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All Journal TELKOMNIKA (Telecommunication Computing Electronics and Control) Spektra: Jurnal Fisika dan Aplikasinya Journal of Physics and Its Applications International Journal of Remote Sensing and Earth Sciences (IJReSES) PROSIDING SEMINAR NASIONAL FISIKA (E-JOURNAL) Metalurgi Journal of Engineering and Technological Sciences
Triyono, Djoko
Department Of Physics, Faculty Mathematics And Natural Sciences, Universitas Indonesia.
Aerospace Engineering Astronomy Automotive Engineering Chemical Engineering, Chemistry & Bioengineering Civil Engineering, Building, Construction & Architecture Computer Science & IT Earth & Planetary Sciences Electrical & Electronics Engineering Energy Industrial & Manufacturing Engineering Materials Science & Nanotechnology Physics Other

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SYNTHESIS OF NICRALX MICROPARTICLES USING DRY MILLING AND WET MILLING PROCESSES Ramandhany, Safitry; Triyono, Djoko; Sugiarti, Eni; Desiati, Resetiana Dwi; Sundawa, Risma Yulita
Metalurgi Vol 38, No 2 (2023): Metalurgi Vol. 38 No. 2 2023
Publisher : National Research and Innovation Agency (BRIN)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.55981/metalurgi.2023.713

Abstract

The characteristics of synthesized NiCrAlY and NiCrAlZr composite powders produced by the milling process were investigated to understand the particle size, the shape of particles, and the properties of crystalline structure. The milling process was carried out by combining dry milling with the wet milling method to prevent agglomeration, produce a homogeneous alloy powder, and reduce the particle size. Ethanol was used during the wet milling process as a process control agent. The PSA (particle size analysis) showed that the particle size was effectively reduced from ±70 μm to less than 30 μm. In addition, surface structure analysis characterized by SEM (scanning electron microscope) revealed that particle shape changed from blocky particles after dry milling into flaky, flattened, and fragmented particles after wet milling. An XRD (x-ray diffraction) was used to identify the phases of powders before and after the mechanical milling process. Crystal structure analysis was calculated from the change of peak broadening in XRD peak spectra. The Williamson-hall method has been performed to calculate the strain and crystallite size of synthesized NiCrAlY and NiCrAlZr composite powder in the present study. The findings in this study show the characteristics of powders, which are important information for producing coatings with good performance.
Surface Enhanced Raman Spectroscopy with La0.5Bi0.5FeO3-Based Substrates for Paraquat Pesticide Detection Tiawati, Nia; Triyono, Djoko; Shiddiq, Muhandis
Journal of Physics and Its Applications Vol 7, No 2 (2025): May 2025
Publisher : Diponegoro University Semarang Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.14710/jpa.v7i2.26211

Abstract

Paraquat is a highly toxic herbicide that poses serious environmental and health risks. Conventional detection methods are accurate but often complex and time-consuming. This study explores the use of La0.5Bi0.5FeO3 (LBFO) perovskite as a novel Surface-Enhanced Raman Spectroscopy (SERS) substrate. LBFO was synthesized via a sol-gel method and characterized using XRD, XRF, UV-Vis, and Raman spectroscopy. The LBFO-based substrate successfully enhanced the Raman signals of paraquat, enabling detection at concentrations as low as 6 ppm. These results suggest the feasibility of LBFO as an effective and low-cost SERS substrate for rapid paraquat detection.
Sensitive Detection of Rhodamine B Using Surface Enhanced Raman Spectroscopy with a BiFeO3 based Substrate Mayora, Diva Cassia; Triyono, Djoko; Shiddiq, Muhandis; Rafsanjani, Rifqi Almusawi; Alaih, Akhmad Futukhillah Fataba
Journal of Engineering and Technological Sciences Vol. 57 No. 6 (2025): Vol. 57 No. 6 (2025): December
Publisher : Directorate for Research and Community Services, Institut Teknologi Bandung

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.5614/j.eng.technol.sci.2025.57.6.10

Abstract

Surface-Enhanced Raman Spectroscopy (SERS) is a highly effective technique for detecting trace amounts of molecular species. However, the widespread use of conventional noble metal substrates is limited by high fabrication costs and scalability issues. Perovskite materials have recently emerged as promising alternatives, though many are lead-based and pose environmental risks. In this study, we present a lead-free bismuth ferrite (BiFeO₃) perovskite synthesized via the sol–gel method as a novel SERS substrate for the detection of Rhodamine B, a toxic dye commonly used illicitly in food products. Comprehensive characterization using X-ray Diffraction (XRD), X-ray Fluorescence (XRF), and UV-Visible Diffuse Reflectance Spectroscopy confirmed the successful formation of a single-phase rhombohedral structure with a direct bandgap of 2.1 eV, indicating strong visible-light absorption. The BiFeO₃ substrate demonstrated effective SERS performance, facilitating a detection of Rhodamine B at concentrations as low as 10 ppm. These results highlight the potential of lead-free BiFeO₃ perovskites as practical and environmentally friendly alternatives to noble metals for SERS-based detection of hazardous dyes and other environmental contaminants.
Co-Authors Affi Nur Hidayah Alaih, Akhmad Futukhillah Fataba Aliyah, Nada Alfi Amaliya, Septiana Tri Ayom Widipaminto Azzahra, Ridha Octa Alhuriyyah Cassia, Diva Dedi Irawadi Donna Monica Eni Sugiarti Erna Sri Adiningsih Indah Prasasti Indah Prasasti Isnaeni Isnaeni Iwan Sugihartono Jalu Tejo Nugroho Jalu Tejo Nugroho Jansen Sitorus Jansen Sitorus Khalifah Insan Nur Rahmi Khomarudin, Muhammad Rokhis Mayora, Diva Cassia Mohar, Rahmat Setiawan NFn Suwarsono Rafsanjani, Rifqi Almusawi Rahmat Arief Ramandhany, Safitry Resetiana Dwi Desiati, Resetiana Dwi Rokhmatuloh Rokhmatuloh Rokhmatuloh, Rokhmatuloh Rosari Saleh Shiddiq, Muhandis Soewoto, Haswi Purwandanu Sundawa, Risma Yulita Suwarsono Suwarsono Suwarsono Suwarsono Tiam, Tan Swee Tiawati, Nia Yohanes Fridolin Hestrio Yudasari, Nurfina Yuliati Herbani Yuvita Dian Safitri