organics matter exceed 30%, which means that others oxides element content are independently favorable. The modified cone chamber can collect the sample up to the total volumes of 30% of the chamber. In contrast to traditional chamber sample collectors, the modified cone extracts volatile organics matter from high un-burnt carbon coal ash divided in two treatments. Results show that the energy of pyrolisis, direct combustion or simple carbonization can be recovered (20%-42%) from wet or dry sample, with extraction efficiency compound-specific. During the direct combustion experimentation, resulted to the embedded energy is pushing up to 2790C for the average of volatile organic matters of 34% and for pyrolisis experimentation is 3300C for average volatile organic matters of 30%. The maximum thermal productivity values of 80 minutes for the direct combustion is 10220C and for pyrolisis is 10310C, and the contrary of 10 minutes, for the direct combustion is 7430C and for pyrolisis is 7010C
Peningkatan Daya Serap Karbon Aktif Terhadap Ion Logam Hexavalent Chromium (CrVI) Melalui Modifikasi Dengan Cationic Surfactant (Ethylinediamine) Eko Tri Sumarnadi Agustinus; Anggoro Tri Mursito; Happy Sembiring
JURNAL RISET GEOLOGI DAN PERTAMBANGAN Vol 23, No 1 (2013)
Publisher : Indonesian Institute of Sciences

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1398.372 KB) | DOI: 10.14203/risetgeotam2013.v23.66

Abstract

ABSTRAK Karbon aktif telah digunakan sebagai adsorban dalam pengolahan limbah cair industri dan terbukti mampu menyerap ion logam berat seperti Hg, Cu, Fe, namun kurang efektif terhadap ion logam hexavalent chromium (Cr.VI). Salah satu upaya peningkatan daya serap karbon aktif dapat dilakukan melalui modifikasi dengan cationic surfactant (Ethylinediamine, EDA), yakni dengan mengubah tegangan permukaan karbon aktif dari yang bersifat hydrophobic menjadi hydrophilic. Tujuan penelitian ini adalah untuk memperoleh prototip SMAC (Surfactant Modified Activated Carbon), yakni karbon aktif yang dimodifikasi dengan surfaktan, sehingga mempunyai daya serap tinggi terhadap ion logam hexavalent chromium (Cr.VI). Guna mencapai tujuan tersebut dilakukan treatment karbon aktif dari batubara dengan metoda batch. Parameter kimia dan fisika yang meliputi perubahan pH, suhu proses, waktu kontak, konsentrasi surfaktan dan berat karbon aktif digunakan sebagai parameter eksperimen. Mekanisme pembentukan prototip SMAC yang menyangkut karakteristik penyerapan diobservasi melalui analisis X-RD (X-Ray Diffractometer), FTIR (Fourier Transformer Infra Red), sedangkan daya serap terhadap ion logam hexavalent chromium (Cr.VI) diamati melalui analisis UV Spectrophotometry. Hasil eksperimen menunjukkan bahwa peningkatan daya serap karbon aktif termodifikasi (SMAC) terhadap  ion logam hexavalent chromium (CrVI) sebesar dua kali lipat dibandingkan dengan karbon aktif biasa, dicapai pada kondisi pH 2, konsentrasi karbon aktif 5 g/liter dalam waktu kontak 2 jam.
Co-Authors Eko Tri Sumarnadi Agustinus Fachruzzaki, Fachruzzaki Feronika Cinthya Mawarni Putri Wawuru Grandistin, Ghea Gristannia HANDAYANI, ISMI Happy Sembiring Isnaniawardani, Vijaya Iwan Setiawan Lediyantje Lintjewas Mutia Dewi Yuniati Praptisih Praptisih Praptisih Vijaya Isnaniawardani Yoga Andriana Sendjaja Yoga Andriana Sendjaja, Yoga Andriana Yuliani, Galuh