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Journal : Science and Technology Indonesia

Calcium oxide from Pomacea canaliculata and Babylonia spirata snails Triayu Septiani; Nurlisa Hidayati; Risfidian Mohadi
Science and Technology Indonesia Vol. 2 No. 3 (2017): July
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (444.253 KB) | DOI: 10.26554/sti.2017.2.3.68-70

Abstract

The preparation of CaO from golden snail (Pomacea canaliculata) and lion snail (Babylonia spirata) through decomposition at various temperature i.e 700o, 800o, 900o and 1000oC during 3 hours has been carried out. Calcium oxide from decomposition was characterized using X-Ray diffractometer. Furthermore, the characterization was continued using FT-IR spectrophotometer and determination of surface area using BET analysis. The results showed that the optimum temperature for preparation of CaO from golden snail and lion snail at 900oC with 2q values are: 32.2° , 37.4o , 54o , 64.2o , 67.3° and 32.4°, 37.5°, 67.5 °, respectively. FT-IR spectra showed characteristic vibrations for the Ca-O in the sample golden snail and lion snail combustion products at a temperature of 900oC. Ca-O absorption of golden snail samples in the wavenumber around 362.62 cm-1 and lion snail seen in wavenumber around 384.76 cm-1 indicating the presence of Ca-O vibration of the metal oxide of preparation. Golden snail and the lion snail combustion at 900oC temperature of each sample which has a surface area of 20.495 m2/g, while the lion snail 17.308 m2/g. The pore diameter of golden snail 3.753 nm and 11.319 nm of lion snail. All CaO can be categorized as mesoporous material. Keywords: golden snail, lion snail, decomposition, CaO
Synthesis and Characterization Chitosan-ZnO nanoparticle and Its Application as Antibacterial Agent of Staphylococus aureus ATCC 25923 Ahmad Fatoni; Ensiwi Munarsih; Kadek Asmadi; Nurlisa Hidayati
Science and Technology Indonesia Vol. 5 No. 1 (2020): January
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (1652.629 KB) | DOI: 10.26554/sti.2020.5.1.1-5

Abstract

The synthesis of modified chitosan has been studied. The aims of this research were modification of chitosan with ZnO nanoparticle to form chitosan-ZnO nanoparticle and its application as antibacterial agent of Staphylococus aureus. Characterization of modified chitosan was conducted using FTIR spectroscopy and X-Ray diffractometer. ZnO nanoparticle was synthesized by leaf extract of Sirih hijau (piper betle L) and zinc acetate dihydrate. Modified chitosan was synthesized by chitosan and ZnO nanoparticle. Modified chitosan solution can act as antibacterial agent with paper disk method. The result showed that chitosan can be modified with ZnO nanoparticle and detected at wave number of 3427 cm−1. The crystalline size of ZnO nanoparticle is 16.47 nm. The average inhibition zone of chitosan-ZnO nanoparticle at concentration 10.000, 5.000 and 2.500 ppm are 28.87 ± 0.4 ; 24.93 ± 0.15 and 19.35 ± 0.3 mm respectively.
CuO Nanoparticles : Biosynthesis, Characterization and In Vitro Study Ahmad Fatoni; Reza Agung Sriwijaya; Umy Habiba; Nurlisa Hidayati
Science and Technology Indonesia Vol. 6 No. 1 (2021): January
Publisher : Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (2336.259 KB) | DOI: 10.26554/sti.2021.6.1.25-29

Abstract

The biosynthesis of CuO nanoparticles was studied. The aims of this research were biosynthesis CuO nanoparticles from Cu2+ion solution and leaves aquoeus extract of sweet star fruit and its in vitro study as antibacterial agent of Escherichia coli. CuO nanoparticles was characterized using FTIR spectroscopy and X-Ray diffractometer. CuO nanoparticles was synthesized by reaction between Cu2+ion solution and leaves aquoeus extract of sweet star fruit. Paper disk method was used as the application of the suspension of CuO nanoparticles. The result showed that Cu-O groups detected at wave number of 503, 619, 767 and 821 cm-1. Diffractogram of CuO nanoparticles had sharp and narrow diffraction peaks. The crystallite size of CuO nanoparticles was 4.25 nm. The average inhibition zone of CuO nanoparticles at concentration 10.000, 7.500, 5.000 and 2.500 ppm was 17.43 ± 1.81 ; 15.73 ± 0.40 ; 14.50 ± 2.96 and 9.67 ± 0.28 mm respectively.