Article Per Year (5 Year)
p-Index From 2020 - 2025
1.152
P-Index
This Author published in this journals
All Journal EKSAKTA: Journal of Sciences and Data Analysis Jurnal Ilmu Dasar Teknosains: Media Informasi Sains dan Teknologi Biology, Medicine, & Natural Product Chemistry Indonesian Journal of Chemistry Aplikasia: Jurnal Aplikasi Ilmu-Ilmu Agama ALKIMIA : Jurnal Ilmu Kimia dan Terapan
Susy Yunita Prabawati
Program Studi Kimia, Fakultas Sains Dan Teknologi, UIN Sunan Kalijaga Yogyakarta Jl. Laksda Adisucipto, Yogyakarta
Religion Agriculture, Biological Sciences & Forestry Humanities Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Civil Engineering, Building, Construction & Architecture Computer Science & IT Control & Systems Engineering Earth & Planetary Sciences Environmental Science Materials Science & Nanotechnology Mathematics Medicine & Pharmacology Physics Public Health Social Sciences Other

Published : 8 Documents Claim Missing Document
Claim Missing Document
Check
Articles

Found 1 Documents
Search
Journal : EKSAKTA: Journal of Sciences and Data Analysis

 1 
Grinding Technique on Synthesis of Calixarene and Its Derivatives Prabawati, Susy Yunita; Mufidati, Afifah; Ratna Djuwita, Titis; Ratna Djuwita, Titis; Nur Ngaini, Siti
EKSAKTA: Journal of Sciences and Data Analysis VOLUME 1, ISSUE 2, August 2020
Publisher : Fakultas Matematika dan Ilmu Pengetahuan Alam

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20885/EKSAKTA.vol1.iss2.art4

Abstract

The synthesis of p-t-butylcalix[6]arene (PK[6]A) and calixresorcinarene derivative compounds, namely C-para-dimethylamino-phenylcalix[4]resorcinarene (CPDAK[4]R) and C-4-hydroxy-phenylcalix[4]-resorcinarene (CHK[4]R), had been carried out by grinding technique. The grinding technique was done with the absence of solvents so that it minimized the waste. Synthesis occurred through electrophilic substitution reactions with KOH as an alkaline catalyst and p-toluene sulfonic acid as an acid catalyst. The three calixarene products were in the form of crystalline solids with a melting point of more than 300°C, insoluble in water with yields of 62.58; 61.94 and 97.49%, respectively. Product characterization using FTIR analysis showed the vibration of the methylene bridge (-CH2-) at a wavenumber of 1473.62 cm-1 and LC-MS analysis for (PK[6]R) showed that the molecular weight was 974.77 g/mole. While the analysis of (CPDAK[4]R) and (CHK[4]R) with 1H NMR showed the presence of protons from the methine bridge (-CH-) that appear at the chemical shift of  4.950 and 3.078 ppm.
Co-Authors Abdul Aziz Astuti, Ratih Dwi Damayanti Iskandar Diza Harris Pratiwi Imelda Fajriati Jumina Jumina Mufidati, Afifah Mustofa Mustofa Nur Ngaini, Siti Ratna Djuwita, Titis Risnandar, Ade Irfan Sri Juari Santosa Triatmaja, Karisma Widiakongko, Priyagung Dhemi Wulandari, Teti Wulan